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    1.
    发明专利
    未知

    公开(公告)号：DE50004141D1

    公开(公告)日：2003-11-27

    申请号：DE50004141

    申请日：2000-09-13

    Applicant: DEGUSSA

    Inventor： LUGINSLAND DR ,  BATZ-SOHN DR ,  MUENZENBERG DR ,  ZEZULKA GERD RAINHARD

    IPC: B60C1/00 ,  C07F7/08 ,  C07F7/12 ,  C07F7/18 ,  C07F19/00 ,  C08J5/00 ,  C08K3/00 ,  C08K3/36 ,  C08K5/548 ,  C08L21/00

    Abstract: A novel organosilicon compound is claimed. The novel organosilicon compound is of formula R )(R )Si-R -S-Zn-S-R -Si(R )(R )(R (I). R - R = H, halogen or optionally branched alkyl or alkoxyl; and R = optionally branched alkylidene. Independent claims are also included for: (a) the preparation of (I) by reaction of a mercaptan compound of formula R )(R )Si-R -S-H (II) and a zinc alcoholate; (b) rubber mixtures containing compound (s) (I), rubber, filler and optional rubber additives; (c) preparation of the rubber mixtures by reaction of the components given in (b); and (d) mould forms comprising the rubber mixtures.

    2.
    发明专利
    未知

    公开(公告)号：DE50110667D1

    公开(公告)日：2006-09-21

    申请号：DE50110667

    申请日：2001-06-21

    Applicant: DEGUSSA

    Inventor： ALIG ALFRED ,  BATZ SOHN CHRISTOPH DR ,  DESCHLER ULRICH DR ,  MICHEL RUDOLF ,  MUENZENBERG JOERG DR ,  SONNENSCHEIN RAYMUND DR ,  WILLI WERNER ,  ZEZULKA GERD RAINHARD ,  RUETZEL KARL-HEINZ

    IPC: C07F7/08 ,  C07F7/18

    Abstract: The invention relates to a process for the preparation of organosilylalkylpolysulfanes, of the general formula I (R1R2R3SiR4)2Sx (I) by reaction of organosilylalkylpolysulfanes of the general formula II (R1R2R3SiR4)2Sy (II) with an ionic sulfide of the general formula M+2S2- (III) and an organosilylalkyl halide of the general formula R1R2R3SiR4X (IV), the long-chain organosilylalkylpolysulfane of the general formula (II) and the organosilylalkyl halide of the general formula (IV) being initially introduced into the reaction vessel and the ionic sulfide of the general formula (III) being added to this solution in several portions.

    3.
    发明专利
    未知

    公开(公告)号：DE50003514D1

    公开(公告)日：2003-10-09

    申请号：DE50003514

    申请日：2000-11-04

    Applicant: DEGUSSA

    Inventor： KRAFCZYK DR ,  MUENZENBERG DR ,  ZEZULKA GERD RAINHARD

    IPC: C07F9/165

    Abstract: A process for the production of sulfur- and phosphorus-containing silane compounds comprises reaction of a halogen containing silane with phosphorus pentasulfide and a metal sulfide. A process for the production of sulfur- and phosphorus-containing compounds of formula (R n(R O)3-n-Si-Alk-S-)3P=S (1) comprises reaction of a halogen-containing silane of formula R n(R O)3-n-Si-Alk-Hal (2) with phosphorus pentasulfide (P4S10) and a metal sulfide. Alk = 1-10C alkylene; R ,R each = 1-5C alkyl, 5-8C cycloalkyl, phenyl, benzyl or 2-methoxyethyl; Hal = halogen; and n = 0-2.

    4.
    发明专利
    未知

    公开(公告)号：BR0100803A

    公开(公告)日：2001-11-06

    申请号：BR0100803

    申请日：2001-03-01

    Applicant: DEGUSSA

    Inventor： MICHEL RUDOLF ,  MUENZENBERG JOERG ,  WILL WERNER ,  ZEZULKA GERD RAINHARD

    IPC: C07F7/18 ,  C07F7/14

    Abstract: Production of organosilylalkyl polysufides (I) by reacting an organosilylalkyl halide (II) with an anhydrous ionic sulfide (III) and elemental sulfur comprises adding (III) to a suspension of elemental sulfur and (II) in a polar organic solvent. Production of organosilylalkyl polysufides of formula (I) by reacting an organosilylalkyl halide of formula (II) with an anhydrous ionic sulfide of formula (III) and elemental sulfur comprises adding (III) to a suspension of elemental sulfur and (II) in a polar organic solvent: (R 1>R 2>R 3>SiR 4>)S x (I) , R 1>R 2>R 3>SiR 4>X (II) and M 2S (III) R 1>-R 3>1-8C alkyl, 1-8C alkoxy or aryl, at least one being alkoxy; R 4>1-8C alkylene or (CH 2) n-C 6H 4-(CH 2) n; n : 1-4; x : more than 1; X : Cl, Br or I; M : an alkali metal or ammonium cation or half an alkaline earth metal or zinc cation.

    PROCEDIMIENTO PARA PREPARAR ORGANOSILILALQUILPOLISULFANOS.
    6.
    发明专利
    PROCEDIMIENTO PARA PREPARAR ORGANOSILILALQUILPOLISULFANOS. 未知

    公开(公告)号：ES2222279T3

    公开(公告)日：2005-02-01

    申请号：ES01103386

    申请日：2001-02-14

    Applicant: DEGUSSA

    Inventor： MICHEL RUDOLF ,  MUNZENBERG JORG DR ,  WERNER WILLI ,  ZEZULKA GERD RAINHARD

    IPC: C07F7/18

    Abstract: Procedimiento para obtener organosililalquilpolisulfanos de fórmula general (R1R2R3SiR4)2Sx (I) en la que R1, R2, R3 significan grupos alquilo y/o alcoxi iguales o distintos entre sí, ramificados o no ramificados, con una longitud de cadena de 1 a 8 átomos de carbono, restos arilo, en donde está presente al menos un grupo alcoxi, R4 significa un resto alquileno divalente con una longitud de cadena de 1 a 8 átomos de carbono, o -(CH2)n-C6H4-(CH2)n-, siendo n = 1 a 4; x es un número mayor que 1, por reacción de un halogenuro de organosililalquilo de fórmula general R1R2R3SiR4X (II) en la que R1, R2, R3 y R4 tienen el significado indicado anteriormente y X es cloro, bromo o yodo, y un sulfuro iónico libre de agua o casi libre de agua de fórmula general M+2S2- (III) en la que M+ representa un catión de metal alcalino, un ion amonio, medio catión de metal alcalinotérreo o medio catión zinc, y azufre elemental, caracterizado porque se pone en un disolvente orgánico polar elazufre elemental y el halogenuro de organosililalquilo, y a esta suspensión se le añade el sulfuro iónico libre de agua o casi libre de agua.

    METHOD FOR SYNTHESIS OF ORGANOSILYLALKYLPOLYSULFANES
    7.
    发明专利
    METHOD FOR SYNTHESIS OF ORGANOSILYLALKYLPOLYSULFANES 未知

    公开(公告)号：UA68389C2

    公开(公告)日：2004-08-16

    申请号：UA2001031439

    申请日：2001-03-01

    Applicant: DEGUSSA

    Inventor： ZEZULKA GERD RAINHARD

    IPC: C07F7/18

    Abstract: The method for synthesis of organosilylalkylpolysulfanes consists in the reaction of the appropriate organosilylalkyl halogenide with the anhydrous or practically anhydrous ionic sulfide and elementary sulfur. The elementary sulfur and organosilylalkyl halogenide are first added to the polar organic solvent, and then ionic sulfide is added to the suspension.

    Process for preparing organosilylalkyl polysulfanes
    8.
    发明专利
    Process for preparing organosilylalkyl polysulfanes 未知

    公开(公告)号：CZ2001684A3

    公开(公告)日：2001-10-17

    申请号：CZ2001684

    申请日：2001-02-22

    Applicant: DEGUSSA

    Inventor： MICHEL RUDOLF ,  MUNZENBERG JORG DR ,  WILL WERNER ,  ZEZULKA GERD RAINHARD

    IPC: C07F7/18

    Abstract: Production of organosilylalkyl polysufides (I) by reacting an organosilylalkyl halide (II) with an anhydrous ionic sulfide (III) and elemental sulfur comprises adding (III) to a suspension of elemental sulfur and (II) in a polar organic solvent. Production of organosilylalkyl polysufides of formula (I) by reacting an organosilylalkyl halide of formula (II) with an anhydrous ionic sulfide of formula (III) and elemental sulfur comprises adding (III) to a suspension of elemental sulfur and (II) in a polar organic solvent: (R 1>R 2>R 3>SiR 4>)S x (I) , R 1>R 2>R 3>SiR 4>X (II) and M 2S (III) R 1>-R 3>1-8C alkyl, 1-8C alkoxy or aryl, at least one being alkoxy; R 4>1-8C alkylene or (CH 2) n-C 6H 4-(CH 2) n; n : 1-4; x : more than 1; X : Cl, Br or I; M : an alkali metal or ammonium cation or half an alkaline earth metal or zinc cation.

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