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    균일한 중형 기공을 갖는 복합 산화물 촉매, 그 제조 방법 및 상기 촉매를 이용하여 에스테르 화합물을 제조하는 방법
    2.
    发明公开
    균일한 중형 기공을 갖는 복합 산화물 촉매, 그 제조 방법 및 상기 촉매를 이용하여 에스테르 화합물을 제조하는 방법 有权
    具有订购的MESOPORES的混合氧化物催化剂，其制备方法和使用其制备酯化合物的方法

    公开(公告)号：KR1020130129739A

    公开(公告)日：2013-11-29

    申请号：KR1020120053823

    申请日：2012-05-21

    Applicant: 서울대학교산학협력단

    Inventor： 이종협 ,  김태용 ,  박대성 ,  최영보 ,  백자연 ,  박재률

    IPC: B01J35/04 ,  B01J23/30 ,  B01J21/06 ,  C07C69/14

    CPC classification number: B01J23/30 ,  B01J23/002 ,  B01J35/1004 ,  B01J35/1061 ,  B01J37/08 ,  B01J2523/00 ,  B01J2523/41 ,  B01J2523/48 ,  B01J2523/69 ,  C07C69/02

    Abstract: The present invention provides a complex oxide catalyst having cylindrical regular mesopores and excellent acid characteristics and a manufacturing method thereof. A complex oxide catalyst according to the concrete example of the present invention includes tungsten oxide, zirconium oxide, and silicon oxide. The atomic fraction of the tungsten and the silicon is 0.1/1-0.14/1, and the atomic fraction of the zirconium and the silicon is 0.1/1-0.14/1. Moreover, the present invention provides a method for effectively manufacturing a high-value ester compound from ethanol and a carboxylic acid compound using the complex oxide catalyst. [Reference numerals] (AA) Example 1;(BB) Example 2;(CC) Example 3;(DD) Comparative example 2;(EE) Comparative example 3

    Abstract translation: 本发明提供具有圆筒形规则中孔和优异酸性特征的复合氧化物催化剂及其制造方法。 根据本发明的具体实例的复合氧化物催化剂包括氧化钨，氧化锆和氧化硅。 钨和硅的原子分数为0.1 / 1-0.14 / 1，锆和硅的原子分数为0.1 / 1-0.14 / 1。 此外，本发明提供一种使用复合氧化物催化剂从乙醇和羧酸化合物有效制造高价值酯化合物的方法。 （AA）实施例1;（BB）实施例2;（CC）实施例3;（DD）比较例2;（EE）比较例3

    3차원의 열린 기공 구조를 갖는 알루미노실리케이트 구형 나노 입자, 그 제조방법 및 상기 나노 입자를 이용하여 글리세롤로부터 아크릴산을 제조하는 방법
    3.
    发明公开
    3차원의 열린 기공 구조를 갖는 알루미노실리케이트 구형 나노 입자, 그 제조방법 및 상기 나노 입자를 이용하여 글리세롤로부터 아크릴산을 제조하는 방법 有权
    具有三维开口孔的二氧化铝纳米球，其制备方法和使用该方法从甘油生产丙烯酸的方法

    公开(公告)号：KR1020130109662A

    公开(公告)日：2013-10-08

    申请号：KR1020120031597

    申请日：2012-03-28

    Applicant: 서울대학교산학협력단

    Inventor： 이종협 ,  최영보 ,  윤양식 ,  박홍석 ,  윤다님

    IPC: C01B33/26 ,  B82B3/00 ,  B82Y40/00

    CPC classification number: C01B33/26 ,  B01J23/22 ,  B01J23/28 ,  C01P2004/32 ,  C01P2004/64 ,  C01P2006/12

    Abstract: PURPOSE: Provided are an aluminosilicate sphere nano particle, a manufacturing method thereof, and a method for acrylic acid using the same, wherein the aluminosilicate sphere nano particle can easily transfer a reactant to the inside of a pore, minimize material transfer resistance, and have wide specific surface area while maintaining an acid characteristic of the aluminosilicate. CONSTITUTION: An aluminosilicate sphere nano particle has an open pore structure in a form wherein the size of the particle increases in a direction in which the radius of the particle increases from the center of the particle. The specific surface area of the nano particle is at least 100 m^2/g. The manufacturing method of the aluminosilicate sphere nano particle comprises the steps of: performing a first hydrothermal process on a solution including a silica precursor, a polar solvent, a non-polar solvent, an ionic surfactant and an alkaline compound in a pressure vessel; controlling the pH of the first hydrothermal process treated solution to 2-7 using an acidic aqueous solution; inserting an aluminum precursor into a pH-controlled solution; and performing a second hydrothermal process on the solution into which aluminum precuesor is inserted in the pressure vessel.

    Abstract translation: 目的：提供一种铝硅酸盐球纳米颗粒及其制造方法和使用该方法的丙烯酸的方法，其中硅铝酸球体纳米颗粒可以容易地将反应物转移到孔内，使材料转移阻力最小化，并具有 同时保持铝硅酸盐的酸特性。 构成：铝硅酸盐球纳米颗粒具有开孔形式，其中颗粒的尺寸在颗粒的半径从颗粒的中心增加的方向上增加。 纳米颗粒的比表面积为至少100m 2 / g。 铝硅酸盐球纳米颗粒的制造方法包括以下步骤：在压力容器中对包含二氧化硅前体，极性溶剂，非极性溶剂，离子表面活性剂和碱性化合物的溶液进行第一水热法; 使用酸性水溶液控制第一次水热处理溶液的pH至2-7; 将铝前体插入pH控制的溶液中; 并在铝压片机插入压力容器中的溶液上进行第二次水热处理。

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