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    New phthalocyanine dyes
    83.
    发明专利
    New phthalocyanine dyes 未知

    公开(公告)号：GB898318A

    公开(公告)日：1962-06-06

    申请号：GB2835060

    申请日：1960-08-16

    Applicant: BASF AG

    Inventor： TARTTER ARNOLD ,  HENSEL HANS RUPRECHT ,  BAUMANN HANS

    IPC: C09B62/18

    Abstract: The invention comprises dyes of the formula and the alkali-metal or ammonium salts thereof, wherein Pc is the radical of copper or nickel phthalocyanine or a copper phthalocyanine having 1 to 4 chlorine atoms or phenyl groups in the molecule, Z1 is hydrogen, chlorine, methyl or methoxy, Z2 is hydrogen, chlorine or a sulphonic acid radical, X is chlorine or bromine, m is a whole number from 0 to 5, n is an integer from 1 to 4 and (n+m) is an integer from 1 to 6. The dyes are made by reacting a sulphonyl chloride of the formula [Pc-]-(SO2Cl)(m+n) with n mols of a compound of the formula and hydrolysing the unreacted sulphochloride groups, or by reacting the above sulphochloride with n mols of a compound of the formula and treating the reaction product with a mineral acid or by reacting a compound of the formula with n mols of mucobromic or mucochloric acid in aqueous mineral acid solution. The dyes dye and print wool, silk, synthetic linear polyamides and cellulose textile materials in blue and green shades, in the case of cellulose in conjunction with an alkali and heat treatment.

    Dyestuffs of the phthalocyanine series containing methylol groups and their production
    84.
    发明专利
    Dyestuffs of the phthalocyanine series containing methylol groups and their production 未知

    公开(公告)号：GB895029A

    公开(公告)日：1962-04-26

    申请号：GB2607660

    申请日：1960-07-27

    Applicant: BASF AG

    Inventor： TARTTER ARNOLD ,  BRAUN WILLY ,  EISELE JULIUS ,  KREHBIEL GUENTER ,  LANGE GEUNTER ,  MUELLER ROLAND ,  WEISSAUER HERMANN

    Abstract: The invention comprises water-soluble dyestuffs containing methylol groups and having the formula (HO3S)n-D-(Z)m where D is the radical of copper phthalocyanine, chlor-copper phthalocyanine having 1-4 chlorine atoms per molecule, phenyl-copper phthalocyanine having 1-4 phenyl groups per molecule, nickel phthalocyanine, iron phthalocyanine, aluminium phthalocyanine, diaza-copper phthalocyanine tetramethyl-dibenzo nickel tetrazaporphin or octaphenyl-nickel tetrazaporphin, Z is one of the radicals -SO2NH2, in which all hydrogen atoms capable of reacting with formaldehyde at a pH of 6 to 11 and a temperature of 0 DEG C. to 80 DEG C. are replaced by methylol groups, n is 1, 2 or 3, m is 1, 2 or 3 and (n+m) is 3 or 4, X is hydrogen or sulphonic acid and Y is hydrogen, sulphonic acid or methoxy. The dyestuffs are made by reacting the appropriate dyestuffs with formaldehyde under the conditions stated above. The preparation of the starting dyestuffs is described and examples are given. The dyes colour natural or regenerated cellulose and paper blue or green shades.

    Improvements in the production of dyed fibres and foils of cellulose
    88.
    发明专利
    Improvements in the production of dyed fibres and foils of cellulose 未知

    公开(公告)号：GB858737A

    公开(公告)日：1961-01-11

    申请号：GB1745659

    申请日：1959-05-22

    Applicant: BASF AG

    Inventor： EISELE JULIUS ,  FEDERKIEL WILHELM ,  TARTTER ARNOLD ,  LANGE GUENTER ,  KREHBIEL GUENTER ,  STEIN HANS WALTHER

    IPC: D06P3/66

    Abstract: Fibres and foils of cellulose are dyed or printed by applying a dyestuff of the formula: in which A represents a tetrazaporphin radical, E represents an aromatic radical containing a mono- or bi-cyclic nucleus, Z represents a radical of the formula: in which R1 and R2 represent hydrogen atoms, alkyl or hydroxyalkyl groups or halogen atoms and R3 represents a hydrogen or halogen atom or an alkyl, hydroxyalkyl or carboxyl group, m is a number from 1-8 and n is a number from 0-4, and also applying an acid-binding agent before, together with or after the dyestuff. Specified acid-binding agents are alkali-metal or alkaline-earth metal hydroxides, carbonates and bicarbonates and alkali-metal phosphates. If necessary, fixation of the dyestuff may be effected by heating or steaming. The dyestuffs may be prepared by acylating a tetrazaporphin derivative of the formula: with acrylic acid chloride, a - methylacrylic acid chloride, a - chloracrylic acid esters, maleic anhydride or acrylic anhydride. Specifications 827,569, 853,364 and 858,184 are referred to.

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