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    SOLID-PIGMENT FORMULATIONS
    31.
    发明专利
    SOLID-PIGMENT FORMULATIONS 未知

    公开(公告)号：AU9192982A

    公开(公告)日：1983-07-07

    申请号：AU9192982

    申请日：1982-12-24

    Applicant: BASF AG

    Inventor： BELDE HORST ,  HARTMANN EDUARD ,  DAUBACH EWALD

    IPC: C09B67/00 ,  C09B67/20 ,  C09B67/46 ,  C09D17/00 ,  C09C1/20 ,  C09C1/24 ,  C09C1/36 ,  C09C1/56 ,  C09C3/08 ,  C09D11/02

    Abstract: Highly concentrated, dust-free, solid and readily dispersible pigment formulations contain (a) from 70 to 95% by weight of one or more finely divided pigments, (b) from 5 to 30% by weight of one or more surfactants which possess 20-45% by weight of ethylene oxide units, have a mean molecular weight of from 4,000 to 15,000 and are obtained by reacting an amine of the formula where R is C2-C6-alkylene, R1 is H or C1-C4-alkyl and n is 1, 2, 3, 4 or 5, or R is 1,3-phenylene, 1,4-phenylene or 4,4'-diphenylenemethane, R1 is H and n is 1, with propylene oxide and then reacting the product with ethylene oxide, and (c) from 0 to 5% by weight of waxes and/or antifoams, with or without (d) other agents conventionally used in pigment formulations, the percentages being based on (a+b+c). The formulations are very useful for pigmenting aqueous, alcoholic or aqueous/alcoholic printing inks and surface coatings, and printing pastes for textiles.

    Readily dispersible pigment form with high colouring strength - prepd. by grinding crude copper phthalocyanine and heating in organic solvent
    32.
    发明专利
    Readily dispersible pigment form with high colouring strength - prepd. by grinding crude copper phthalocyanine and heating in organic solvent 未知

    公开(公告)号：DE2933896A1

    公开(公告)日：1981-03-12

    申请号：DE2933896

    申请日：1979-08-22

    Applicant: BASF AG

    Inventor： ROTH KARL ,  SAPPOK REINHARD DIPL CHEM DR ,  BELDE HORST ,  DAUBACH EWALD DIPL CHEM DR

    IPC: C09B67/12 ,  C09B67/00 ,  C09B1/00

    Abstract: Copper phthalocyanine (CuPc) was converted to a form suitable for colouring use by grinding the crude prod. until it consisted of agglomerates composed of particles whose mean size was 0.05 microns or less, suspending the ground material in the 0.8-10 fold (pref. 2-8 fold) amt. by wt. of an organic solvent (1), and heating to 20-180 deg.C (pref. 50-150 deg.C) until the desired colouring strength was attained. Crude CuPc-prepd. e.g. by fusing a mixt. of o-phthalodinitrile and CuCl in anhyd. Na2SO4, and freed from salt by H2O treatment prior to grinding (10-40 hours in a ball mill, pref. 25-35 hours) - has a chlorine content of 2-4 wt.%. (1) may be amino-2-8C-alkanols (pref. 3-aminopropanol), mono- or bi-nuclear 6-membered aromatic nitrogen heterocycles (pref. pyridine), N,N-di(1-8C alkyl) amides of 1-3C carboxylic acids, N-methyl(or cyclohexyl)pyrrolid-2-one, or mixts. of these solvents. Depending on the organic solvent used, the pigment form was isolated from the mixt. either by direct filtration at 80-120 deg.C (or after treatment with H2O or aq. mineral acid) or by first removing the solvent by steam distn. and then filtering the resulting aq. suspension. The CuPc pigment forms have excellent dispersibility and high colouring strength.

    Dispersant for dyes and pigments - based on phenolsulphonic acid, urea and formaldehyde condensate
    33.
    发明专利
    Dispersant for dyes and pigments - based on phenolsulphonic acid, urea and formaldehyde condensate 未知

    公开(公告)号：DE2327579A1

    公开(公告)日：1975-01-02

    申请号：DE2327579

    申请日：1973-05-30

    Applicant: BASF AG

    Inventor： DAUBACH EWALD DIPL CHEM DR ,  KLINGSHIRN WERNER DIPL CHEM DR ,  BELDE HORST

    IPC: C08G14/08

    Abstract: Light-fast condensates are prepd. by (i) condensing 0.5-1.5 mol. pts. of >=1 phenolsulphonic acid, free from uncondensed rings, with 0.8-2 mol. pts. urea and 1-3 mol. pts. HCHO or HCHO-yielding cpds., (ii) neutralising reaction mixt. with a base, (iii) after condensation with 0.3-1.5 mol. pts. of at least one mono- to deca-hydric (2-10)C alcohol and 0.5-1.5 mol. pts. HCHO or HCHO-yielding cpd. and (iv) neutralising. Condensates are used as dispersants pref. for pigments/dyes, partic. those sensitive to reduction, e.g. dispersion dyes for dyeing polyester fabrics; also in leather and textile industry.

    Aqs pigment dispersions - for addition to white pigments or distempers
    34.
    发明专利
    Aqs pigment dispersions - for addition to white pigments or distempers 未知

    公开(公告)号：DE2156603A1

    公开(公告)日：1973-05-24

    申请号：DE2156603

    申请日：1971-11-15

    Applicant: BASF AG

    Inventor： BELDE HORST ,  OPPENLAENDER KNUT DR ,  DAUBACH EWALD DR ,  FIKENTSCHER ROLF DR

    IPC: C08G65/26 ,  C08L71/02 ,  C09B67/42 ,  C09D101/02 ,  C09B67/00

    Abstract: The aqs. pigment dispersion which is non-flocking in plastics dispersions or distempers contg. cellulose ethers, contains, calc. on (a+b+c): (a) 20-55% of a finely divided pigment; (b) 5-25% of a water sol. surfactant or a mixture thereof, obtained by reacting (1) amines of formula (I): N2N-(R.R'N)n-H (I) (where R is satd. 2-6C alkylene; R' is H, 1-6C alkyl, or phenyl; n is 1-5 and when n is 1 the gp. NHR' may be linked with the other amino gp.) or (2) aromatic or cycloaliphatic diamines, with (3) 3-50 mol. propylene oxide per equivalent of reactive amino H, and then (4) with 2-70 mol. ethylene oxide per equivalent reactive amino H, and (c) 40-75% water or mixture of water and a water-reserving agent.

    Water-dispersable preparations of water-insoluble dyes
    38.
    发明专利
    Water-dispersable preparations of water-insoluble dyes 未知

    公开(公告)号：GB1043490A

    公开(公告)日：1966-09-21

    申请号：GB3686265

    申请日：1965-08-27

    Applicant: BASF AG

    Inventor： DAUBACH EWALD ,  PREUGSCHAS HELMUT ,  WAECHTER RUDOLF ,  BELDE HORST ,  VESCIA MICHELE ,  BEST MANFRED

    IPC: C09B67/00 ,  C09B67/42 ,  C09B67/46

    Abstract: A water-dispersible powder or paste preparation of a water-insoluble dye contains at least one sodium salt of a water-soluble condensation product of (I) a naphthalene monosulphonic acid or derivative thereof and formaldehyde or (II) a mononuclear aromatic compound capable of reacting with 2 moles of formaldehyde, a napthol sulphonic acid, formaldehyde and optionally sodium sulphite, the content of inorganic salt in said preparation being less than 5%, preferably 0.5% by weight of compound (I) or (II). Products (I) and (II) may be prepared free from salts from the start by a conventional method or the conventional industrial product may be freed from salts by dialysis, ion exchange, electrolysis or precipitation with organic liquids. The preparations may also contain urea or thiourea as dispersion assistants. Suitable dyes are vat or disperse dyes. The preparations may be prepared by grinding, kneading or spray drying. Suitable products (I) and (II) are specified and examples are given.

    40.
    发明专利
    未知

    公开(公告)号：ES2077335T3

    公开(公告)日：1995-11-16

    申请号：ES92120624

    申请日：1992-12-03

    Applicant: BASF AG

    Inventor： BELDE HORST ,  HERRMANN MANFRED DR ,  LEPPMEIER FRANZ DR ,  LACH DIETRICH DR

    IPC: C09B67/00 ,  C09B67/20 ,  C09D17/00 ,  C09D125/00 ,  C09D125/08 ,  C14C11/00

    Abstract: Pigment preparations useful for pigmenting or delustering finishes for leather and leather substitutes consist essentially of pigments or delusterants or a mixture thereof, binders, water and if desired further customary dispersants and auxiliaries, the binders used being copolymers of A) from 40 to 80% by weight of at least one aromatic vinyl compound of the general formula I (* CHEMICAL STRUCTURE *) I where R1, R2 and R3 are each hydrogen, methyl or ethyl and n is 1 or 2, B) from 20 to 60% by weight of acrylic acid or methacrylic acid or a mixture thereof, and C) from 0 to 10% by weight of further copolymerizable monomers, in the form of their salts.

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