83.
    发明专利
    未知

    公开(公告)号:BR8704512A

    公开(公告)日:1988-04-19

    申请号:BR8704512

    申请日:1987-09-01

    Applicant: DEGUSSA

    Abstract: Mixtures of sulfurous triazine compounds and methods of preparing these compounds with the general formula I in which R1, R2=H,R2=benzyl, R2, R3, R4=C1-C8-alkyl, allyl, C3-C8 cycloalkyl, the latter unsubstituted or substituted with 1-3 methyl groups, 2-hydroxyethyl, 3-hydroxypropyl, 2-hydroxypropyl or R3 and R4 (together): C4-C6-alkylene, -(CH2-CHX)2 Y with X=H, CH3, Y=O,S, Sa: Polysulfide chain with 2-10 S atoms (i.e. 2 I in which R1, R2, R3, R4 have the meanings indicated above is reacted with an ammonium polysulfide or alkali polysulfide and dissolved in a protic polar solvent, especially water, at a temperature of 80 DEG to 140 DEG C.

    85.
    发明专利
    未知

    公开(公告)号:DE3525475C1

    公开(公告)日:1986-10-09

    申请号:DE3525475

    申请日:1985-07-17

    Applicant: DEGUSSA

    Abstract: A process for preparing titanium disulfide for use as electrode material in batteries. The starting material to be purified has an approximate composition corresponding to TiS2, a content of free sulfur greater than 0.1 weight % and/or a particle diameter d90% greater than 10 mu m and is dispersed in an organic liquid that dissolves sulfur but not TiS2 in a shearing device, is then separated from the liquid phase, washed, and dried with exclusion of air.

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