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公开(公告)号:BR0102897A
公开(公告)日:2002-04-02
申请号:BR0102897
申请日:2001-07-16
Applicant: DEGUSSA
Inventor: ALIG ALFRED , BATZ-SOHN CHRISTOPH , DESCHLER ULRICH , MICHEL RUDOLF , MUENZENBERG JOERG , SONNENSCHEIN RAYMUND , WILL WERNER , ZEZULKA GERD RAINHARD , RUETZEL KARL-HEINZ
Abstract: The invention relates to a process for the preparation of organosilylalkylpolysulfanes, of the general formula I (R1R2R3SiR4)2Sx (I) by reaction of organosilylalkylpolysulfanes of the general formula II (R1R2R3SiR4)2Sy (II) with an ionic sulfide of the general formula M+2S2- (III) and an organosilylalkyl halide of the general formula R1R2R3SiR4X (IV), the long-chain organosilylalkylpolysulfane of the general formula (II) and the organosilylalkyl halide of the general formula (IV) being initially introduced into the reaction vessel and the ionic sulfide of the general formula (III) being added to this solution in several portions.
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公开(公告)号:HU0102967A2
公开(公告)日:2002-01-28
申请号:HU0102967
申请日:2001-07-13
Applicant: DEGUSSA
Inventor: ALIG ALFRED , DR BATZ-SOHN CHRISTOPH , DR DESCHLER ULRICH , MICHEL RUDOLF , DR MUENZENBERG JOERG , RUETZEL KARL-HEINZ , DR SONNENSCHEIN RAYMUND , WILL WERNER , ZEZULKA GERD RAINHARD
Abstract: The invention relates to a process for the preparation of organosilylalkylpolysulfanes, of the general formula I (R1R2R3SiR4)2Sx (I) by reaction of organosilylalkylpolysulfanes of the general formula II (R1R2R3SiR4)2Sy (II) with an ionic sulfide of the general formula M+2S2- (III) and an organosilylalkyl halide of the general formula R1R2R3SiR4X (IV), the long-chain organosilylalkylpolysulfane of the general formula (II) and the organosilylalkyl halide of the general formula (IV) being initially introduced into the reaction vessel and the ionic sulfide of the general formula (III) being added to this solution in several portions.
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公开(公告)号:HU0100921A2
公开(公告)日:2001-12-28
申请号:HU0100921
申请日:2001-02-28
Applicant: DEGUSSA
Inventor: MICHEL RUDOLF , DR MUENZENBERG JOERG , WILL WERNER
IPC: C07F7/18
Abstract: Production of organosilylalkyl polysufides (I) by reacting an organosilylalkyl halide (II) with an anhydrous ionic sulfide (III) and elemental sulfur comprises adding (III) to a suspension of elemental sulfur and (II) in a polar organic solvent. Production of organosilylalkyl polysufides of formula (I) by reacting an organosilylalkyl halide of formula (II) with an anhydrous ionic sulfide of formula (III) and elemental sulfur comprises adding (III) to a suspension of elemental sulfur and (II) in a polar organic solvent: (R 1>R 2>R 3>SiR 4>)S x (I) , R 1>R 2>R 3>SiR 4>X (II) and M 2S (III) R 1>-R 3>1-8C alkyl, 1-8C alkoxy or aryl, at least one being alkoxy; R 4>1-8C alkylene or (CH 2) n-C 6H 4-(CH 2) n; n : 1-4; x : more than 1; X : Cl, Br or I; M : an alkali metal or ammonium cation or half an alkaline earth metal or zinc cation.
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公开(公告)号:CZ20010684A3
公开(公告)日:2001-10-17
申请号:CZ20010684
申请日:2001-02-22
Applicant: DEGUSSA
Inventor: MICHEL RUDOLF , MUNZENBERG JORG DR , WILL WERNER , ZEZULKA GERD RAINHARD
IPC: C07F7/18
CPC classification number: C07F7/1892
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公开(公告)号:HU0102967D0
公开(公告)日:2001-09-28
申请号:HU0102967
申请日:2001-07-13
Applicant: DEGUSSA
Inventor: ALIG ALFRED , DR BATZ-SOHN CHRISTOPH , DR DESCHLER ULRICH , MICHEL RUDOLF , DR MUENZENBERG JOERG , RUETZEL KARL-HEINZ , DR SONNENSCHEIN RAYMUND , WILL WERNER , ZEZULKA GERD RAINHARD
Abstract: The invention relates to a process for the preparation of organosilylalkylpolysulfanes, of the general formula I (R1R2R3SiR4)2Sx (I) by reaction of organosilylalkylpolysulfanes of the general formula II (R1R2R3SiR4)2Sy (II) with an ionic sulfide of the general formula M+2S2- (III) and an organosilylalkyl halide of the general formula R1R2R3SiR4X (IV), the long-chain organosilylalkylpolysulfane of the general formula (II) and the organosilylalkyl halide of the general formula (IV) being initially introduced into the reaction vessel and the ionic sulfide of the general formula (III) being added to this solution in several portions.
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公开(公告)号:CA2244597A1
公开(公告)日:1999-02-08
申请号:CA2244597
申请日:1998-08-07
Applicant: DEGUSSA
Inventor: MUENZENBERG JOERG , ZEZULKA GERD , WILL WERNER
Abstract: The preparation of high-purity organosilicon disulphanes in which, in a two-stage process, elemental sulphur and an anhydrous alkali sulphide in a deficient amount is first reacted with a halogen alkylalkoxysilane, and the sulphur deficit is then made up by the addition of further alkali sulphide.
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公开(公告)号:ES2672307T3
公开(公告)日:2018-06-13
申请号:ES05755290
申请日:2005-06-16
Applicant: EVONIK DEGUSSA GMBH
Inventor: LORTZ WOLFGANG , BATZ-SOHN CHRISTOPH , MANGOLD HELMUT , PERLET GABRIELE , WILL WERNER , REITZ SASCHA
IPC: C01B33/148 , C09K21/02
Abstract: Dispersión de dióxido de silicio pirogénico que se puede verter, estable, donde - el diámetro de los agregados relacionado con el número promedio de las partículas de dióxido de silicio en la dispersión es inferior a 200 nm; la dispersión comprende - al menos un 35% en peso de polvo de dióxido de silicio, - de un 3 a un 35% en peso de al menos un poliol, - de un 20 a un 60% en peso de agua, - de un 0 a un 10% en peso de un aditivo, en cada caso basado en la cantidad total de la dispersión, - y comprende una sustancia que tiene una acción alcalina en una cantidad tal que se establezca un pH de 10
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公开(公告)号:AT506323T
公开(公告)日:2011-05-15
申请号:AT06763616
申请日:2006-06-09
Applicant: EVONIK DEGUSSA GMBH
Inventor: LORTZ WOLFGANG , BATZ-SOHN CHRISTOPH , PERLET GABRIELE , LACH HEINZ , WILL WERNER
Abstract: Aluminum oxide dispersion, which is stable in a pH range 5 from 5 to 9 and has an aluminum oxide content of at least 40 wt. %, obtainable by dispersing pyrogenically produced aluminum oxide particles in an aqueous phase, wherein one or several at least dibasic hydroxycarboxylic acids present dissolved in the dispersion and at least one salt of a 10 dialkali metal hydrogen phosphate and/or alkali metal dihydrogen phosphate are added to the aqueous phase each mutually independently in a quantity of 0.3-3×10-6 mol/m2 of aluminum oxide specific surface area.
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49.
公开(公告)号:DE502008001884D1
公开(公告)日:2011-01-05
申请号:DE502008001884
申请日:2008-04-02
Applicant: EVONIK DEGUSSA GMBH
Inventor: LORTZ WOLFGANG , FILZ KARLHEINZ , WILL WERNER , DIENER UWE
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公开(公告)号:AT485238T
公开(公告)日:2010-11-15
申请号:AT04725037
申请日:2004-04-01
Applicant: EVONIK DEGUSSA GMBH
Inventor: LORTZ WOLFGANG , BATZ-SOHN CHRISTOPH , PERLET GABRIELE , WILL WERNER , SCHNEIDER GERRIT
Abstract: Process for the production of an aqueous dispersion of pyrogenically produced metal oxide and metalloid oxide powders with a BET surface area of between 5 and 600 m2/g, with a metal oxide or metalloid oxide content in the dispersion of between 5 and 25 wt. %, comprising the following steps: water, which is optionally adjusted to pH values of between 2 and 4 by adding acids, is circulated from a receiving vessel via a rotor/stator machine, and metal oxide or metalloid oxide powder is introduced, using a feed device, into the shear zone between the slots in the rotor teeth and the stator slots, continuously or discontinuously and with the rotor/stator machine running, in a quantity such that a predispersion with a solids content of between 20 and 40 wt. % results, and, after all the metal oxide powder or metalloid oxide powder has been added, the feed device closes and shearing continues in such a way that the shear rate is in the range of between 10000 and 40000 s-1, and then, by dilution, the predispersion is adjusted to the desired solids content of the dispersion while maintaining the dispersing conditions.
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