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公开(公告)号:DE59904662D1
公开(公告)日:2003-04-24
申请号:DE59904662
申请日:1999-09-21
Applicant: BASF AG
Inventor: ADRIAN TILL , BESSLING BERND , HASSE HANS , VANSANT FRANS , THEIS GERHARD
Abstract: A process for the distillative recovery of high purity monoethylene glycol from the hydrolysis product of ethylene oxide by pressure dewatering, vacuum dewatering and subsequent purifying distillation, which includes the pressure dewatering columns or at least the first pressure dewatering column of the battery (2, 3, 4) having a stripping section with at least one separating stage, preferably with from 2 to 10 separating stages, particularly preferably with from 3 to 6 stages, and a portion of the overhead stream of the pressure dewatering column(s) (2, 3, 4) having a stripping section being removed from the system.
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公开(公告)号:AT234799T
公开(公告)日:2003-04-15
申请号:AT99952457
申请日:1999-09-21
Applicant: BASF AG
Inventor: ADRIAN TILL , BESSLING BERND , HASSE HANS , VANSANT FRANS , THEIS GERHARD
Abstract: A process for the distillative recovery of high purity monoethylene glycol from the hydrolysis product of ethylene oxide by pressure dewatering, vacuum dewatering and subsequent purifying distillation, which includes the pressure dewatering columns or at least the first pressure dewatering column of the battery (2, 3, 4) having a stripping section with at least one separating stage, preferably with from 2 to 10 separating stages, particularly preferably with from 3 to 6 stages, and a portion of the overhead stream of the pressure dewatering column(s) (2, 3, 4) having a stripping section being removed from the system.
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公开(公告)号:NO20023514A
公开(公告)日:2002-08-22
申请号:NO20023514
申请日:2002-07-23
Applicant: BASF AG
Inventor: AUER HEINZ , BESSLING BERND , HAMMER HANS , HASSE HANS , SAUER FRIEDRICH , VICARI MAXIMILIAN , ADRIAN TILL
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公开(公告)号:NO20023481L
公开(公告)日:2002-08-21
申请号:NO20023481
申请日:2002-07-22
Applicant: BASF AG
Inventor: AUER HEINZ , BESSLING BERND , HAMMER HANS , HASSE HANS , SAUER FRIEDRICH , VICARI MAXIMILIAN , ADRIAN TILL
Abstract: The invention relates to a process for obtaining anhydrous or substantially anhydrous formic acid, in which firstly aqueous formic acid is prepared by hydrolysis of methyl formate and is freed from water in the subsequent work-up. The process has the special feature that steam, which is employed for the hydrolysis of methyl formate and for heating a distillation column serving for work-up, is also used as stripping steam for waste-water stripping. The stripped waste water is produced during work-up.
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公开(公告)号:ES2161380T3
公开(公告)日:2001-12-01
申请号:ES96938088
申请日:1996-11-05
Applicant: BASF AG
Inventor: BESSLING BERND , ZECK SEBASTIAN , PLUCKHAN JURGEN , MAYER THOMAS , LOFFLER ULRICH , SPIEGEL GUNTER
IPC: B01D3/00 , B01D3/16 , C07D301/32 , C07D303/02 , C07D303/04
Abstract: PCT No. PCT/EP96/04818 Sec. 371 Date May 18, 1998 Sec. 102(e) Date May 18, 1998 PCT Filed Nov. 5, 1996 PCT Pub. No. WO97/19069 PCT Pub. Date May 29, 1997A process for distilling ethylene oxide out of a mixture including ethylene oxide in a column at an absolute pressure of from 2 to 10 bar and a temperature of 20 to 180 DEG C. by withdrawing pure ethylene oxide in the liquid or gaseous state overhead or via a sidestream in the rectifying section of the column includes effecting the distillation in a column having on its inside a plurality of successive zones of structured sheet-metal packing or dumped beds of packing elements, these zones being assigned one or more extinguishing systems on the outside of the column.
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公开(公告)号:AU3541601A
公开(公告)日:2001-08-07
申请号:AU3541601
申请日:2001-01-12
Applicant: BASF AG
Inventor: AUER HEINZ , BESSLING BERND , HAMMER HANS , HASSE HANS , SAUER FRIEDRICH , VICARI MAXIMILIAN , ADRIAN TILL
Abstract: The invention relates to a process for obtaining anhydrous or substantially anhydrous formic acid, in which firstly aqueous formic acid is prepared by hydrolysis of methyl formate and is freed from water in the subsequent work-up. The process has the special feature that steam, which is employed for the hydrolysis of methyl formate and for heating a distillation column serving for work-up, is also used as stripping steam for waste-water stripping. The stripped waste water is produced during work-up.
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37.
公开(公告)号:AU2848701A
公开(公告)日:2001-08-07
申请号:AU2848701
申请日:2001-01-24
Applicant: BASF AG
Inventor: AUER HEINZ , BESSLING BERND , HAMMER HANS , HASSE HANS , SAUER FRIEDRICH , VICARI MAXIMILIAN , WAGNER GERHARD , ADRIAN TILL
Abstract: The invention relates to a process for obtaining anhydrous or substantially anhydrous formic acid in which, during the work-up, a compound of the general formula Iwhere the radicals R1 and R2 are alkyl, cycloalkyl, aryl or aralkyl groups, or R1 and R2 jointly, together with the N atom, form a heterocyclic 5- or 6-membered ring, and only one of the radicals is an aryl group, and where R3 is hydrogen or a C1-C4-alkyl group,is employed simultaneously as extractant for formic acid and as antifoam for a distillation process.
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公开(公告)号:BR9913891A
公开(公告)日:2001-07-03
申请号:BR9913891
申请日:1999-09-21
Applicant: BASF AG
Inventor: ADRIAN TILL , BESSLING BERND , HASSE HANS , VANSANT FRANS , THEIS GERHARD
Abstract: A process for the distillative recovery of high purity monoethylene glycol from the hydrolysis product of ethylene oxide by pressure dewatering, vacuum dewatering and subsequent purifying distillation, which includes the pressure dewatering columns or at least the first pressure dewatering column of the battery (2, 3, 4) having a stripping section with at least one separating stage, preferably with from 2 to 10 separating stages, particularly preferably with from 3 to 6 stages, and a portion of the overhead stream of the pressure dewatering column(s) (2, 3, 4) having a stripping section being removed from the system.
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公开(公告)号:CA2345140A1
公开(公告)日:2000-03-30
申请号:CA2345140
申请日:1999-09-21
Applicant: BASF AG
Inventor: HASSE HANS , THEIS GERHARD , VANSANT FRANS , ADRIAN TILL , BESSLING BERND
Abstract: The invention relates to a method for obtaining highly pure monoethylene glycol from the product of hydrolysis of ethylene oxide by distillation, by means of dehydration under pressure, preferably in a cascade, vacuum dehydration and subsequent pure distillation. According to the inventive method, the pressure dehydration column or at least the first pressure dehydration column of the cascade (2, 3, 4) has a stripping section with at least one separation stage, preferably 2-10 separation stages, especially 3- 6 stages, and in that part of the top flow of the dehydration column(s) (2, 3, 4) is sluiced out with the stripping section.
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公开(公告)号:AU8855898A
公开(公告)日:1999-01-25
申请号:AU8855898
申请日:1998-07-03
Applicant: BASF AG
Inventor: BESSLING BERND , KNAB JEAN WERNER , BROX WOLFGANG , LOHE BERND
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