형광체, 및 이의 제조 방법
    41.
    发明公开
    형광체, 및 이의 제조 방법 有权
    磷酸盐及其制备方法

    公开(公告)号:KR1020140006147A

    公开(公告)日:2014-01-16

    申请号:KR1020120068520

    申请日:2012-06-26

    Abstract: The present invention relates to a manufacturing method for phosphors comprising: a step of obtaining a mixed solution containing alkaline-earth metal salt, rare earth metal salt, group 4 metal salt and the oxide precursor excessive group 4 elements; and a step of performing heat treatment after adding cellulose in the mixed solution and phosphors manufactured thereby. [Reference numerals] (AA) Obtain a mixed solution containing alkaline-earth metal salt, rare earth metal salt, group 3 metal salt and excessive oxide precursors of group 4 elements; (BB) Perform heat treatment after adding cellulose in the mixed solution; (CC) Obstain phosphors powders

    Abstract translation: 本发明涉及一种荧光体的制造方法,包括:获得含有碱土金属盐,稀土金属盐,第4族金属盐和氧化物前体过量基团4的元素的混合溶液的步骤; 以及在混合溶液中加入纤维素后由其制成的荧光体进行热处理的步骤。 (AA)获得包含碱土金属盐,稀土金属盐,第3族金属盐和第4族元素的过量氧化物前体的混合溶液; (BB)在混合溶液中加入纤维素后进行热处理; (CC)卤素荧光粉

    염소-함유 실리케이트계 형광체의 알칼리 처리를 이용하여 제조된 형광체 분말 및 그의 제조 방법
    44.
    发明公开
    염소-함유 실리케이트계 형광체의 알칼리 처리를 이용하여 제조된 형광체 분말 및 그의 제조 방법 有权
    通过碱处理含有氯硅酸盐的氯化镁制备的磷光体及其制备方法

    公开(公告)号:KR1020120098546A

    公开(公告)日:2012-09-05

    申请号:KR1020120020630

    申请日:2012-02-28

    Abstract: PURPOSE: A manufacturing method of chlorine-based phosphor or oxide-based phosphor is provided to increase light-emitting intensity of phosphor, in which rare earth metal is added, through strong oxidation or reduction using chloride, and to able to manufacture a more stable phosphor. CONSTITUTION: A manufacturing method of chlorine-based phosphor or oxide-based phosphor comprises a step of treating chloride-containing silicate phosphor to alkaline material. The alkaline material comprises a compound containing -OH, -NH2, or NH3. The alkaline compound comprising -OH comprises LiOH, NaOH, KOH, RbOH, CsOH, NH4OH, H2O2, or combinations thereof. A treatment to the alkaline material is conducted at (-100) - 1500 °C. The chloride-based phosphor additionally comprises rare earth metal.

    Abstract translation: 目的:提供氯系荧光体或氧化物系荧光体的制造方法,通过使用氯化物的强氧化或还原来提高添加稀土金属的荧光体的发光强度,能够制造更稳定 磷。 构成:氯系荧光体或氧化物系荧光体的制造方法包括将含氯化物的硅酸盐荧光体处理成碱性物质的工序。 碱性材料包含含有-OH,-NH 2或NH 3的化合物。 包含-OH的碱性化合物包括LiOH,NaOH,KOH,RbOH,CsOH,NH 4 OH,H 2 O 2或其组合。 在(-100)-100℃下对碱性物质进行处理。 基于氯化物的荧光体还包括稀土金属。

    염화실리케이트계 형광체 및 그 제조 방법
    45.
    发明公开
    염화실리케이트계 형광체 및 그 제조 방법 有权
    氯硅酸盐及其制备方法

    公开(公告)号:KR1020120098545A

    公开(公告)日:2012-09-05

    申请号:KR1020120020629

    申请日:2012-02-28

    Abstract: PURPOSE: A manufacturing method of silicate chloride-based phosphor is provided to provide a spherical silicate chloride-based phosphor having uniform particle size, excellent luminance efficiency, excellent productivity, and excellent profitability. CONSTITUTION: A manufacturing method of silicate chloride-based phosphor comprises: a step of obtaining metal salt-SiO2 sol mixed solution by mixing metal salt mixed solution, which comprises metal sat for synthesizing silicate chloride-based phosphor with rare earth metal, together with sol to liquid phase; a step of impregnating the metal salt-SiO2 sol mixed solution into a polymer material, drying the polymer material, and conducting low-temperature calcinations, preoxidation firing, and post reduction firing to obtain silicate chloride-based phosphor. [Reference numerals] (AA) Metal solution, aqueous silicon compound(WSS); (BB) Impregnation(cellulose); (CC) Mixing, stirring and drying under ultra sonic waves; (DD) First sintering(150-400°C, air); (EE) Second sintering(500-1000°C, air); (FF) 700-1400°C, sintering under reduction; (GG) Phosphor

    Abstract translation: 目的:提供一种硅酸氯化物系荧光体的制造方法,提供粒径均匀,发光效率好,生产率优异,利润率优异的球形硅酸氯化物系荧光体。 构成:一种硅酸氯化物系荧光体的制造方法,其特征在于,通过混合金属盐混合溶液得到金属盐-SiO 2溶胶混合溶液的步骤,所述金属盐混合溶液包括用于合成硅酸氯化物基荧光体与稀土金属的金属sat,以及溶胶 到液相; 将金属盐-SiO 2溶胶混合溶液浸渍到聚合物材料中,干燥聚合物材料,进行低温煅烧,预氧化烧结和后还原烧成,得到硅酸氯化物系荧光体。 (标号)(AA)金属溶液,硅酸水溶液(WSS); (BB)浸渍(纤维素); (CC)在超声波下混合搅拌干燥; (DD)第一烧结(150-400℃,空气); (EE)第二烧结(500-1000℃,空气); (FF)700-1400℃,还原烧结; (GG)荧光体

    형광체 분말 및 그의 제조 방법
    46.
    发明公开
    형광체 분말 및 그의 제조 방법 无效
    磷肥粉及其制备方法

    公开(公告)号:KR1020120096221A

    公开(公告)日:2012-08-30

    申请号:KR1020110015495

    申请日:2011-02-22

    CPC classification number: C09K11/59 C09K11/0883 H01J17/49 Y02B20/181

    Abstract: PURPOSE: A manufacturing method of phosphor powder is provided to provide oxynitride-based or nitride-based phosphor powder emitting blue to yellow excitation light in a range of blue ray to ultra violet ray, and having excellent luminous efficiency and temperature performance even in high temperatures. CONSTITUTION: A manufacturing method of phosphor powder comprises a step of obtaining precursor by impregnating aqueous solution comprising divalent metal salt for forming Si-based oxynitride group through hydrothermal synthesis at 80-200 °C; and a step of primary sintering the precursor at 300-800 °C under oxygen-containing atmosphere; a step of secondary sintering under ammonia- or nitrogen-containing atmosphere at 900-1400 °C.

    Abstract translation: 目的:提供荧光体粉末的制造方法,以提供在蓝光至紫外线范围内发射蓝色至黄色激发光的氮氧化物基或氮化物系荧光体粉末,即使在高温下也具有优异的发光效率和温度性能 。 构成:荧光体粉末的制造方法包括通过在80〜200℃下通过水热合成浸渍含有二价金属盐的水溶液以形成Si系氮氧化物基团而获得前体的工序; 以及在含氧气氛下在300-800℃下初始烧结前体的步骤; 在900-1400℃的氨水或含氮气氛下二次烧结的步骤。

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