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    ELECTROCHEMICAL PRODUCTION OF LITHIUM
    1.
    发明专利
    ELECTROCHEMICAL PRODUCTION OF LITHIUM 失效

    公开(公告)号：JP2000290791A

    公开(公告)日：2000-10-17

    申请号：JP2000081115

    申请日：2000-03-23

    Applicant: BASF AG

    Inventor： SCHIERLE KERSTIN ,  PUETTER HERMANN ,  HUBER GUENTHER DIPL ING ,  SCHLAEFER DIETER DR ,  GUTH JOSEF

    IPC: C25C1/02 ,  C25C1/24 ,  C25C3/02

    Abstract: PROBLEM TO BE SOLVED: To provide an improving method as to an electrochemical production of metallic lithium high in energy efficiency. SOLUTION: By using a method consisting of a stage (I) in which lithium amalgam is produced from and aq. soln. of at least one kind of lithium salt and a stage (II) in which, using an anode contg. lithium amalgam, a solid electrolyte having lithium ion conductivity and a cathode of fused lithium, electrolysis is executed while the driving state of lithium amalgam as the anode is maintained, starting from the aq. soln. of at least one kind of lithium salt, metallic lithium is produced.

    METHOD FOR ELECTROCHEMICALLY MANUFACTURING ALKALI METAL FROM ALKALI METAL AMALGAM
    2.
    发明专利
    METHOD FOR ELECTROCHEMICALLY MANUFACTURING ALKALI METAL FROM ALKALI METAL AMALGAM 失效

    公开(公告)号：JP2000219989A

    公开(公告)日：2000-08-08

    申请号：JP37660199

    申请日：1999-12-15

    Applicant: BASF AG

    Inventor： HUBER GUENTHER DIPL ING ,  PUETTER HERMANN ,  SCHIERLE A KERSTIN ,  SCHLAEFER DIETER DR ,  GUTH JOSEF ,  SCHUBE BERND ,  LENZ DIETHARD

    IPC: C22B26/00 ,  C25C1/20 ,  C25C3/02

    Abstract: PROBLEM TO BE SOLVED: To reduce the energy consumption in the manufacture by maintaining the dynamic condition of an alkali metal amalgam forming an anode. SOLUTION: A liquid anode preferably maintains its dynamic condition by the stirring under the atmospheric pressure or the pressure slightly higher than the atmospheric pressure, or the circulation by a pump, or the combination thereof. An anode area and a cathode area are separated from each other by a solid electrolyte which is an alkali metal ion conductor through which helium is impermeable. For example, appropriate solid electrolytes in manufacturing sodium include sodium β"-alumina, and sodium p-alumina. The manufacturing temperature is preferably 310-400 deg.C for sodium, and 260-400 deg.C for potassium. The current density during the manufacture is generally >=250 A/m2, but preferably 0.5-10 kA/m2 for sodium, and 0.3-3 kA/m2 for potassium.

    ELECTROLYTIC CELL FOR PRODUCING ALKALI METAL
    3.
    发明专利
    ELECTROLYTIC CELL FOR PRODUCING ALKALI METAL 失效

    公开(公告)号：JP2001059196A

    公开(公告)日：2001-03-06

    申请号：JP2000172849

    申请日：2000-06-09

    Applicant: BASF AG

    Inventor： HUBER GUENTHER DIPL ING ,  PUETTER HERMANN ,  SCHIERLE A KERSTIN ,  SCHLAEFER DIETER DR ,  GUTH JOSEF

    IPC: C25B1/36 ,  C25C3/02 ,  C25C7/00 ,  C25C7/02 ,  C25C7/04 ,  C25D1/14

    Abstract: PROBLEM TO BE SOLVED: To energically preferably produce sodium and potassium. SOLUTION: This electrolytic cell being a stirred state comprises an alkali metal amalgam-contg. anode, a solid electrolyte having alkali metal ion conductivity and a cathode. The solid electrolyte and the cathode are mutually divided through an electrolytic soln. As the electyrolyte, dissolved NaOH, NaNH2 or a mixture thereof, or dissolved KOH, KNH2 or a mixture of is used, and the solid electrolyte can be selected from the group consisting of sodium β-alumina, sodium β"-alumina and β/β"-alumina or the group consisting of potassium β-alumina, potassium β" and potassium β/β"-alumina.

    PROCESS FOR PREPARING POROUS METAL ORGANIC FRAMEWORKS
    5.
    发明申请
    PROCESS FOR PREPARING POROUS METAL ORGANIC FRAMEWORKS 审中-公开
    用于生产多孔金属有机骨架

    公开(公告)号：WO2007131948A3

    公开(公告)日：2008-02-07

    申请号：PCT/EP2007054554

    申请日：2007-05-11

    Applicant: BASF AG ,  PUETTER HERMANN ,  SCHUBERT MARKUS ,  RICHTER INGO ,  MUELLER ULRICH ,  TRUKHAN NATALIA

    Inventor： PUETTER HERMANN ,  SCHUBERT MARKUS ,  RICHTER INGO ,  MUELLER ULRICH ,  TRUKHAN NATALIA

    IPC: C25B3/12

    CPC classification number: C25B3/12

    Abstract: The present invention relates to a process for preparing a porous metal organic framework comprising at least two organic compounds coordinated to at least one metal ion, which comprises the steps (a) oxidation of at least one anode containing metal corresponding to the at least one metal ion in a reaction medium in the presence of at least a first organic compound, where the first organic compound is an optionally substituted monocyclic, bicyclic or polycyclic saturated or unsaturated hydrocarbon in which at least two ring carbons are replaced by heteroatoms selected from the group consisting of N, O and S, to form a reaction intermediate containing at least one metal ion and the first organic compound; and (b) reaction of the reaction intermediate at a prescribed temperature with an at least second organic compound which coordinates to the at least one metal ion, where the second organic compound is derived from a dicarboxylic, tricarboxylic or tetracarboxylic acid.

    Abstract translation: 本发明涉及一种用于制备包含配位的至少两个的至少一种金属有机化合物，包括（a）氧化中的至少一种的存在下相应的含有金属的阳极中的反应介质中的至少一种金属离子的至少之一中的步骤的多孔金属有机骨架 第一有机化合物，其中所述第一有机化合物和任选取代的单 - ，双 - 或多环饱和或未饱和烃基，其中至少两个环碳原子被选自下组的杂原子取代由选自N，O和S的取代， 形成所述至少一个金属离子和第一含有机化合物的中间体反应产物; 和（b）反应，该反应与至少其协调结合到所述至少一种金属离子，其中，二，三或四羧酸的第二有机化合物导出的第二有机化合物中间体在设定温度。

    ELECTROCHEMICAL ALKOXYLATING OXIDATIVE CARBON-CARBON BOND CLEAVAGE IN 1,2-DIPHENYLETHANE AND DERIVATIVES THEREOF ON A DIAMOND ELECTRODE
    8.
    发明申请
    ELECTROCHEMICAL ALKOXYLATING OXIDATIVE CARBON-CARBON BOND CLEAVAGE IN 1,2-DIPHENYLETHANE AND DERIVATIVES THEREOF ON A DIAMOND ELECTRODE 审中-公开
    电化学氧化的烷氧基化炭键裂解AM 1,2-二苯基乙烷及其衍生物AT的金刚石电极

    公开(公告)号：WO2005066390A3

    公开(公告)日：2005-09-22

    申请号：PCT/EP2005000085

    申请日：2005-01-07

    Applicant: BASF AG ,  GRIESBACH ULRICH ,  PUETTER HERMANN ,  ZOLLINGER DANIEL

    Inventor： GRIESBACH ULRICH ,  PUETTER HERMANN ,  ZOLLINGER DANIEL

    IPC: C25B3/02

    CPC classification number: C25B3/02

    Abstract: The invention relates to a method for the electrolytic oxidative alkoxylating cleavage of 1,2-diarylethane derivatives by electrolytically oxidizing the respective 1,2-diarylethane derivative in a solvent containing the alcohol required for alkoxylation, electrolytic oxidation being performed on a diamond electrode. The inventive method makes it possible to especially produce diaryl derivatives when a 1,2-diarylethane derivative in which the two aryl radicals are directly bonded to each other is used as a substrate.

    Abstract translation: 本发明涉及一种用于通过在含有必需的烷氧基化醇，其中所述电解氧化在金刚石电极进行溶剂中的相应的1,2- Diarylethanderivats的电解氧化烷氧基化1,2- Diarylethanderivaten的电解氧化裂解 ， 特别是本发明的方法允许联芳基衍生物的制备中，当1,2- Diarylethanderivat被用作衬底，其中，所述两个芳基直接连接到彼此。

    ANODIC DIMERISATION OF SUBSTITUTED BENZOLS
    9.
    发明申请
    ANODIC DIMERISATION OF SUBSTITUTED BENZOLS 审中-公开
    阳极二聚取代苯

    公开(公告)号：WO2005075709A2

    公开(公告)日：2005-08-18

    申请号：PCT/EP2005001066

    申请日：2005-02-03

    Applicant: BASF AG ,  ROMMEL CHRISTINA E ,  MALKOWSKY ITAMAR ,  WALDVOGEL SIEGFRIED ,  PUETTER HERMANN ,  GRIESBACH ULRICH

    Inventor： ROMMEL CHRISTINA E ,  MALKOWSKY ITAMAR ,  WALDVOGEL SIEGFRIED ,  PUETTER HERMANN ,  GRIESBACH ULRICH

    IPC: C25B3/10

    CPC classification number: C25B3/10

    Abstract: The invention relates to a method for producing biarylalcohols by means of the electrodimerisation of arylalcohols, said method comprising the following steps: a) an aryloxy compound of the alcohol to be coupled is produced with an element from the group B and Al; b) the aryloxy compounds obtained in a) are electrolytically oxidised and coupled to form the corresponding biaryl derivatives; and c) the desired biaryl alcohols are released. The inventive method enables the dimerisation of arylalcohols with a high degree of selectivity in order to obtain an ortho product.

    Abstract translation: 本发明描述了通过包括以下步骤的芳基醇的electrodimerization为Biarylalkoholen的制备方法：a）制备醇的芳氧基化合物被加上从B组和Al的元素; B）电解氧化，并在获得的Arylloxyverbindungen的耦合），得到相应的二芳基衍生物; c）中释放期望的Biarylalkohole。 本发明的方法使得能够芳基醇的二聚化具有高选择性的邻位产物。

    METHOD FOR PRODUCING ALCOXYLATED CARBONYL COMPOUNDS BY AN ANODIC OXIDATION METHOD USING A CATHODIC COUPLED REACTION FOR ORGANIC SYNTHESIS
    10.
    发明申请
    METHOD FOR PRODUCING ALCOXYLATED CARBONYL COMPOUNDS BY AN ANODIC OXIDATION METHOD USING A CATHODIC COUPLED REACTION FOR ORGANIC SYNTHESIS 审中-公开
    PROCESS FOR烷氧基化由阳极氧化法UNDER阴极KOPPEL反应在有机合成中使用的制备羰基

    公开(公告)号：WO0242524A2

    公开(公告)日：2002-05-30

    申请号：PCT/EP0113587

    申请日：2001-11-22

    Applicant: BASF AG ,  PUETTER HERMANN ,  FISCHER ANDREAS

    Inventor： PUETTER HERMANN ,  FISCHER ANDREAS

    IPC: C25B3/02 ,  C25B3/00

    CPC classification number: C25B3/00

    Abstract: A method for producing alcoxylated carbonyl compounds of general formula (I) (compounds I): R aR C(OR )b wherein R , R represent hydrogen or C1- C6-alkyl, R independently means C1- C6-alkyl, a is 0 or 1, b 2 or 3 with the proviso that the sum of a and b is 3, by means of anodic oxidation of germinal dialcoxy compounds of general formula (II) (compounds II) wherein R , R , R , R represent hydrogen or C1- C6-alkyl, R , R represent C1- C6-alkyl or C1- C6-alcoxy, in the presence of a C1-C6-alkyl alcohol (compounds III).A usual compound (compound IV) is used as a cathodic depolarizer suitable for electrochemical oxidation. The anodic oxidation and cathodic reduction is carried out in an undivided electrolyte cell in the presence of C1-C6-alkyl alcohols.

    Abstract translation: 一种生产通式（I）的烷氧基​​化的羰基化合物的方法（I化合物）：R <1> AR <2> C（OR <3>）b式中[R <1>，R <2>是氢或C 1 -C -C 6 - 烷基，R <3>彼此独立地C1-C6烷基，a是0或1，b 2或3，条件是a和b的总和为3，由通式的偕二烷氧基化合物的阳极氧化 （II）（化合物II），其中R <4>，R <5> - [R <6> - [R <7>是氢或C1-C6烷基，R <5> - [R <6>的C1至C6 在C1的存在下C6烷基醇或烷基C1至C6烷氧基（化合物III），被用作消偏振镜一个常规有机化合物（化合物IV）阴极，其适合用于电化学氧化和得到 阳极氧化和在未分割的电解槽的阴极还原在C1-C6烷基醇执行的存在。

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