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    DEVICE FOR THE MIXING, DRYING AND COATING OF POWDERED, GRANULAR OR MOULDED BULK MATERIAL IN A FLUID BED AND METHOD FOR PRODUCTION OF SUPPORTED CATALYSTS WITH SUCH A DEVICE
    2.
    发明申请
    DEVICE FOR THE MIXING, DRYING AND COATING OF POWDERED, GRANULAR OR MOULDED BULK MATERIAL IN A FLUID BED AND METHOD FOR PRODUCTION OF SUPPORTED CATALYSTS WITH SUCH A DEVICE 审中-公开
    装置进行搅拌，流化床和工艺干燥和涂敷粉末状，颗粒状或形状BULK生产负载型催化剂使用这种装置

    公开(公告)号：WO2005030380A2

    公开(公告)日：2005-04-07

    申请号：PCT/EP2004010748

    申请日：2004-09-24

    Applicant: BASF AG ,  NETO SAMUEL ,  RUMMEL WOLFGANG ,  STORCK SEBASTIAN ,  ZUEHLKE JUERGEN ,  ROSOWSKI FRANK

    Inventor： NETO SAMUEL ,  RUMMEL WOLFGANG ,  STORCK SEBASTIAN ,  ZUEHLKE JUERGEN ,  ROSOWSKI FRANK

    IPC: B01J2/16 ,  B01J8/18 ,  B01J23/00 ,  B01J23/22 ,  B01J27/199 ,  B01J35/02 ,  B01J37/02 ,  F26B3/08 ,  F26B3/092 ,  B01J

    CPC classification number: B01J23/002 ,  B01J2/16 ,  B01J23/22 ,  B01J27/199 ,  B01J35/023 ,  B01J37/0219 ,  B01J37/0221 ,  B01J37/0232 ,  B01J2523/00 ,  F26B3/0926 ,  B01J2523/15 ,  B01J2523/47 ,  B01J2523/51 ,  B01J2523/53 ,  B01J2523/55

    Abstract: The invention relates to a device for the mixing, drying and coating of powdered, granular or moulded bulk material in a fluid bed, in particular, a method for the production of supported catalysts for gas phase oxidations, with a container (10), for holding the bulk goods, whereby a dished recess (17) is provided in a lower region (13) of the container (10), a central tube (27) for the introduction of a gas, whereby the central tube enters in an upper region (12) of the container (10), extending essentially axially downwards into the container (10) and opens out in the recess (17), an essentially annular deflector screen (29), fixed to the central tube (27) in the upper region (12) of the container (10), a guide ring (31), arranged in the lower region (13) of the container (10), which surrounds the central tube (27) over a part of the length thereof essentially concentrically with a separation (L) such that a first passage (34) is formed between the wall of the container (10) at the upper edge of the recess and the lower end (33) of the guide ring (31) and a second outlet (36) is formed between the deflector screen (29) and the upper edge (35) of the guide ring (31) and means for introduction of a fluid into the container (10), such as, for example, nozzles (21). Said device is characterised in that the external wall of the central tube (27) is at least partly provided with a non-stick coating (38). In a preferred embodiment the separation (L) between the wall of the central tube (27) and the wall of the guide ring (27) is greater than the open height (H3) of the first passage (34). The invention further relates to a method for the production of supported catalysts using such a device.

    Abstract translation: 本发明涉及一种用于一过程混合，干燥和涂层的粉状，粒状或成形松散物料在流化床中，特别是用于气相氧化的负载型催化剂的制备方法，包括容器（10），用于接收散装材料，其中，（在其下部13 ）的容器（10）的具有用于供给气体，其中，所述中心管（在该容器的上部12）（10）进入所述容器中的碗状凹部（17）在前置式所看到的，中心管（27），位于所述 一个容器（10）基本上延伸轴向向下并进入凹槽（17）打开时，基本上环形的偏转防护罩（29）在容器（10）的上部区域（12）至所述中心管（27）是固定的， 布置成一个在所述容器的下部部分（13）的中心管（27）（10）导向环（31）在其长度的一部分基本上以一定距离（L），以便COLL同心 IBT，在凹部的上边缘（22）的容器（10）的壁和所述导向环（31），第一通路（34）的下端（33）（29）35之间以及Abweisschirrn之间和顶边（ ）所述导向环（31）的第二通道（36）的形成，以及用于将流体引入所述容器（10），例如喷嘴（21）。 本发明的装置的特征在于，所述中心管（27）的外壁至少部分地设置有减少附着的涂层（38）。 在一个优选的实施例中，中心管（27）和导向环（27）的所述壁的所述壁之间的距离（L）大于所述第一通道（34）的净高（H3）更大。 本发明还涉及一种使用这种装置的负载型催化剂的制备方法。

    Catalyst for gas phase oxidations
    4.
    发明专利
    Catalyst for gas phase oxidations 未知

    公开(公告)号：IN411CH2006A

    公开(公告)日：2007-07-06

    申请号：IN411CH2006

    申请日：2006-02-01

    Applicant: BASF AG

    Inventor： NETO SAMUEL ,  ZUEHLKE JUERGEN ,  STORCK SEBASTIAN ,  ROSOWSKI FRANK

    IPC: B01J21/06 ,  B01J23/22 ,  B01J27/198 ,  B01J37/02 ,  C07C51/265

    Abstract: A catalyst for gas-phase oxidations which comprises an inert support and a catalytically active composition comprising transition metal oxides applied thereto, or a precatalyst, is described. The (pre)catalyst is obtained by treating the inert support with an aqueous suspension or solution of the transition metal oxides or their precursor compounds, where the suspension contains a binder dispersion and the binder is a copolymer of an alpha-olefin and a vinyl-C 2 -C 4 -carboxylate whose vinyl C 2 -C 4 -carboxylate content is at least 62 mol %.

    6.
    发明专利
    未知

    公开(公告)号：AT360480T

    公开(公告)日：2007-05-15

    申请号：AT04763675

    申请日：2004-07-30

    Applicant: BASF AG

    Inventor： NETO SAMUEL ,  ZUEHLKE JUERGEN ,  STORCK SEBASTIAN ,  ROSOWSKI FRANK

    IPC: B01J21/06 ,  B01J23/22 ,  B01J27/198 ,  B01J37/02 ,  C07C51/265 ,  B01J31/06 ,  C07C51/215

    Abstract: A catalyst for gas-phase oxidations which comprises an inert support and a catalytically active composition comprising transition metal oxides applied thereto, or a precatalyst, is described. The (pre)catalyst is obtained by treating the inert support with an aqueous suspension or solution of the transition metal oxides or their precursor compounds, where the suspension contains a binder dispersion and the binder is a copolymer of an alpha-olefin and a vinyl-C 2 -C 4 -carboxylate whose vinyl C 2 -C 4 -carboxylate content is at least 62 mol %.

    7.
    发明专利
    未知

    公开(公告)号：BRPI0410759A

    公开(公告)日：2006-06-27

    申请号：BRPI0410759

    申请日：2004-05-21

    Applicant: BASF AG

    Inventor： ZUEHLKE JUERGEN ,  NETO SAMUEL ,  ROSOWSKI FRANK ,  STORCH SEBASTIAN

    IPC: C07C51/265 ,  C07C51/31 ,  C07C63/16

    Abstract: A description is given of a process for preparing aldehydes, carboxylic acids and/or carboxylic anhydrides, in particular phthalic anhydride, in which a gaseous stream comprising an aromatic hydrocarbon and molecular oxygen is passed at elevated temperature over a bed of a first catalyst and a bed which is made up of a second catalyst having a higher activity than the first catalyst and is located downstream of the first catalyst in the flow direction of the gaseous stream, wherein the catalytically active composition of the first catalyst comprises at least vanadium oxide, titanium dioxide and antimony oxide and the ratio of vanadium, calculated as V 2 O 5 , to antimony, calculated as Sb 2 O 3 , in the first catalyst is from 3.5:1 to 5:1. The source of antimony oxide used for the first catalyst is preferably particulate antimony trioxide having a mean particle size of from 0.5 to 5 mum. The process allows the desired oxidation products to be obtained in high yield over longer periods of time.

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