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公开(公告)号：KR101262967B1
公开(公告)日：2013-05-10
申请号：KR1020110048572
申请日：2011-05-23
Applicant: 이창호 , 충남대학교산학협력단
IPC: C08K9/04 , C08K3/34 , C08L101/00 , C08J3/20
Abstract: 고분자내에서일라이트의분산성을향상시키는방법이개시된다. 본발명에의한일라이트의분산성향상방법은, (1) 용매에아민계화합물과산을가하여복합용액을제조하는제1단계; (2) 상기제1단계를통하여제조된복합용액에일라이트를가하고반응시키는제2단계; 및 (3) 상기제2단계를통하여복합용액과반응된일라이트를세척및 건조시키는제3단계;를포함하여이루어진다.
Abstract translation: 公开了一种改善铟在聚合物中的分散性的方法。 根据本发明，提供了一种改善Hanilite分散性的方法，包括以下步骤：（1）通过向溶剂中加入胺化合物和酸来制备复合溶液; （2）向通过第一步骤制备的复合溶液中加入二锂并使稀释溶液反应的第二步骤; （3）通过第二步清洗并干燥与复合溶液反应的刺激物。
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公开(公告)号：KR1020120130558A
公开(公告)日：2012-12-03
申请号：KR1020110048572
申请日：2011-05-23
Applicant: 이창호 , 충남대학교산학협력단
IPC: C08K9/04 , C08K3/34 , C08L101/00 , C08J3/20
CPC classification number: C08K3/346 , C07C211/03 , C08J3/03 , C08K9/04
Abstract: PURPOSE: A method for improving dispersity of illite in a polymer is provided to improve the dispersity of illite through a reaction with an amine-based compound-containing composite solution and a fluoric acid solution. CONSTITUTION: A method for improving dispersity of illite in a polymer comprises: a first step of preparing a composite solution by adding a silane-based compound to a solvent; a second step of adding illite to the composite solution and conducting a reaction; and a third step of cleaning and drying illite which is reacted with the composite solution through the second step; and an additional fourth step of adding fluorine gas to the illite to conduct a reaction. [Reference numerals] (AA) Comparative embodiment; (BB) Embodiment 1; (CC) Embodiment 2
Abstract translation: 目的：提供改善聚合物中伊利石分散性的方法，以通过与含胺类化合物的复合溶液和氟酸溶液的反应来改善伊利石的分散性。 构成：提高聚合物中伊利石分散性的方法包括：通过向溶剂中加入硅烷类化合物制备复合溶液的第一步骤; 将伊利石添加到复合溶液中并进行反应的第二步; 以及通过第二步骤清洗和干燥与复合溶液反应的伊利石的第三步骤; 以及向伊利石添加氟气以进行反应的另外的第四步骤。 （附图标记）（AA）比较实施例; （BB）实施例1; （CC）实施例2
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Patent Agency Ranking
公开(公告)号：KR101419908B1
公开(公告)日：2014-07-16
申请号：KR1020130063035
申请日：2013-05-31
Applicant: 충남대학교산학협력단
Abstract: Disclosed are a high crystalline TIOF2 and a method of preparing the same. According to the present invention, the method of preparing a high crystalline TIOF2 includes: a first step (1) of preparing a titanium dioxide precursor solution by mixing an alcohol and a titanium dioxide precursor; a second step (2) of adjusting a pH by adding an acid to a solution obtained through the first step; a third step (3) of gelling a mixture solution obtained through the second step; and a fourth step (4) of preparing TIOF2 by settling a resultant mixture obtained through the third step in a reactor and injecting a nitrogen trifluoride to the reactor to react with the resultant mixture. The present invention can provide a high crystalline TIOF2 with a uniform shape in a nano-size by even a simple process.
Abstract translation: 公开了高结晶TIOF2及其制备方法。 根据本发明，制备高结晶TIOF2的方法包括：通过混合醇和二氧化钛前体制备二氧化钛前体溶液的第一步骤（1） 通过向通过第一步获得的溶液中加入酸来调节pH的第二步骤（2）; 第三步骤（3），其通过第二步骤获得的混合溶液胶凝; 以及通过将通过第三步骤获得的所得混合物沉淀在反应器中并将三氟化氮注入反应器以与所得混合物反应来制备TIOF2的第四步骤（4）。 本发明可以通过简单的工艺提供具有纳米尺寸均匀形状的高结晶TIOF2。
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公开(公告)号：KR101206488B1
公开(公告)日：2012-11-30
申请号：KR1020100101867
申请日：2010-10-19
Applicant: 충남대학교산학협력단
IPC: C08K9/04 , C08K3/34 , C08L101/00 , C09K21/14
Abstract: 일라이트를 함유한 난연성 고분자 복합체 및 그 제조방법이 개시된다.
본 발명에 따른 일라이트를 함유한 난연성 고분자 복합체의 제조방법은, (1) 일라이트를 반응기 내에 투입하고, 열처리하는 제1단계; (2) 반응기 내에 불소 가스를 주입하여, 제1단계를 통하여 열처리된 일라이트를 불소 처리하는 제2단계; (3) 상기 제2단계를 통하여 불소 처리된 일라이트를 고분자와 혼합하여 혼합물을 제조하는 제3단계; (4) 상기 제3단계를 통하여 얻어진 혼합물에 가교제를 혼합하는 제4단계; 및 (5) 상기 제4단계에서 얻어진 혼합물을 이용하여 고분자 복합체를 제조하는 제5단계;를 포함하여 이루어진다.-
公开(公告)号：KR1020120040442A
公开(公告)日：2012-04-27
申请号：KR1020100101867
申请日：2010-10-19
Applicant: 충남대학교산학협력단
IPC: C08K9/04 , C08K3/34 , C08L101/00 , C09K21/14
CPC classification number: C08K9/02 , C08K3/016 , C08K3/346 , C08K5/0025 , C08L101/00 , C08L2201/02
Abstract: PURPOSE: A manufacturing method of an Illite-containing flame-retarding polymer composite is provided to improve the dispersity of illite by fluorine-treating illite, thereby manufacturing a polymer composite with excellent flame-retardancy and properties. CONSTITUTION: A manufacturing method of an Illite-containing flame-retarding polymer composite comprises a step of manufacturing heat-treating by putting illite into a reactor; a step of fluorine-treating the illite by putting fluorine gas into the reactor; a step of manufacturing mixture by mixing the illite with a polymer; a step of mixing a cross-linking agent with the mixture; and a step of manufacturing polymer composite by using the mixture.
Abstract translation: 目的：提供含有伊利石的阻燃聚合物复合材料的制造方法，以通过氟化处理伊利石来改善伊利石的分散性，从而制造具有优异阻燃性和特性的聚合物复合材料。 构成：含有伊利石的阻燃聚合物复合材料的制造方法包括通过将伊利石放入反应器中来进行热处理的步骤; 通过将氟气进入反应器来对伊利石进行氟处理的步骤; 通过将伊利石与聚合物混合制造混合物的步骤; 将交联剂与混合物混合的步骤; 以及通过使用该混合物制造聚合物复合材料的步骤。
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公开(公告)号：KR101262966B1
公开(公告)日：2013-05-10
申请号：KR1020110048567
申请日：2011-05-23
Applicant: 이창호 , 충남대학교산학협력단
Abstract: 고분자내에서일라이트의분산성을향상시키는방법이개시된다. 본발명에의한일라이트의분산성향상방법은, (1) 용매에실란계화합물을가하여복합용액을제조하는제1단계; (2) 상기제1단계를통하여제조된복합용액에일라이트를가하고반응시키는제2단계; 및 (3) 상기제2단계를통하여복합용액과반응된일라이트를세척및 건조시키는제3단계;를포함하여이루어진다.
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公开(公告)号：KR1020120130554A
公开(公告)日：2012-12-03
申请号：KR1020110048567
申请日：2011-05-23
Applicant: 이창호 , 충남대학교산학협력단
CPC classification number: C08K3/346 , C07C211/03 , C08J3/03 , C08K3/015 , C08K9/06
Abstract: PURPOSE: A method of improving dispersity of illite is provided to obtain illite with improved dispersity in a polymer by reacting illite with a composite solution comprising a silane-based compound; and a fluorine gas. CONSTITUTION: A method of improving dispersity of illite comprises: a first step of preparing a composite solution by adding a silane-based compound to a solvent; a second step of adding illite to the composite solution and conducting a reaction; and a third step of cleaning and drying illite which is reacted with the composite solution through the second step; and an additional fourth step putting the illite into a reactor and reacting illite and fluorine gas by injecting fluorine gas into the reactor. [Reference numerals] (AA) Comparative embodiment; (BB) Embodiment 1; (CC) Embodiment 2
Abstract translation: 目的：提供改善伊利石分散性的方法，以使伊利石与包含硅烷基化合物的复合溶液反应，从而获得具有改善聚合物分散性的伊利石; 和氟气。 构成：改善伊利石分散性的方法包括：通过向溶剂中加入硅烷基化合物来制备复合溶液的第一步骤; 将伊利石添加到复合溶液中并进行反应的第二步; 以及通过第二步骤清洗和干燥与复合溶液反应的伊利石的第三步骤; 另外还有第四步，将伊利石放入反应器中，并将氟气注入反应器中，从而使伊利石和氟气反应。 （附图标记）（AA）比较实施例; （BB）实施例1; （CC）实施例2
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