84.
    发明专利
    未知

    公开(公告)号:DE50115253D1

    公开(公告)日:2010-01-21

    申请号:DE50115253

    申请日:2001-04-30

    Applicant: BASF SE

    Abstract: A process for the preparation of caprolactam is provided, whereina) a mixture (I) containing 6-aminocapronitrile and water is reacted in the liquid phase, in the presence of a catalyst, to give a mixture (II) containing caprolactam, ammonia, water, high-boiling components and low-boiling components,b) ammonia is then removed from the mixture (II) to give a mixture (III) containing caprolactam, water, high-boiling components and low-boiling components,c) water is then removed from the mixture (III) to give a mixture (IV) containing caprolactam, high-boiling components and low-boiling components, andd) a solid (V) containing caprolactam is then obtained from the mixture (IV) by crystallization, the proportion by weight of caprolactam in the solid (V) being greater than in the mixture (IV).

    85.
    发明专利
    未知

    公开(公告)号:DE502005008533D1

    公开(公告)日:2009-12-31

    申请号:DE502005008533

    申请日:2005-01-20

    Applicant: BASF SE

    Abstract: Process and apparatus for the continuous preparation of a chemical compound in at least one reactor, where at least one of the reactors is a shell-and-tube reactor which has a shell and at least one internal tube located within the shell, wherein at least one of the internal tubes has, at least in part, a noncircular cross section and a helical configuration in the region in which it is surrounded by the shell.

    87.
    发明专利
    未知

    公开(公告)号:AT451353T

    公开(公告)日:2009-12-15

    申请号:AT01951465

    申请日:2001-04-30

    Applicant: BASF SE

    Abstract: A process for the preparation of caprolactam is provided, whereina) a mixture (I) containing 6-aminocapronitrile and water is reacted in the liquid phase, in the presence of a catalyst, to give a mixture (II) containing caprolactam, ammonia, water, high-boiling components and low-boiling components,b) ammonia is then removed from the mixture (II) to give a mixture (III) containing caprolactam, water, high-boiling components and low-boiling components,c) water is then removed from the mixture (III) to give a mixture (IV) containing caprolactam, high-boiling components and low-boiling components, andd) a solid (V) containing caprolactam is then obtained from the mixture (IV) by crystallization, the proportion by weight of caprolactam in the solid (V) being greater than in the mixture (IV).

    88.
    发明专利
    未知

    公开(公告)号:AT402155T

    公开(公告)日:2008-08-15

    申请号:AT04727899

    申请日:2004-04-16

    Applicant: BASF SE

    Abstract: Process for preparing propylene oxide, which comprises at least the steps (iii) and (iv) (iii) separating off propylene oxide from a mixture (M1) comprising propylene oxide and at least one solvent by distillation in a distillation column, giving a bottom stream and a vapor stream consisting essentially of propylene oxide; (iv) compressing the vapor stream obtained in (iii) by means of at least one compressor to give a compressed vapor.

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