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公开(公告)号:JP2000281830A
公开(公告)日:2000-10-10
申请号:JP8966999
申请日:1999-03-30
Applicant: KUMAMOTO PREFECTURE , AGENCY IND SCIENCE TECHN
Inventor: SUGATA TAKESHI , SAKO TAKESHI , OTAKE KATSUTO , NAGAOKA SHOJI , NAGATA MASANORI
Abstract: PROBLEM TO BE SOLVED: To provide the methods for separating and purifying carbon material that comprises the removal of resol resin or novolak resins from the carbon material without damage to the carbon material at a low temperature efficiently without occurrence of injurious or harmful substance on the outside of the system and provide the purification of the carbon material. SOLUTION: A carbon material-containing resin of crushed resol resin or novolak resin is allowed to react in a basic organic solvent of >=0.5 M of alkali concentration and contains 20 to 100 vol.% of water at 300-400 deg.C in the reactor to remove the resol resin or novolak resin component from the carbon material. Then, the carbon material is washed and purified whereby the carbon material is recovered from the carbon material-containing resin.
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公开(公告)号:JPH1087872A
公开(公告)日:1998-04-07
申请号:JP26124096
申请日:1996-09-09
Applicant: AGENCY IND SCIENCE TECHN , KUMAMOTO PREFECTURE
Inventor: SUGATA TAKESHI , NAKANE TAKASHI , SAKO TAKESHI , OTAKE KATSUTO , UENO KATSUHIKO , SATO SHINJI , NAGAOKA SHOJI , NAGATA MASANORI , NAGAYAMA SANPEI , KAMIMURA MAKOTO
IPC: C08J11/10
Abstract: PROBLEM TO BE SOLVED: To enable reinforcing fibers to be separated, recovered, and reused efficiently without damaging the fibers by bringing a fiber-reinforced plastic into contact and reaction with (sub)supercritical water. SOLUTION: After a fiber-reinforced plastic is charged into a reactor 1 and water supplied from a water cylinder 2 to a water tank 3 is charged into the reator 1 through a high-pressure pump 4 so that water occupies 1-50vol.% of the reactor 1, valves 5, 6 are closed and the reactor 1 is hermetically sealed. Then, a heat exchanger 8 and the reactor 1 are heated to 320-500 deg.C with a constant temp. bath 7 to bring water in the reactor 1 into a (sub)supercritical state. The reinforced plastic is brought into contact with the water in a (sub) supercritical state and thus is reacted. The reactor 1 is then returned to normal temp. and the valve 6 is opened to separate and recover a gaseous part contg. hydrocarbons, carbon dioxide, nitrogen, etc., through a trap 9.
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公开(公告)号:DE69711575D1
公开(公告)日:2002-05-08
申请号:DE69711575
申请日:1997-12-15
Applicant: AGENCY IND SCIENCE TECHN
Inventor: SAKO TAKESHI , SATO MASAHITO , SUGETA TSUTOMU , OTAKE KATSUTO , OKANO MAKOTO
IPC: A62D3/20 , A62D101/22 , A62D3/00
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公开(公告)号:DE19712045A1
公开(公告)日:1997-12-11
申请号:DE19712045
申请日:1997-03-21
Applicant: AGENCY IND SCIENCE TECHN
Inventor: SAKO TAKESHI , SATO MASAHITO , SUGETA TSUTOMU , OTAKE KATSUTO , TSUGUMI MASAYUKI
IPC: A62D3/20 , A62D3/38 , A62D101/08 , A62D101/22 , A62D101/26 , A62D101/28 , B09B3/00 , A62D3/00
Abstract: A method of decomposing dioxin compounds, such as polychlorodibenzo-p-dioxins and polychlorodibenzofurans, contained in a waste material into unharmful substances, wherein the waste material is treated with a supercritical water at a temperature higher than the critical temperature of water and a pressure higher than the critical pressure of water.
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公开(公告)号:DE69711575T2
公开(公告)日:2002-11-28
申请号:DE69711575
申请日:1997-12-15
Applicant: AGENCY IND SCIENCE TECHN
Inventor: SAKO TAKESHI , SATO MASAHITO , SUGETA TSUTOMU , OTAKE KATSUTO , OKANO MAKOTO
IPC: A62D3/20 , A62D101/22 , A62D3/00
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公开(公告)号:GB2314079B
公开(公告)日:2000-06-28
申请号:GB9706070
申请日:1997-03-24
Applicant: AGENCY IND SCIENCE TECHN
Inventor: SAKO TAKESHI , SATO MASAHITO , SUGETA TSUTOMU , OTAKE KATSUTO , TSUGUMI MASAYUKI
IPC: A62D3/20 , A62D3/38 , A62D101/08 , A62D101/22 , A62D101/26 , A62D101/28 , B09B3/00 , A62D3/00
Abstract: A method of decomposing dioxin compounds, such as polychlorodibenzo-p-dioxins and polychlorodibenzofurans, contained in a waste material into unharmful substances, wherein the waste material is treated with a supercritical water at a temperature higher than the critical temperature of water and a pressure higher than the critical pressure of water.
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公开(公告)号:GB2314079A
公开(公告)日:1997-12-17
申请号:GB9706070
申请日:1997-03-24
Applicant: AGENCY IND SCIENCE TECHN
Inventor: SAKO TAKESHI , SATO MASAHITO , SUGETA TSUTOMU , OTAKE KATSUTO , TSUGUMI MASAYUKI
IPC: A62D3/20 , A62D3/38 , A62D101/08 , A62D101/22 , A62D101/26 , A62D101/28 , B09B3/00 , A62D3/00
Abstract: A method of decomposing dioxin compounds, such as polychlorodibenzo-p-dioxins and polychlorodibenzofurans, contained in a waste material into unharmful substances, wherein the waste material is treated with a supercritical water at a temperature higher than the critical temperature of water and a pressure higher than the critical pressure of water.
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公开(公告)号:JPH11209317A
公开(公告)日:1999-08-03
申请号:JP940198
申请日:1998-01-21
Applicant: AGENCY IND SCIENCE TECHN , SHIN NIPPON AIR TECH CO LTD
Inventor: SAKO TAKESHI , KANZAWA CHIYOJI , SUGATA TAKESHI , OTAKE KATSUTO , TSUGUMI MASAYUKI , SHUDO HARUHISA
Abstract: PROBLEM TO BE SOLVED: To provide a method for recovering monomers from polyethylene terephthalate, harmless to human bodies and natural environment, etc., and capable of simply carrying out separation and recovery, etc. of the monomer under industrially advantageous conditions. SOLUTION: This method for recovering monomers from polyethylene terephthalate comprises obtaining diethyl terephthalate and ethylene glycol which are monomers by reacting polyethylene terephthalate with supper critical ethanol.
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公开(公告)号:JPH09327678A
公开(公告)日:1997-12-22
申请号:JP14694096
申请日:1996-06-10
Applicant: AGENCY IND SCIENCE TECHN
Inventor: SAKO TAKESHI , SATO SHINJI , SUGATA TAKESHI , OTAKE KATSUTO , TSUGUMI MASAYUKI
IPC: A62D3/20 , A62D3/38 , A62D101/08 , A62D101/22 , A62D101/26 , A62D101/28 , B09B3/00 , A62D3/00
Abstract: PROBLEM TO BE SOLVED: To make dioxins harmless by an industrially advantageous method wherein inorg. powder contg. dioxins is dispersed into supercritical water held at least at the critical temp. and at least under the critical pressure and dioxins are decomposed under this condition. SOLUTION: Inorg. powder contg. dioxins, water and open air are filled in a reactor and it is heated at 653-873K being at least critical temp. of water, pref. 653-773K. In this case, the reaction pressure is controlled by wt. of water filled in the reactor and 22-40MPa, pref. 25-35MPa is pref. After a specified reaction time passes, in the case where an oxidizing agent is not incorporated, at least 96.5% dioxins in the reactor are decomposed and in the case where such an oxidizing agent as hydrogen peroxide and oxygen gas is incorporated, at least 98.5% dioxins are decomposed. Thereby, dioxins can be made harmless by an industrially advantageous method without necessitating high reaction temp. and complicated reaction control.
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公开(公告)号:JP2001089129A
公开(公告)日:2001-04-03
申请号:JP26477899
申请日:1999-09-20
Applicant: AGENCY IND SCIENCE TECHN
Inventor: YODA SATOSHI , OTAKE KATSUTO , TAKEBAYASHI YOSHIHIRO , SUGATA TAKESHI , SAKO TAKESHI
Abstract: PROBLEM TO BE SOLVED: To solve the problems of conventional process for the impregnation of a metal compound in a wet silica gel in liquid phase comprising the long time necessary for the impregnation into the gel depending on the kind and concentration of the compound and the formation of an insufficiently impregnated product to cause frequent failure in getting a monolithic composite material of metal compound and silica aerogel. SOLUTION: A dry medium mixed with a metal compound is impregnated in a wet silica gel and dried to obtain a silica aerogel composed of the metal compound and silica particles forming a composite material. In the above process, both of the impregnation process and the drying process are carried out under supercritical condition of the dry medium to obtain the objective monolithic composite material of metal compound and silica aerogel.
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