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    CRYSTALLINE MODIFICATION OF FIPRONIL
    33.
    发明专利
    CRYSTALLINE MODIFICATION OF FIPRONIL 未知

    公开(公告)号：NZ576639A

    公开(公告)日：2012-03-30

    申请号：NZ57663907

    申请日：2007-11-05

    Applicant: BASF SE

    Inventor： SAXELL HEIDI EMILIA ,  ERK PETER ,  TARANTA CLAUDE ,  KROHL THOMAS ,  COX GERHARD ,  DESIRAJU GAUTAM R ,  BANERJEE RAHUL ,  BHATT PRASHANT M ,  SUKOPP MARTIN ,  SCHERER STEFAN ,  OJALA ANTTI

    IPC: A01N25/00 ,  A01N47/02 ,  A01P7/00

    Abstract: Disclosed is a process for preparing solid fipronil comprising at least 85 percent by weight of the crystalline modification I of fipronil being present in the monoclinic system having the centrosymmetric space group C2/c comprising the steps of: step i) preparing a solution of a solid form of fipronil being different from the crystalline modification I in a solvent S comprising at least one acetonitrile, dimethylsulfoxide, or at least one benzene derivative; step ii) effecting crystallization of fipronil; and step iii) isolating the resulting precipitate wherein, in case the solvent S is pure acetonitrile, the crystallization step ii) is conducted at temperatures below 40 degrees Celsius and in case the solvent S is pure dimethylsulfoxide, the crystallization step ii) is conducted at temperatures below 80 degrees Celsius.

    CRYSTALLINE MODIFICATIONS TO PYRACLOSTROBIN
    35.
    发明专利
    CRYSTALLINE MODIFICATIONS TO PYRACLOSTROBIN 未知

    公开(公告)号：RS51954B

    公开(公告)日：2012-02-29

    申请号：RSP20110475

    申请日：2006-06-19

    Applicant: BASF SE

    Inventor： ERK PETER ,  KROEHL THOMAS ,  COX GERHARD ,  ZIEGLER HANS ,  MAYER WINFRIED ,  SCHNEIDER KARL-HEINRICH ,  VOGELBACHER UWE JOSEF ,  NOACK RAINER ,  GOETZ ROLAND ,  WUCKELT JOERG ,  RAULS MATTHIAS

    IPC: A01N47/24 ,  C07D231/22

    Abstract: Crystalline modification IV of pyraclostrobin (A) exhibits at least three reflexes in an X-ray powder diffractogram at 25[deg]C, where the reflections (d) are 6.02 +- 0.01 Å, 4.78 +- 0.01 Å, 4.01 +- 0.01 Å, 3.55 +- 0.01 Å and 3.01 +- 0.01 Å. Independent claims are included for: (1) the preparation of (A); (2) crystalline modification II of pyroclostobin (A1) exhibiting at least four reflexes in a X-ray powder diffractogram at 25[deg]C, where the reflections (d) are 5.93 +- 0.01 Å, 5.82 +- 0.01 Å, 4.89 +- 0.01 Å, 4.78 +- 0.01 Å, 4.71 +- 0.01 Å, 3.97 +- 0.01 Å, 3.89 +- 0.01 Å, 3.77 +- 0.01 Å, 3.75 +- 0.01 Å, 3.57 +- 0.01 Å and 3.43 +- 0.01 Å; (3) the preparation of (A1); and (4) a plant protection agent, which comprises pyraclostrobin in the form of modification IV or in the form of modification II and carrier materials and/or additives. ACTIVITY : Fungicide. MECHANISM OF ACTION : None given.

    PIGMENTOS DE PERILENO NEGROS.
    39.
    发明专利
    PIGMENTOS DE PERILENO NEGROS. 未知

    公开(公告)号：ES2359831T3

    公开(公告)日：2011-05-27

    申请号：ES05701347

    申请日：2005-02-04

    Applicant: BASF SE

    Inventor： ERK PETER ,  STOHR ANDREAS ,  BOEHM ARNO ,  KURTZ WALTER ,  MIZUGUCHI JIN ,  SENS BENNO

    IPC: C09B5/62 ,  C09B67/22

    Abstract: Pigmentos de perileno negros que contienen uno de los isómeros de las fórmulas Ia o Ib en la cual las variables tienen el siguiente significado: R 1 , R 2 son independientemente uno de otro fenileno, naftileno o piridileno, que pueden estar en cada caso sustituidos una o varias veces por alquilo C1-C12, alcoxi C1-C6, hidroxi, nitro y/o halógeno; X es halógeno; n es 0 a 4, o contienen una mezcla de ambos isómeros y en un esmalte de secado al horno de alquid/melamina exhiben un valor negro >=210.

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