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公开(公告)号:AU4758400A
公开(公告)日:2000-12-12
申请号:AU4758400
申请日:2000-05-23
Applicant: BASF AG
Inventor: MOHRSCHLADT RALF , HILDEBRANDT VOLKER , KRAUSS DIETER , LEEMANN MARTIN
Abstract: In a process for producing polyamides, a mixture comprising hexamethylenediamine and aminocapronitrile and obtained from the hydrogenation of adiponitrile is reacted with water and a dicarboxylic acid.
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公开(公告)号:CA2374367A1
公开(公告)日:2000-11-30
申请号:CA2374367
申请日:2000-05-23
Applicant: BASF AG
Inventor: LEEMANN MARTIN , KRAUSS DIETER , MOHRSCHLADT RALF , HILDEBRANDT VOLKER
Abstract: The invention relates to a method for the production of polyamides, wherein a mixture consisting of hexamethylene diamine and aminocapronitrile obtained b y hydrogenating adipodinitrile is reacted with water and a dicarboxylic acid.
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33.
公开(公告)号:CZ20002837A3
公开(公告)日:2000-11-15
申请号:CZ20002837
申请日:1999-01-29
Applicant: BASF AG
Inventor: MOHRSCHLADT RALF , KRAUSS DIETER , HILDEBRANDT VOLKER
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34.
公开(公告)号:CZ67599A3
公开(公告)日:1999-06-16
申请号:CZ67599
申请日:1997-08-26
Applicant: BASF AG
Inventor: WEISS ROBERT , KRAUSS DIETER , KELLER DIETER , PIPPER GUNTER , HARDER WOLFGANG , LUDWIG ALFONS , MOHRSCHLADT RALF
Abstract: A process for preparing a polyamide by reacting at least one aminonitrile with water comprises:(1) reacting at least one aminonitrile with water at a temperature from 100 to 360° C. and a pressure from 0.1 to 35x106 Pa to obtain a reaction mixture,(2) further reacting the reaction mixture at a temperature from 150 to 400° C. and a pressure which is lower than the pressure in step 1, the temperature and the pressure being selected so as to obtain a first gas phase and a first liquid or a first solid phase or a mixture of first solid and first liquid phase, and the first gas phase is separated from the first liquid or the first solid phase or from the mixture of first liquid and first solid phase, and(3) admixing the first liquid or the first solid phase or the mixture of first liquid and first solid phase with a gaseous or liquid phase comprising water at a temperature from 150 to 360° C. and a pressure from 0.1 to 30x106 Pa to obtain a product mixture.
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公开(公告)号:TR9900422T2
公开(公告)日:1999-04-21
申请号:TR9900422
申请日:1997-08-26
Applicant: BASF AG
Inventor: WEISS ROBERT , KRAUSS DIETER , KELLER DIETER , PIPPER GUNTER , HARDER WOLFGANG , LUDWIG ALFONS , MOHRSCHLADT RALF
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公开(公告)号:TR199900422T2
公开(公告)日:1999-04-21
申请号:TR9900422
申请日:1997-08-26
Applicant: BASF AG
Inventor: WEISS ROBERT , KRAUSS DIETER , KELLER DIETER , PIPPER GUNTER , HARDER WOLFGANG , LUDWIG ALFONS , MOHRSCHLADT RALF
Abstract: A process for preparing a polyamide by reacting at least one aminonitrile with water comprises:(1) reacting at least one aminonitrile with water at a temperature from 100 to 360° C. and a pressure from 0.1 to 35x106 Pa to obtain a reaction mixture,(2) further reacting the reaction mixture at a temperature from 150 to 400° C. and a pressure which is lower than the pressure in step 1, the temperature and the pressure being selected so as to obtain a first gas phase and a first liquid or a first solid phase or a mixture of first solid and first liquid phase, and the first gas phase is separated from the first liquid or the first solid phase or from the mixture of first liquid and first solid phase, and(3) admixing the first liquid or the first solid phase or the mixture of first liquid and first solid phase with a gaseous or liquid phase comprising water at a temperature from 150 to 360° C. and a pressure from 0.1 to 30x106 Pa to obtain a product mixture.
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公开(公告)号:CA2264023A1
公开(公告)日:1998-03-05
申请号:CA2264023
申请日:1997-08-26
Applicant: BASF AG
Inventor: MOHRSCHLADT RALF , LUDWIG ALFONS , KRAUSS DIETER , PIPPER GUNTER , KELLER DIETER , HARDER WOLFGANG , WEISS ROBERT
Abstract: A process for producing a polyamide by reacting at least one aminonitrile with water has the following steps: (1) at least one aminonitrile is reacted with water at a temperature from 100 to 360 ~C and pressure from 0.1 to 35.x 106 Pa, yielding a reaction mixture; (2) the reaction mixture is further reacted at a temperature from 150 to 400 ~C and pressure lower than the pressure in step 1. The temperature and pressure are selected to yield a first gaseous phase and a first liquid or solid phase or a mixture of a first solid and a first liquid phase. The first gaseous phase is separated from the first liquid or solid phase or the mixture of a first liquid and a first solid phase is separated; and (3) the first liquid or solid phase or the mixture of a first liquid and first solid phase is mixed with a water-containing gaseous or liquid phase at a temperature from 150 to 360 ~C and pressure from 0.1 to 30 x 106 Pa, yielding a product mixture. Also disclosed are other embodiments of this process and the thus produced polyamides.
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