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公开(公告)号：KR101621310B1
公开(公告)日：2016-05-16
申请号：KR1020140074245
申请日：2014-06-18
Applicant: 고등기술연구원연구조합
IPC: B01D53/02
Abstract: 활성탄소섬유를이용한흡탈착장치및 흡탈착방법이개시된다. 이중 활성탄소섬유를이용한흡탈착장치는오염가스내 오염물질을제거하기위한활성탄소섬유가충진되는흡착탑과, 흡착탑내에전개되는열매체파이프와, 활성탄소섬유의흡착반응시저온의열매체를열매체파이프에제공하고, 활성탄소섬유의탈착반응시고온의열매체를열매체파이프에제공하는열매체공급유닛을포함할수 있다.
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公开(公告)号：KR1020130110292A
公开(公告)日：2013-10-10
申请号：KR1020120032114
申请日：2012-03-29
Applicant: 고등기술연구원연구조합
CPC classification number: C01B32/30 , B01J20/20 , B01J20/28066 , B82B3/0009 , B82Y40/00 , C01B32/354
Abstract: PURPOSE: A manufacturing method of nanopores on carbon matrix is provided to increase the surface area even in case of lowering the carbonizing temperature and activation temperature. CONSTITUTION: A manufacturing method of nanopores on carbon matrix comprises: a step of preparing the precursors which are the respective woody material for activated carbon and fiber material for active carbon fiber as starting materials (S100); a step of stabilizing the precursors by being in contact with air at 200-300°Cand oxidizing (S200); a step of carbonizing the carbon body, which is formed by the stabilizing step, by carbonizing under the anoxic condition at 1000°C and forming the primary pore (S300); a step of performing surface treatment by contacting the carbon body having the primary pore with acid solution (S400); a step of submerging the carbon body which the surface treatment is performed in alkali metal aqueous solution (S500); and a step of performing surface activation by heating under the anoxic atmosphere at 800°C or below and inducing the oxidation and reduction of the alkali metal, and developing the nanopore of 3nm or smaller (S600). [Reference numerals] (S100) Precursor (fiber type, woody type); (S200) Stabilization; (S300) Carbonization; (S400) Surface treatment; (S500) Dipping alkali metal solution; (S600) Surface activation; (S700) Cleaning & drying; (S800) Active carbon fiber, activated carbon (surface area 2,500m^2/g or more)
Abstract translation: 目的：提供碳基体上纳米孔的制造方法，即使在降低碳化温度和活化温度的情况下也能增加表面积。 构成：碳基体上的纳米孔的制造方法包括：制备作为活性炭的各种木质材料的前体和作为起始原料的活性炭纤维的纤维材料的步骤（S100）。 通过与200-300℃的空气接触来稳定前体的步骤，可以进行氧化（S200）。 通过在稳定化步骤中形成的碳体碳化碳酸化步骤，在1000℃的缺氧条件下碳化并形成一次孔（S300）; 通过使具有一次孔的碳体与酸溶液接触进行表面处理的步骤（S400）; 浸渍在碱金属水溶液中进行表面处理的碳体的工序（S500）。 通过在800℃以下的缺氧气氛下进行加热而引起碱金属的氧化还原，显影3nm以下的纳米孔（S600）进行表面活化的工序。 （附图标记）（S100）前体（纤维型，木质型）; （S200）稳定化; （S300）碳化; （S400）表面处理; （S500）浸渍碱金属溶液; （S600）表面活化; （S700）清洗干燥; （S800）活性炭纤维，活性炭（表面积2500m ^ 2 / g以上）
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公开(公告)号：KR1020180028826A
公开(公告)日：2018-03-19
申请号：KR1020160116687
申请日：2016-09-09
Applicant: 고등기술연구원연구조합
CPC classification number: C10C3/002 , C10G1/02 , C10G2300/4006
Abstract: 역청원료의열분해장치및 열분해방법이개시된다. 본발명의실시예에따른역청원료의열분해장치는역청원료를저장하는저장조, 저장조로부터역청원료를공급받고, 역청원료를열분해가스와무기부산물로열분해하는열분해반응기, 열분해가스를기체생성물과액체생성물로분리하는기액분리기, 기체생성물과무기부산물을공급받아서서로열교환시키는열교환기및 열분해반응기, 기액분리기및 열교환기를제어하는제어부를포함하고, 열교환기를통과하여온도가상승된기체생성물은저장조및 열분해반응기중 적어도어느하나에공급된다.
Abstract translation: 公开了用于沥青材料的原料的热解设备和热解方法。 根据本发明的实施例的沥青材料的热解设备正在从贮存供给到沥青材料，贮存器，用于存储所述沥青材料，热解反应器，所述热解气体的气体产物和液体产物热解副产物的沥青材料的热解气体和无机 气 - 液分离器，一个热交换器和热分解反应器，气 - 液分离器，以及用于控制热交换器的控制单元，并且温度上升通过在气体产品储罐和用于气态产物的热解反应器的热交换器和进行无机副产物供应热给对方，通过分离 或者类似的。
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公开(公告)号：KR101419868B1
公开(公告)日：2014-07-16
申请号：KR1020130044024
申请日：2013-04-22
Applicant: 고등기술연구원연구조합
CPC classification number: C01B32/05 , B01J6/00 , B82B1/008 , B82B3/0009 , C01B32/30
Abstract: Disclosed is a method of preparing a nano-pore on a carbon material. According to the disclosed invention, the method includes: a preparation process S100 of preparing a precursor using an wood-based material for an activated carbon and a fiber-based material for an activated carbon fiber as starting materials; an oxidation process S200 of contacting the precursor with air in a temperature range of 200-300°C to oxidize the precursor; a carbonization process S300 of carbonizing a carbon material formed during the oxidation at a temperature of 1,000°C in an anaerobic condition to form a primary pore; a surface treatment process S400 of performing a surface treatment by bringing the carbon material on which the primary pore is formed into contact with an ozone, to uniformly form an oxygen functional group on a surface of a carbon lattice at a high concentration, a dipping process S500 of dipping the carbon material having undergone the surface treatment in the an aqueous solution of alkali metal to bring the alkali metal into contact with the oxygen functional group formed by the ozone contact of the surface treatment process; a surface modification process S600 of performing a surface modification by inducing oxidation and reduction of the alkali metal at a temperature condition of 600-800°C in an anaerobic atmosphere to develop a micro pore less than or equal to 3 nm; and a surface stabilization process of cooling the carbon to 300°C while maintaining the anaerobic atmosphere and injecting water to generate steam, thus cooling the carbon material from 300°C to room temperature.
Abstract translation: 公开了一种在碳材料上制备纳米孔的方法。 根据所公开的发明，该方法包括：使用活性炭用木基材料制备前体的制备方法S100和活性炭纤维用纤维类原料作为原料; 在200-300℃的温度范围内使前体与空气接触以氧化前体的氧化工艺S200; 碳化处理S300，在厌氧条件下在1000℃的温度下氧化形成的碳材料碳化，形成初级孔; 进行表面处理的表面处理工序S400，其中使形成有一次孔的碳材料与臭氧接触，在碳晶格表面上以高浓度均匀地形成氧官能团，浸渍处理 S500将经过表面处理的碳材料浸渍在碱金属水溶液中，使碱金属与由表面处理工艺的臭氧接触形成的氧官能团接触; 通过在厌氧气氛中在600-800℃的温度条件下诱导碱金属氧化还原而进行表面改性以形成小于或等于3nm的微孔的表面改性方法S600; 以及将碳冷却至300℃同时保持厌氧气体并注入水以产生蒸汽的表面稳定化方法，从而将碳材料从300℃冷却至室温。
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Patent Agency Ranking
公开(公告)号：KR1020140085974A
公开(公告)日：2014-07-08
申请号：KR1020120155910
申请日：2012-12-28
Applicant: 고등기술연구원연구조합
IPC: C07D403/12 , C07D233/84 , C10G1/00
Abstract: Disclosed is a method for synthesizing an ionic liquid for dissolving coal. The method for synthesizing an ionic liquid for dissolving coal disclosed according to an embodiment of the present invention comprises the steps of: (S100) dissolving a first precursor in methylene chloride at an appropriate ratio in order to be cooled; (S200) injecting tosyl chloride and potassium hydroxide in the solution; (S300) agitating the solution at room temperature after a particular period of time in order to be changed into a white suspension, washing a filtrate several times with distilled water in a filtering process, removing the moisture of an organic layer, and performing vacuum concentration; (S400) synthesizing a second precursor which is a white solid through a plurality of column chromatography techniques; (S500) injecting methylimidazole in the second precursor in order to be mixed into a solvent which is also a reagent; (S600) performing a reflux process at an appropriate temperature; and (S700) obtaining a plurality of final ionic liquids by washing layer-separated oil with anhydrous ether dozens of times.
Abstract translation: 公开了一种合成用于溶解煤的离子液体的方法。 根据本发明实施方案的合成溶解煤的离子液体的方法包括以下步骤：（S100）以适当的比例将第一前体溶解在二氯甲烷中以便冷却; （S200）在溶液中注入甲苯磺酰氯和氢氧化钾; （S300）在特定时间后在室温下搅拌溶液，以便变成白色悬浮液，在过滤过程中用蒸馏水洗涤滤液数次，除去有机层的水分，并进行真空浓缩 ; （S400）通过多个柱色谱技术合成作为白色固体的第二前体; （S500）在第二前体中注入甲基咪唑以便混合到也是试剂的溶剂中; （S600）在适当的温度下进行回流处理; 和（S700）通过用无水乙醚洗涤分层的油几十次获得多个最终的离子液体。
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公开(公告)号：KR1020120121952A
公开(公告)日：2012-11-07
申请号：KR1020110039867
申请日：2011-04-28
Applicant: 고등기술연구원연구조합
CPC classification number: B01J20/2808 , B01J20/20 , B01J20/28023 , B01J20/3078 , C01B32/382
Abstract: PURPOSE: A manufacturing method of carbon matrix nano-pores is provided to increase surface area by developing micro pores having 3 nano meters or less on the carbon matrix having pores. CONSTITUTION: A manufacturing method of carbon matrix nano-pores comprises the following steps: (S100) preparing a precursor made of wood composite or fiber materials; (S200) oxidizing the precursor at 200-300 deg. Celsius by contacting with air; (S300) forming first pores by carbonizing the formed carbon body at 1000 deg. Celsius under inert condition; (S400) forming oxygen functional group of the carbon grating surface by surface treating thereof by contacting with ozone; (S500)contacting alkali metal to the oxygen functional group by precipitating the surface treated carbon body into an alkali metal aqueous solution; and (S600) increasing the temperature up to 800 deg. Celsius or less under the anoxic atmosphere, and developing micro pores having 3 nano meters or less by inducing oxidation and reduction of the alkali metals. [Reference numerals] (S100) Precursor made of wood composite or fiber materials; (S200) Stabilization; (S300) Carbonization; (S400) Surface treatment; (S500) Dipping alkali metal solution; (S600) Surface activation; (S700) Cleaning & drying; (S800) Active carbon fiber, active carbon(2500 m^2/g of surface stone or higher)
Abstract translation: 目的：提供碳基质纳米孔的制造方法，通过在具有孔隙的碳基质上开发具有3纳米或更小的微孔来增加表面积。 构成：碳基纳米孔的制造方法包括以下步骤：（S100）制备由木材复合材料或纤维材料制成的前体; （S200）在200-300度氧化前体。 与空气接触; （S300）通过在1000度碳化碳化碳体而形成第一孔。 在惰性条件下摄取; （S400）通过与臭氧接触进行表面处理而形成碳素光栅表面的氧官能团; （S500）通过将表面处理的碳体沉淀到碱金属水溶液中使碱金属与氧官能团接触; 和（S600）将温度升高到800度。 在缺氧气氛下摄氏度以下，通过诱导碱金属的氧化还原，显影3微米以下的微孔。 （附图标记）（S100）由木质复合材料或纤维材料制成的前体 （S200）稳定化; （S300）碳化; （S400）表面处理 （S500）浸渍碱金属溶液; （S600）表面活化; （S700）清洗干燥; （S800）活性碳纤维，活性炭（2500m ^ 2 / g表面石或更高）
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公开(公告)号：KR101851313B1
公开(公告)日：2018-04-23
申请号：KR1020160116537
申请日：2016-09-09
Applicant: 고등기술연구원연구조합
Abstract: 역청원료의열분해장치및 열분해방법이개시된다. 본발명의실시예에따른역청원료의열분해장치는역청원료를저장하는저장조, 저장조로부터역청원료를공급받고, 역청원료를열분해하여제 1 열분해가스와제 1 무기부산물을생성하는제 1 열분해반응기, 제 1 열분해가스를제 1 기체생성물과제 1 액체생성물로분리하는제 1 기액분리기, 제 1 열분해반응기의하단에설치되고, 제 1 열분해반응기에서열분해된역청원료를재차열분해하여제 2 열분해가스와제 2 무기부산물을생성하는제 2 열분해반응기, 제 2 열분해가스를제 2 기체생성물과제 2 액체생성물로분리하는제 2 기액분리기, 제 1 액체생성물을포집하는제 1 포집조, 제 2 액체생성물을포집하는제 2 포집조및 제 1 열분해반응기, 제 1 기액분리기, 제 2 열분해반응기및 제 2 기액분리기를제어하는제어부를포함한다.
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公开(公告)号：KR1020180028832A
公开(公告)日：2018-03-19
申请号：KR1020160116712
申请日：2016-09-09
Applicant: 고등기술연구원연구조합
CPC classification number: C10C3/002 , C10G1/02 , C10G2300/4006
Abstract: 역청원료의열분해장치및 열분해방법이개시된다. 본발명의실시예에따른역청원료의열분해장치는역청원료를저장하는저장조, 저장조로부터역청원료를공급받고, 역청원료를열분해하는열분해반응기, 역청원료를열분해하는열분해반응기, 열분해반응기에서열분해된열분해가스를기체생성물과액체생성물로분리하는기액분리기, 기액분리기에서분리된기체생성물을공급받고, 기체생성물을연소시켜서역청원료의열분해에필요한열원을열분해반응기에제공하는연소부및 상기열분해반응기, 상기기액분리기및 상기연소부를제어하는제어부를포함한다.
Abstract translation: 公开了用于沥青材料的原料的热解设备和热解方法。 根据本发明的实施例的沥青材料的热解设备是在热解反应器热裂解的热解，热解反应器到储存罐，热解反应器的热分解，所述沥青材料从贮存器被供应到所述沥青材料，沥青材料，用于存储沥青材料的热裂解 气 - 液分离器的气体中分离的气体产品和液体产品在被供给到气液分离器分离的气态产物，通过燃烧气体产物中的燃烧器单元，以提供沥青材料的热解的热解反应器和所述热解反应器，所需要的热源 装置液体分离器和用于控制燃烧单元的控制单元。
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