Conversion of pyridazinium salts - by anion exchange

    公开(公告)号:DE2211662A1

    公开(公告)日:1973-09-20

    申请号:DE2211662

    申请日:1972-03-10

    Applicant: BASF AG

    Abstract: Originally issued as Basic No. 58387 U-E in Week U 40. Pyridazinium salts are converted by transferring a neutral pyridazine deriv. which is the basis of the starting pyridazinium salt, from an aq. soln. of the starting pyridazinium salt into the org. phase by addn. of bases and simultaneous extraction with an org. solvent which is water-immiscible or only difficultly miscible with water; sepg. the aq. phase; admixing the org. phase with an acid contg. the desired anion; and isolating the resulting pyridazinium salt in known manner.

    1 subst 4 amino 6 pyridazones with herbicidal - activity

    公开(公告)号:DE1966312A1

    公开(公告)日:1972-03-09

    申请号:DE1966312

    申请日:1969-03-13

    Applicant: BASF AG

    Abstract: 1-Subst-4-amino-6-pyridazones with herbicidal activity Title cpds. are 1-R-4-X-5-Y-6-pyridazones where R is phenyl or aralkyl (opt. subst. by halogen, alkyl, alkoxy or haloalkyl) or cyclohexyl (opt. subst by halogen, or alkyl), Y is H, halogen, alkoxy or mercaptoalkyl and X is cyclopropanecarboxamido, (m-alkanoylaminophenoxy) carbonylamino, (m-alkoxycarbonylaminophenoxy)carbonylamino, N'-cycloalkyl-N'-hydroxy-ureido or N'-chlorosulphonyl-ureido; X can also be NH2 or acetamido when Y is H or is aralkyl. The cpds. may be prepd. by reacting corr. 4-isocyrindopyridazines with m-acylaminophenols or hydroxylamines, by reacting 4-aminopyridazones with chlorosulphonyl isocyanate or cyclopropanecarboxylic acid chloride, by reacting 4,5-dihalopyridazones with NH3, or by reacting 4-amino-5-chloropyridazones with hydrogen.

    1 subst 4 amino 6 pyridazones with herbicidal - activity

    公开(公告)号:DE1966313A1

    公开(公告)日:1972-02-17

    申请号:DE1966313

    申请日:1969-03-13

    Applicant: BASF AG

    Abstract: 1-Subst-4-amino-6-pyridazones with herbicidal activity Title cpds. are 1-R-4-X-5-Y-6-pyridazones where R is phenyl or aralkyl (opt. subst. by halogen, alkyl, alkoxy or haloalkyl) or cyclohexyl (opt. subst by halogen, or alkyl), Y is H, halogen, alkoxy or mercaptoalkyl and X is cyclopropanecarboxamido, (m-alkanoylaminophenoxy) carbonylamino, (m-alkoxycarbonylaminophenoxy)carbonylamino, N'-cycloalkyl-N'-hydroxy-ureido or N'-chlorosulphonyl-ureido; X can also be NH2 or acetamido when Y is H or is aralkyl. The cpds. may be prepd. by reacting corr. 4-isocyrindopyridazines with m-acylaminophenols or hydroxylamines, by reacting 4-aminopyridazones with chlorosulphonyl isocyanate or cyclopropanecarboxylic acid chloride, by reacting 4,5-dihalopyridazones with NH3, or by reacting 4-amino-5-chloropyridazones with hydrogen.

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