公开(公告)号：WO03029784A2

公开(公告)日：2003-04-10

申请号：PCT/EP0210910

申请日：2002-09-27

Applicant: BASF AG ,  SCHROF WOLFGANG ,  MUELLER THORSTEN ,  KOLTZENBURG SEBASTIAN ,  KRONER MATTHIAS ,  LEHMANN STEPHAN ,  HADELER JOACHIM

Inventor： SCHROF WOLFGANG ,  MUELLER THORSTEN ,  KOLTZENBURG SEBASTIAN ,  KRONER MATTHIAS ,  LEHMANN STEPHAN ,  HADELER JOACHIM

IPC: G01N11/00 ,  G01N3/00 ,  G01N3/06 ,  G01N3/42

CPC classification number: G01N3/42 ,  G01N2203/0092 ,  G01N2203/0682

Abstract: The invention relates to a method for combined analysis of the hardening of hardenable liquid or viscous formulations, wherein (a) n hardenable formulations are provided in parallel in n containers, and (b) at least one degree of hardening is determined for each of the n formulations, wherein a measuring tip is inserted into the formulation with a determined amount of force and the maximum penetration depth thus obtained is taken as a measure of the degree of hardening of said formulations, and (c) one or several parameters characterizing the hardening kinetics are determined for a respective composition of the formulations from the measured values for the depths of penetration at various times after the production of the formulations . Preferably, steps (a) - (c) are carried out on several occasions and by analyzing the large number of individual values of the parameters characterizing the hardening characteristics thus obtained, it is possible to ascertain the dependency of the characteristic parameter(s) in relation to the composition of the formulations, whereupon the composition of the formulations can be optimized with regard to the hardening behavior thereof.

Abstract translation: 本发明涉及一种方法，用于在其中设置在平行于正固化配方可固化液体或粘性制剂的固化的组合研究ÑBehäitern的（a）和（b）固化的程度anjeder所述n制剂至少一次测定， 通过测量末端以一定的力刺穿制剂和达到制剂的固化度的最大穿透深度AIS度量被测量，和制备所述制剂的后（c）对于每个由用于在不同时间的穿透深度的测量值的制剂的组合物的 或固化参数的动力学的多个特征被确定第二十 根据所述步骤（a）（c）是优选进行多次，它是由这样获得的大量的一种或硬化参数的动力学特性的个体值的分析来确定是的函数，或制剂的组合物的特征参数 由此制剂的组合物可以相对于它们的固化行为进行优化。

公开(公告)号：DE10148567A1

公开(公告)日：2003-07-31

申请号：DE10148567

申请日：2001-10-01

Applicant: BASF AG

Inventor： SCHROF WOLFGANG ,  MUELLER THORSTEN ,  KOLTZENBURG SEBASTIAN ,  KRONER MATTHIAS ,  LEHMANN STEPHAN ,  HADELER JOACHIM

IPC: G01N11/00 ,  G01N3/00 ,  G01N3/06 ,  G01N3/42

Abstract: The invention relates to a process for the combinatorial investigation of the hardening of hardenable liquid or viscous formulations (a) in which n hardenable formulations are prepared in parallel in n containers, and (b) the degree of hardening is determined at least once on each of the n formulations by inserting a measurement tip into the formulation with a certain force and measuring the maximum penetration depth achieved as a measure of the degree of hardening of this formulation, and (c) for in each case one composition of the formulations, one or more parameters that are characteristic of the kinetics of hardening are determined from the measurement values for the penetration depth at various times after preparation of the formulations. Steps (a) to (c) are preferably carried out a number of times, and a dependence of the characteristic parameter(s) on the composition of the formulations is determined by analysis of the large number of individual values obtained in this way for the parameter(s) that is (are) characteristic of the kinetics of hardening, enabling the composition of the formulations to be optimized with respect to its hardening behavior.