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公开(公告)号:JP2014139190A
公开(公告)日:2014-07-31
申请号:JP2014031226
申请日:2014-02-21
Applicant: Basf Se , ビーエーエスエフ ソシエタス・ヨーロピアBasf Se
Inventor: HEIDI EMILIA SAXELL , ERK PETER , CLAUDE TARANTA , KROEHL THOMAS , COX GERHARD , DESIRAJU GAUTAM R , RAHUL BANERJEE , BHATT PRASHANT M
IPC: C07D231/44 , A01N25/00 , A01N25/04 , A01N25/14 , A01N47/02 , A01P5/00 , A01P7/00 , A01P7/04 , A61K31/415 , A61P33/10 , A61P33/14
CPC classification number: A01N47/02 , A01N2300/00
Abstract: PROBLEM TO BE SOLVED: To provide a novel crystalline transformation of fipronyl, and a method for producing said crystalline transformation, and also a composition for combating pests and parasites.SOLUTION: Use of a novel crystalline transformation IV of fipronyl of formula I below that exists in a triclinic crystalline system having center symmetric space group P-1. Said fipronyl is dissolved into acetone and crystallized to obtain crystalline transformation IV, and which is used, as it is (crystalline transformation IV), as a composition for controlling pests. High purity fipronyl of said crystalline transformation IV is a raw material for converting to crystalline transformation IV by further tempering the crystalline transformation IV at 90 to 100°C, or to crystalline transformation V by tempering at 100 to 130°C.
Abstract translation: 要解决的问题:提供呋喃尼基的新型结晶转化及其生产所述结晶转化的方法,以及用于防治害虫和寄生虫的组合物。解决方案:使用存在下述式I的呋喃基的新结晶转化IV 具有中心对称空间群P-1的三斜晶系。 将所述氟虫酰基溶于丙酮中并结晶,得到结晶转化IV,并将其作为(结晶转化IV)用作防治害虫的组合物。 所述结晶转变IV的高纯度fipronyl是通过在90至100℃进一步回火结晶转变IV或通过在100至130℃回火的结晶转变V而转化为结晶转变IV的原料。
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公开(公告)号:JP2012067107A
公开(公告)日:2012-04-05
申请号:JP2011229798
申请日:2011-10-19
Applicant: Basf Se , ビーエーエスエフ ソシエタス・ヨーロピアBasf Se
Inventor: ZIEGLER HANS , MAYER UINFRIED , KROEHL THOMAS , SCHNEIDER KARL-HEINRICH , COX GERHARD , ERK PETER , VOGELBACHER UWE JOSEF , NOACK RAINER , GOETZ ROLAND , WUCKELT JOERG , RAULS MATTHIAS
IPC: C07D231/22 , A01N47/24 , A01P3/00
CPC classification number: A01N47/24 , C07D231/22 , A01N25/04 , A01N25/02 , A01N2300/00
Abstract: PROBLEM TO BE SOLVED: To provide a novel crystalline modification to pyraclostrobin, and to provide a method for production and use of the novel modification for the production of a plant protection agent.SOLUTION: The crystalline modification II to pyraclostrobin shows at least four reflections represented by formula in an X-ray powder diffraction figure at 25°C.
Abstract translation: 要解决的问题:为了提供一种新的嘧菌酯的结晶改性,并提供生产和使用植物保护剂生产的新型修饰方法。 解决方案:在25℃的X射线粉末衍射图中,结晶修饰II至吡咯烷四唑基显示出由式表示的至少四个反射。 版权所有(C)2012,JPO&INPIT
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公开(公告)号:JP2014139188A
公开(公告)日:2014-07-31
申请号:JP2014031221
申请日:2014-02-21
Applicant: Basf Se , ビーエーエスエフ ソシエタス・ヨーロピアBasf Se
Inventor: HEIDI EMILIA SAXELL , ERK PETER , CLAUDE TARANTA , KROEHL THOMAS , COX GERHARD , GAUTAM R DESIRAJU , RAHUL BANERJEE , PRASHANT M BHATT
CPC classification number: A01N47/02 , A01N2300/00
Abstract: PROBLEM TO BE SOLVED: To provide a novel crystalline transformation of fipronyl of the formula below that was found and of which characteristics were determined, and a novel method for producing said crystalline transformation with high yield while excluding the production of other crystalline transformed forms, also a mixture and composition for killing insects and parasites comprising said crystalline transformation, and a method of their use for combating pests and parasites.SOLUTION: A crystalline transformation of fipronyl that has a particular X-ray powder diffraction chart, and undergoes, at 105°C to 145°C, phase transformation to two other crystalline transformations respectively having melting points of 196 to 197°C and 202 to 203°C.
Abstract translation: 要解决的问题:为了提供下面所公开的下列式子基的新型结晶转变,其特征是确定的,以及一种新的制备高产率的结晶转化同时排除其它结晶转化形式的生产的新方法 用于杀死昆虫和包含所述结晶转化的寄生虫的混合物和组合物及其用于防治害虫和寄生虫的方法。解决方案:具有特定X射线粉末衍射图的fipronyl的结晶转化并在105° C至145℃,相转变为分别具有196至197℃和202至203℃的熔点的两个其它结晶转化。
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公开(公告)号:JP2014141494A
公开(公告)日:2014-08-07
申请号:JP2014031217
申请日:2014-02-21
Applicant: Basf Se , ビーエーエスエフ ソシエタス・ヨーロピアBasf Se
Inventor: HEIDI EMILIA SAXELL , ERK PETER , CLAUDE TARANTA , KROEHL THOMAS , COX GERHARD , MARTIN SUKOPP , STEFAN SCHERER , ANTTI OJALA , GAUTAM R DESIRAJU , RAHUL BANERJEE , PRASHANT M BHATT
IPC: C07D231/38 , A01N47/02 , A01P7/04 , A61K9/10 , A61K31/415 , A61P33/00 , A61P33/10 , A61P33/14
CPC classification number: A01N43/56 , A01N47/02 , A01N2300/00
Abstract: PROBLEM TO BE SOLVED: To provide a fipronyl crystal allowing easy filtration and drying with less dust in a production procedure and a composition which is blended with the crystal, has formulation stability and is for insecticidal and parasiticidal mixtures.SOLUTION: A solid fipronyl is present as a monoclinic system having a center-symmetry space group C2/c, shows a specific reflection in an X-ray powder diffraction diagram recorded at 25°C by using Cu-Kα radiation rays and contains at least 85 wt.% of a crystal transformation I of fipronyl. A method of producing the crystal transformation I comprises dissolving a solid fipronyl different from the crystal transformation I in a solvent selected from one or more of alcohols, acetonitrile(AN), dimethylsulfoxide(DMSO), one or more of benzene derivatives, etc. and crystallizing from the resultant solution. When the solvent is AN, crystallization is carried out at 40°C or lower. When the solvent is DMSO, crystallization is carried out at 80°C or lower.
Abstract translation: 要解决的问题:提供一种氟虫腈基晶体,其允许在制备方法中容易地过滤和干燥较少的粉尘,并且与晶体混合的组合物具有制剂的稳定性,并且是杀虫剂和杀寄生虫剂的混合物。解决方案:存在固体氟虫基 作为具有中心对称空间群C2 / c的单斜晶系,通过使用Cu-Kα射线在25℃记录的X射线粉末衍射图中显示特定的反射,并含有至少85重量%的结晶 氟吡酮的转化I。 制造晶体转变I的方法包括将不同于晶体转变I的固体氟虫酰基溶解在选自醇,乙腈(AN),二甲基亚砜(DMSO),一种或多种苯衍生物等中的一种或多种的溶剂中,以及 从所得溶液中结晶。 当溶剂为AN时,在40℃或更低温度下进行结晶。 当溶剂为DMSO时,在80℃或更低温度下进行结晶。
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公开(公告)号:JP2014139189A
公开(公告)日:2014-07-31
申请号:JP2014031222
申请日:2014-02-21
Applicant: Basf Se , ビーエーエスエフ ソシエタス・ヨーロピアBasf Se
Inventor: HEIDI EMILIA SAXELL , ERK PETER , CLAUDE TARANTA , KROEHL THOMAS , COX GERHARD , MARTIN SUKOPP , DESIRAJU GAUTAM R , RAHUL BANERJEE , BHATT PRASHANT M
IPC: C07D231/44 , A01N25/04 , A01N25/12 , A01N47/02 , A01P5/00 , A01P7/04 , A61K31/415 , A61P33/10 , A61P33/14
CPC classification number: A01N47/02 , A01N2300/00
Abstract: PROBLEM TO BE SOLVED: To provide a novel crystal-transformed fipronil and an insecticidal and a parasiticidal composition.SOLUTION: A fipronil of a triclinic-system crystal transformation V is obtained by crystallizing a solid-form fipronil of formula (I) with dimethylsulfoxide at 100-150°C or acetonitrile at 60-81°C as solvent. A combination of the fipronil with an other insecticidal or parasiticidal compound provides an insecticidal or a parasiticidal composition having a synergistic effect against a specified target of an insect, an acarid or a parasite. The fipronil can be used as a mixture with a fungicidal compound.
Abstract translation: 要解决的问题:提供新型晶体转化的氟虫腈和杀虫剂和杀寄生虫剂组合物。解决方案:通过用二甲基亚砜结晶式(I)的固体形式的氟虫腈获得三斜晶系的晶体转变V的氟虫腈 100-150℃或乙腈在60-81℃作为溶剂。 氟虫腈与其他杀虫剂或杀寄生虫化合物的组合提供对昆虫,螨虫或寄生虫的特定靶标具有协同效应的杀虫剂或杀寄生虫剂组合物。 氟虫腈可以与杀真菌化合物混合使用。
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公开(公告)号:EA025630B1
公开(公告)日:2017-01-30
申请号:EA201400181
申请日:2012-07-17
Applicant: BASF SE
Inventor: SCHNABEL GERHARD , NOLTE MARC , ETCHEVERRY MARIANO IGNACIO , GENARI GERHARD , KROEHL THOMAS , BRATZ MATTHIAS , CANNAN TERRANCE , BOWE STEVEN , BROMMER CHAD , FRIHAUF JOHN , FINCH CHARLES W , THOMAS WALTER
Abstract: Изобретениеотноситсяк жидкойводнойкомпозиции, котораяимеетзначениерН, котороесоставляетпоменьшеймере 7,0, котораясодержитанионныйгербицидс группойкарбоновойкислоты, выбранныйизгербицидовнаосновеароматическойкислоты, игербицидовнаосновефеноксикарбоновойкислотыи основание, выбранноеизсолищелочногометаллагидрокарбоната; илик жидкойводнойкомпозиции, котораяимеетзначениерН, котороесоставляетбольшечем 8,0, котораясодержитсольщелочногометалладикамбы, сольщелочногометаллаглифосата, аоснование, выбранноеизфосфатаи карбоната. Изобретениетакжеотноситсяк способуборьбыс нежелательнойрастительностьюпутемвоздействиягербицидноэффективногоколичествауказанныхкомпозицийнарастения, ихприроднуюсредуилинасеменауказанныхрастений.
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公开(公告)号:BRPI0407358B1
公开(公告)日:2014-11-18
申请号:BRPI0407358
申请日:2004-01-28
Applicant: BASF SE
Inventor: COX GERHARD , MAYER HORST , MAYER WINFRIED , ZIEGLER HANS , SCHNEIDER KARL-HEINRICH , KROEHL THOMAS , ERK PETER , STIERL REINHARD
IPC: C07D213/82 , A01N43/40
Abstract: Monoclinic boscalide (2-chloro-N-(4'-chloro-2-biphenylyl)-nicotinamide) crystal modification (modification II) with a m. pt. of 147-148[deg]C, is new. An independent claim is also included for a preparation of modification II. ACTIVITY : Herbicide. No agricultural data is given. MECHANISM OF ACTION : None given.
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公开(公告)号:EA017180B1
公开(公告)日:2012-10-30
申请号:EA200900633
申请日:2007-11-05
Applicant: BASF SE
Inventor: SAXELL HEIDI EMILIA , ERK PETER , TARANTA CLAUDE , KROEHL THOMAS , COX GERHARD , DESIRAJU GAUTAM R , BANERJEE RAHUL , BHATT PRASHANT M
Abstract: Настоящееизобретениеотноситсяк новойкристаллическоймодификациифипронила, кспособуееполучения, кпестицидными паразитициднымсмесями композициям, которыевключаютуказаннуюкристаллическуюмодификацию, ик ихприменениюдляборьбыс вредителямии паразитами.
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公开(公告)号:CR20120430A
公开(公告)日:2012-09-13
申请号:CR20120430
申请日:2012-08-17
Applicant: BASF SE
Inventor: TARANTA CLAUDE , LEVY TATJANA , BENLAHMAR OUIDAD , NOLTE MARC , KROEHL THOMAS , RANDT CHRISTOPH , BORK THOMAS , MEIER WOLFGANG , KLEIN CLARK D , HENNESSEY TIFFANY
Abstract: Un método para controlar artrópodos, que comprende la aplicación de un gel acuoso que contiene un insecticida, un atrayente y un espesante, en donde el gel acuoso se aplica en forma de manchas en árboles frutales. También, un gel acuoso que comprende un insecticida, un atrayente, un espesante, un humectante y un estimulante alimenticio. Además, un gel concentrado para preparar el gel acuoso.
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公开(公告)号:MX2012008135A
公开(公告)日:2012-08-15
申请号:MX2012008135
申请日:2011-01-18
Applicant: BASF SE
Inventor: MEIER WOLFGANG , KROEHL THOMAS , TARANTA CLAUDE , BORK THOMAS , LEVY TATJANA , KLEIN CLARK D , HENNESSEY TIFFANY , BENLAHMAR OUIDAD , NOLTE MARC , RANDT CHRISTOPH
Abstract: Un método para controlar artrópodos, que comprende la aplicación de un gel acuoso que contiene un insecticida, un atrayente y un espesante, en donde el gel acuoso se aplica en forma de manchas en árboles frutales. También, un gel acuoso que comprende un insecticida, un atrayente, un espesante, un humectante y un estimulante alimenticio. Además, un gel concentrado para preparar el gel acuoso.
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