Abstract:
The present invention relates to a manufacturing method for phosphors comprising: a step of obtaining a mixed solution containing alkaline-earth metal salt, rare earth metal salt, group 4 metal salt and the oxide precursor excessive group 4 elements; and a step of performing heat treatment after adding cellulose in the mixed solution and phosphors manufactured thereby. [Reference numerals] (AA) Obtain a mixed solution containing alkaline-earth metal salt, rare earth metal salt, group 3 metal salt and excessive oxide precursors of group 4 elements; (BB) Perform heat treatment after adding cellulose in the mixed solution; (CC) Obstain phosphors powders
Abstract:
The present invention relates to nitride-based phosphor which is synthesized at low temperature in a relative sense by making chloride-based phosphor react with Si3N4 or Si2ON2, or oxynitride-based phosphor or oxynitride-based phosphor powder synthesized through a carbothermal reduction and nitridation (CRN) method, and a manufacturing method thereof.
Abstract:
본원은, 브라운관, 발광다이오드 (LED), 플라즈마 디스플레이 패널 (PDP), 냉음극형광램프(CCFL), 전계방출디스플레이(FED)와 같은 디스플레이용 및 램프용 발광기구에 사용 할 수 있는 초미세입자의 알칼리토 금속을 포함하는 AlO계 형광체 분말의 제조방법 관한 것으로서, 상기 제조 방법은 알칼리토 금속 염 및 알루미늄 염을 포함하는 수용액을 고분자 물질에 함침시켜 전구체를 수득하고 상기 전구체를 2단계로 소성함으로써 나노 크기 내지 서브 마이크로 크기의 AlO계(알루미네이트계) 산화물 형광체 분말을 수득하는 것을 포함한다.
Abstract:
PURPOSE: A manufacturing method of chlorine-based phosphor or oxide-based phosphor is provided to increase light-emitting intensity of phosphor, in which rare earth metal is added, through strong oxidation or reduction using chloride, and to able to manufacture a more stable phosphor. CONSTITUTION: A manufacturing method of chlorine-based phosphor or oxide-based phosphor comprises a step of treating chloride-containing silicate phosphor to alkaline material. The alkaline material comprises a compound containing -OH, -NH2, or NH3. The alkaline compound comprising -OH comprises LiOH, NaOH, KOH, RbOH, CsOH, NH4OH, H2O2, or combinations thereof. A treatment to the alkaline material is conducted at (-100) - 1500 °C. The chloride-based phosphor additionally comprises rare earth metal.
Abstract:
PURPOSE: A manufacturing method of silicate chloride-based phosphor is provided to provide a spherical silicate chloride-based phosphor having uniform particle size, excellent luminance efficiency, excellent productivity, and excellent profitability. CONSTITUTION: A manufacturing method of silicate chloride-based phosphor comprises: a step of obtaining metal salt-SiO2 sol mixed solution by mixing metal salt mixed solution, which comprises metal sat for synthesizing silicate chloride-based phosphor with rare earth metal, together with sol to liquid phase; a step of impregnating the metal salt-SiO2 sol mixed solution into a polymer material, drying the polymer material, and conducting low-temperature calcinations, preoxidation firing, and post reduction firing to obtain silicate chloride-based phosphor. [Reference numerals] (AA) Metal solution, aqueous silicon compound(WSS); (BB) Impregnation(cellulose); (CC) Mixing, stirring and drying under ultra sonic waves; (DD) First sintering(150-400°C, air); (EE) Second sintering(500-1000°C, air); (FF) 700-1400°C, sintering under reduction; (GG) Phosphor
Abstract:
PURPOSE: A manufacturing method of phosphor powder is provided to provide oxynitride-based or nitride-based phosphor powder emitting blue to yellow excitation light in a range of blue ray to ultra violet ray, and having excellent luminous efficiency and temperature performance even in high temperatures. CONSTITUTION: A manufacturing method of phosphor powder comprises a step of obtaining precursor by impregnating aqueous solution comprising divalent metal salt for forming Si-based oxynitride group through hydrothermal synthesis at 80-200 °C; and a step of primary sintering the precursor at 300-800 °C under oxygen-containing atmosphere; a step of secondary sintering under ammonia- or nitrogen-containing atmosphere at 900-1400 °C.