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    2.
    发明专利
    未知

    公开(公告)号：DE59201217D1

    公开(公告)日：1995-03-02

    申请号：DE59201217

    申请日：1992-03-28

    Applicant: BASF AG

    Inventor： KOPPENHOEFER GERHARD ,  SCHROEDER WOLFGANG DR ,  VOGES DIETER DR

    IPC: C07C213/02

    Abstract: alpha , omega -Amino alcohols of the general formula I HO-CH2-X-CH2-NH2 (I> in which X represents a C1- to C20-alkylene chain which is optionally substituted by inert radicals and/or optionally interrupted by oxygen or nitrogen, are prepared by reacting alpha , omega -alkanediols of the general formula II HO-CH2-X-CH2-OH (II> in which the bridging member X has the abovementioned meanings, with ammonia and a catalyst at temperatures from 150 to 300 DEG C and pressures from 50 to 300 bar, characterised in that catalysts are employed whose catalytically active mass consists to 5 to 100% by weight of iron.

    3.
    发明专利
    未知

    公开(公告)号：DE4010227A1

    公开(公告)日：1991-10-02

    申请号：DE4010227

    申请日：1990-03-30

    Applicant: BASF AG

    Inventor： MERGER FRANZ DR ,  PRIESTER CLAUS-ULRICH DR ,  WITZEL TOM DR ,  KOPPENHOEFER GERHARD ,  HARDER WOLFGANG DR

    IPC: B01J21/04 ,  B01J21/06 ,  B01J23/46 ,  B01J27/18 ,  C07B61/00 ,  C07C209/00 ,  C07C209/26 ,  C07C209/48 ,  C07C209/52 ,  C07C211/36

    Abstract: Process for the preparation of 3-aminomethyl-3,5,5-trimethylcyclohexylamine from 3-cyano-3,5,5-trimethylcyclohexanone by carrying out the following steps in two reaction spaces spatially separated from one another: a) reacting the 3-cyano-3,5,5-trimethylcyclohexanone in a first reaction space with excess ammonia over acid metal oxide catalysts at temperatures of 20 to 150 DEG C and pressures of 15 to 500 bar and b) hydrogenating the reaction products formed in a second reaction space with hydrogen in the presence of excess ammonia over cobalt-, nickel-, ruthenium- and/or other noble metal-containing catalysts which may contain basic components or are present on neutral or basic supports at temperatures of 60 to 150 DEG C and pressures of 50 to 300 bar.

    PREPARATION OF 2,2-DISUBSTITUTED PENTANE-1,5-DIAMINES
    4.
    发明专利
    PREPARATION OF 2,2-DISUBSTITUTED PENTANE-1,5-DIAMINES 未知

    公开(公告)号：CA2039326A1

    公开(公告)日：1991-10-01

    申请号：CA2039326

    申请日：1991-03-28

    Applicant: MERGER FRANZ ,  PRIESTER CLAUS ULRICH ,  WITZEL TOM ,  KOPPENHOEFER GERHARD ,  SCHUSTER LUDWIG ,  BASF AG

    Inventor： MERGER FRANZ ,  PRIESTER CLAUS-ULRICH ,  WITZEL TOM ,  KOPPENHOEFER GERHARD ,  SCHUSTER LUDWIG

    IPC: B01J23/40 ,  B01J23/74 ,  B01J29/06 ,  C07B61/00 ,  C07C209/48 ,  C07C211/09 ,  C08G69/00 ,  C08G73/02 ,  C08K5/17 ,  C08J3/24

    Abstract: A process for the preparation of a 2,2-disubstituted pentane-1,5-diamine of the formula I (see formula I) where R1 and R2, independently of one another, are C1- to C10-alkyl or C2- to C10-alkenyl or together are a C4- to C7- alkylene chain which is unsubstituted or monosubstituted to pentasubstituted by C1- to C4-alkyl, from a 2,2-di- substituted 4-cyanobutanal of the formula II (see formula II) where R1 and R2 are as defined above, comprises, in two spatially separate reaction spaces, a) reacting the 4-cyanobutanal of the formula II, in a first reaction space, with excess ammonia on an acidic heterogeneous catalyst at from 20 to 150.degree.C and at from 15 to 500 bar, and b) hydrogenating the resultant reaction product, in a second reaction space, using excess hydrogen in the presence of excess ammonia on a catalyst containing cobalt, nickel, ruthenium and/or another noble metal, if desired with a basic component or on a basic or neutral carrier, at from 60 to 150.degree.C and at from 50 to 500 bar. 2,2-Disubstituted pentane- 1,5-diamines of the formula I' (see formula III) where R1' and R2', independently of one another, are C1- to C10-alkyl or C2- to C10-alkenyl or together are a C4- to C7-alkylene chain which is unsubstituted or monosubstituted to pentasubstituted by C1-to C4-alkyl, with the proviso that R1' and R2' are not simultaneously methyl are also described.

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