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    METHOD FOR PRODUCING AMINES FROM SUGAR ALCOHOLS
    3.
    发明申请
    METHOD FOR PRODUCING AMINES FROM SUGAR ALCOHOLS 审中-公开
    从糖醇制备胺的方法

    公开(公告)号：WO2009027249A3

    公开(公告)日：2009-06-18

    申请号：PCT/EP2008060742

    申请日：2008-08-15

    Applicant: BASF SE ,  ERNST MARTIN ,  HOFFER BRAM WILLEM ,  MELDER JOHANN-PETER

    Inventor： ERNST MARTIN ,  HOFFER BRAM WILLEM ,  MELDER JOHANN-PETER

    IPC: C07C209/16 ,  C07C211/10 ,  C07C211/11 ,  C07D241/02 ,  C07D295/00

    CPC classification number: C07C209/16 ,  C04B24/122 ,  C04B28/02 ,  C07C213/02 ,  C07D241/04 ,  C07D295/02 ,  C07D295/023 ,  C07C211/09 ,  C07C211/10 ,  C07C211/11 ,  C07C215/08

    Abstract: The invention relates to a method for producing amines by reacting sugar alcohols with hydrogen and an amination agent, selected from the group containing ammonia, primary and secondary amines, in the presence of a catalyst at a temperature of between 100°C and 400°C and at a pressure of between 1 and 40 MPa (10 to 400 bar). The catalyst preferably contains a metal or several metals or one or more oxygen-containing compounds of metals in groups 8 and/or 9 and/or 10 and/or 11 of the periodic table of elements. Preferably, the sugar alcohol is obtained by the hydrogenation of the corresponding sugars. The invention also relates to the use of the reaction product as an additive in cement or concrete production and in other application areas.

    Abstract translation: 本发明涉及一种通过糖醇与氢气和选自氨，伯和仲胺中选择的胺化剂反应制备胺的方法，在催化剂的存在下，在100℃的温度至400℃和压力 1至40MPa（10至400巴）。 催化剂优选含有一种或多种金属或一种或多种元素周期表第8和/或9族和/或10和/或11族金属的含氧化合物。 糖醇优选通过相应糖的氢化获得。 本发明还涉及反应产物作为水泥或混凝土生产和其它应用中的添加剂的用途。

    HYDROGENATING CATALYSTS, PRODUCTION AND USE THEREOF
    4.
    发明申请
    HYDROGENATING CATALYSTS, PRODUCTION AND USE THEREOF 审中-公开
    加氢催化剂，生产和使用

    公开(公告)号：WO2010089266A3

    公开(公告)日：2010-12-23

    申请号：PCT/EP2010051143

    申请日：2010-02-01

    Applicant: BASF SE ,  WIGBERS CHRISTOF WILHELM ,  STEINER JOCHEN ,  ERNST MARTIN ,  HOFFER BRAM WILLEM ,  SCHWAB EKKEHARD ,  MELDER JOHANN-PETER

    Inventor： WIGBERS CHRISTOF WILHELM ,  STEINER JOCHEN ,  ERNST MARTIN ,  HOFFER BRAM WILLEM ,  SCHWAB EKKEHARD ,  MELDER JOHANN-PETER

    IPC: B01J23/78 ,  B01J23/83 ,  B01J27/18 ,  B01J27/185 ,  B01J35/04 ,  B01J37/02 ,  C07C209/48 ,  C07C211/11 ,  C07C211/12 ,  C07C211/36 ,  C07C253/30 ,  C07C255/24

    CPC classification number: B01J23/78 ,  B01J23/83 ,  B01J27/1853 ,  B01J35/04 ,  B01J37/0201 ,  B01J37/0205 ,  B01J37/0215 ,  B01J37/0234 ,  C07C209/48 ,  C07C253/30 ,  C07C2601/14 ,  C07C211/11 ,  C07C211/12 ,  C07C211/36 ,  C07C255/24

    Abstract: The invention relates to a method for improving the catalytic properties of a catalyst that exists in the form of a structured monolith and comprises one or more elements selected from the group comprising cobalt, nickel and copper, wherein the catalyst is brought into contact with one or more base compounds selected from the group of alkali, earth alkali and rare earth metals. The invention further relates to a method for hydrogenating compounds comprising at least one unsaturated carbon-carbon, carbon-nitrogen or carbon-oxygen compound, in the presence of a catalyst comprising one or more elements selected from the group comprising cobalt, nickel and copper, wherein the catalyst exists in the form of a structured monolith, characterized in that the catalyst is brought into contact with one or more base compounds selected from the group of alkali, earth alkali and rare earth metals. In addition, the invention relates to the use of a base compound selected from the group of alkali, earth alkali and rare earth metals for improving the catalytic properties of a catalyst, comprising copper and/or cobalt and/or nickel, wherein the catalyst exists in the form of a structured monolith.

    Abstract translation: 本发明涉及一种用于改善的催化剂，其存在于结构化的整料和或多种元素的选自由钴，镍的含有基团和铜中选择的形式的催化性质，其中与所述催化剂的一种或多种基本 选自碱金属，碱土金属和稀土金属的选择的化合物所接触。 本发明还涉及一种方法，用于包含在催化剂的存在下对含至少一个不饱和碳 - 碳，碳 - 氮或碳 - 氧键的化合物的氢化的组中选择的一种或多种元素自由钴，镍 和铜，其中，所述催化剂是在结构化的单块形式，其特征在于，所述催化剂与选自碱金属，碱土和在接触稀土金属中的一种或多种碱性化合物接触。 此外，本发明是使用选自碱金属，碱土金属和稀土金属中选出的碱性化合物，以提高催化剂的催化性能而言，包含铜和/或钴和/或镍，其特征在于，以结构化的形式的催化剂 整料是存在的。

    METHOD FOR PRODUCING N,N-SUBSTITUTED-3-AMINOPROPAN-1-OLS
    8.
    发明申请
    METHOD FOR PRODUCING N,N-SUBSTITUTED-3-AMINOPROPAN-1-OLS 审中-公开
    用于生产N，N-二取代-3-氨基-1- OLAND

    公开(公告)号：WO2010052181A3

    公开(公告)日：2010-09-30

    申请号：PCT/EP2009064438

    申请日：2009-11-02

    Applicant: BASF SE ,  WIGBERS CHRISTOF WILHELM ,  MELDER JOHANN-PETER ,  ERNST MARTIN

    Inventor： WIGBERS CHRISTOF WILHELM ,  MELDER JOHANN-PETER ,  ERNST MARTIN

    IPC: C07C213/00 ,  C07C215/08

    CPC classification number: C07C213/02 ,  C07C227/08 ,  Y02P20/582 ,  C07C215/08 ,  C07C229/12

    Abstract: The present invention relates to a method for producing N,N-substituted-3-aminopropan-1-ols by a) converting secondary amine with acrolein at a temperature of (-50) to 100°C and a pressure of 0.01 to 300 bar, and b) converting the reaction mixture obtained in step a) with hydrogen and ammonia in the presence of a hydrogenation catalyst at a pressure of 1 to 400 bar, characterized in that in step a) the molar ratio of secondary amine to acrolein is 1:1 or more and the temperature in step b) is in the range of (-50) to 70°C. In a preferred embodiment, an acrolein that was obtained from glycerine based on renewable raw materials is used. The invention further relates to the use of an N,N-dimethyl-3-aminopropan-1-ol (DMAPOL) based on renewable raw materials as a catalyst for producing polyurethane, as a scrubbing liquid in gas scrubbing, in the field of electronics chemicals and electroplating, as a feed material in organic synthesis, and as an intermediate product in the production of pharmaceuticals and plant protection agents.

    Abstract translation: 本发明涉及一种方法，用于制备的N，N-取代的3-氨基丙-1-醇通过a）在（-50的温度下与丙烯醛仲胺的反应）至100℃和0.01的压力 至300巴，和b））在1至400巴的压力下在步骤a）与氢气和氨在氢化催化剂的存在下反应混合物中得到的产物，其特征在于，在阶段的仲胺为丙烯醛1的摩尔比反应： 1以上且在步骤b的范围为（-50）至70℃的温度） 在一个优选的实施方案中，丙烯醛被用于已经从甘油基于可再生资源获得的。 此外，本发明涉及使用一个N，基于可再生原料的N-二甲基-3-氨基丙烷-1-醇（DMAPOL）的，作为用于聚氨酯生产的催化剂，如在气体洗涤器中的洗涤液，在电子化学品和电镀领域中，如在起始原料 有机合成并作为医药和农药的制造中间体。

    METHOD FOR PRODUCING N,N-SUBSTITUTED-1,3-PROPANDIAMINES
    9.
    发明申请
    METHOD FOR PRODUCING N,N-SUBSTITUTED-1,3-PROPANDIAMINES 审中-公开
    用于生产N，N-取代的1,3-丙二胺

    公开(公告)号：WO2009138377A2

    公开(公告)日：2009-11-19

    申请号：PCT/EP2009055655

    申请日：2009-05-11

    Applicant: BASF SE ,  ERNST MARTIN ,  MELDER JOHANN-PETER

    Inventor： ERNST MARTIN ,  MELDER JOHANN-PETER

    IPC: C07C209/26 ,  C07C209/60

    CPC classification number: C07C211/11 ,  C07C209/60 ,  Y02P20/582

    Abstract: The invention relates to a method for producing N,N-substituted- 1,3-propandiamine by a) reacting secondary amines with acrolein at a temperature between (-50) - 100°C and at a pressure between 0,01 - 300 bar, and b) reacting the reaction mixture obtained in step a) with hydrogen and ammonia in the presence of a hydrogenation catalyst at a temperature between 40 - 400°C and at a pressure of 1 - 400 bar. The invention is characterised in that in step a) the molar ratio of secondary amines to acrolein is 2:1 or more and the hydrogenation catalyst used in step b) contains cobalt. In a preferred embodiment, acrolein that is obtained from glycerin based on renewable raw material is used. The invention also relates to the use of a N,N-dimethyl-1,3-propandiamine (DMAPA) based on renewable raw material as charge material for soft soaps and other detergents, coagulation agents, polymers and comb polymers. In another preferred embodiment, step b) takes place in the presence of water.

    Abstract translation: 本发明涉及一种方法，用于制备的N，N-甲基-1,3-丙二胺substiuierten-通过用丙烯醛仲胺的）反应在温度（-50）至100℃和0.01〜300的压力 巴，和b）），在温度40〜400℃和1〜400巴的压力下在步骤a）与氢气和氨在氢化催化剂的存在下反应混合物中得到的产物，其特征在于，在阶段a的摩尔比反应 仲胺为丙烯醛的是2：1或更大，并包含在步骤b中使用）氢化催化剂的钴。 在一个优选的实施方案中，丙烯醛被用于已经从甘油基于可再生资源获得的。 此外，本发明涉及基于可再生Rohstoffenals原料用于在存在一个进一步优选的实施方案中进行软皂和其它清洁剂，凝结剂聚合物和Kammpolymere.In中，阶段b）中使用的N，N-二甲基-1,3-丙二胺（DMAPA）的 水。

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