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    METHOD FOR PRODUCING M-SUBSTITUTED PHENYLALKANOLS BY MEANS OF ISOMERIZATION
    1.
    发明申请
    METHOD FOR PRODUCING M-SUBSTITUTED PHENYLALKANOLS BY MEANS OF ISOMERIZATION 审中-公开
    用于生产M-取代的苯基链烷醇异构化

    公开(公告)号：WO2011048068A3

    公开(公告)日：2011-07-07

    申请号：PCT/EP2010065673

    申请日：2010-10-19

    Applicant: BASF SE ,  LANVER ANDREAS ,  EBEL KLAUS ,  BECK KARL ,  PELZER RALF ,  BOTZEM JOERG ,  GRIESBACH ULRICH

    Inventor： LANVER ANDREAS ,  EBEL KLAUS ,  BECK KARL ,  PELZER RALF ,  BOTZEM JOERG ,  GRIESBACH ULRICH

    IPC: C07C29/56 ,  C07C33/20 ,  C07C45/29 ,  C07C47/228 ,  C11B9/00

    CPC classification number: C07C29/56 ,  C07C45/29 ,  C11B9/0061 ,  C07C33/20 ,  C07C47/228

    Abstract: The invention relates to a method for producing m-substituted phenylalkanols of the formula (I), R1 denoting C1-C5-alkyl, and R2, R3, R4, and R5 independently denoting hydrogen or methyl, characterized in that a p-substituted phenylalkanol of the formula (II), where R1, R2, R3, R4, and R5 have the meanings given under formula (I), is isomerized in the presence of a Friedel-Craft catalyst to form an m-substituted phenylalkanol of the formula (I). The corresponding aldehydes known as fragrances and aroma chemicals can be formed as valuable products from the m-substituted phenylalkanols of the formula (I) by means of oxidation or dehydration.

    Abstract translation: 本发明涉及一种制备式（I）其中R1是C1-C5烷基，和表示R2，R3，R4和R5独立地是氢或甲基，m的取代的苯基链烷醇，其包括的p反应 式的取代的苯基链烷醇，其中R1，R2，R3，R4和R5如式表示（I）（II）定义，在Friedel-Crafts催化剂的存在下，形成式（I）的间位取代苯基链烷醇被异构化。 从式（I）的间位取代苯基链烷醇可以是由值作为形成相应的醛，其已知为香料和调味化学品氧化或脱氢产物。

    METHOD FOR PRODUCING ALIPHATIC ALDEHYDES
    3.
    发明申请
    METHOD FOR PRODUCING ALIPHATIC ALDEHYDES 审中-公开
    用于生产脂肪醛

    公开(公告)号：WO2011067386A2

    公开(公告)日：2011-06-09

    申请号：PCT/EP2010068865

    申请日：2010-12-03

    Applicant: BASF SE ,  BOTZEM JOERG ,  LANVER ANDREAS ,  EBEL KLAUS ,  BECK KARL ,  GRIESBACH ULRICH ,  PELZER RALF ,  SORG ACHIM ,  POLLMER NADJA

    Inventor： BOTZEM JOERG ,  LANVER ANDREAS ,  EBEL KLAUS ,  BECK KARL ,  GRIESBACH ULRICH ,  PELZER RALF ,  SORG ACHIM ,  POLLMER NADJA

    IPC: C07C45/74

    CPC classification number: C07C45/62 ,  C07C45/74 ,  C11B9/0015 ,  C07C47/02 ,  C07C47/21

    Abstract: The invention relates to a method for producing aliphatic aldehydes of the general formula (I) by reacting aldehyde of the general formula (II) with an aldehyde of the general formula (III), where R1 is hydrogen or a methyl group, R2 is a straight-chain or branched alkyl radical having 1 to 4 carbon atoms, and the two X are each hydrogen or together are a further C-C bond, in the presence of an aldol condensation catalyst to form the substituted octenal of the general formula (I) and subsequently optionally hydration, either continuously or in batches, to form the corresponding octanal of the formula (I). The invention is characterized in that the aldehydes of the general formula III and II are used in a molar ratio of III:II between 1.4:1 and 0.6:1.

    Abstract translation: 一种通式（I）的脂族醛的制备方法中，通过与通式（III）其中R 1是氢或甲基的醛通式（II）的醛的反应中，R 2是直链或支链烷基基团，具有 为1至4个碳原子和两个X各自为氢或一起是另一CC-键，在醇醛缩合催化剂的式（I）的取代的辛烯醛的存在下，然后任选连续或间歇氢化，得到相应的辛醛 式（I），其特征在于，在III和III II的摩尔比的通式的醛：1的使用，从1.4 II之间：和0.6 1。

    ELECTROCHEMICAL PRODUCTION OF STERICALLY HINDERED AMINES
    4.
    发明申请
    ELECTROCHEMICAL PRODUCTION OF STERICALLY HINDERED AMINES 审中-公开
    电化学方法生产受阻胺

    公开(公告)号：WO2008003620A3

    公开(公告)日：2009-05-14

    申请号：PCT/EP2007056390

    申请日：2007-06-27

    Applicant: BASF SE ,  GRIESBACH ULRICH ,  WALDVOGEL SIEGFRIED R ,  MALKOWSKY ITAMAR ,  KULISCH JOERG

    Inventor： GRIESBACH ULRICH ,  WALDVOGEL SIEGFRIED R ,  MALKOWSKY ITAMAR ,  KULISCH JOERG

    IPC: C25B3/04 ,  C07C209/30

    CPC classification number: C25B3/04 ,  C07C209/30 ,  C07C2601/14 ,  C07C211/35 ,  C07C211/40

    Abstract: The invention relates to a method for producing an amine, comprising the step of cathodic reduction of a corresponding oxime derivative of general formula (I), wherein R represents C1-6 alkyl or C2-6 alkenyl, which is optionally substituted with one or more substituents independently selected from the group consisting of phenyl, O-C1-6 alkyl, NH-C1-6 alkyl, N(C1-6 alkyl)2, OH and NH2; R1 represents H; C1-6 alkyl or C(O)-C1-6 alkyl and A represents a 5-, 6- or 7-membered hydrocarbon ring which is saturated or which has a double bond and wherein optionally at least one CH2 group is replaced by -O-, -S- -NH-, -N=, or -N(C1-6 alkyl)- and which is optionally substituted with one or more other substituents independently selected from the group consisting of phenyl, C1-6 alkyl, O-C1-6 alkyl, NH-C1-6-alkyl, N(C1-6 alkyl)2, OH and NH2; and the oxime derivative, with respect to the carbon ring having the substituent R, having an excess of the R or S form of at least 10 %.

    Abstract translation: 一种含有通式（I）其中R是C 1-6烷基或C 2-6烯基任选被一个或多个Substi取代的相应的肟衍生物的阴极还原的胺的制备方法tuenten从基独立地选自由苯基，O-C1 是1-6烷基，NH-C 1-6烷基，N（C 1-6烷基）2，OH和NH 2基团; R1 H; C 1-6烷基或C（O）-C 1-6烷基，和A是5-，6-或7-元烃其为饱和环或具有双键，并且其中被-O - 任选地至少一种CH 2基团 ， - S - NH - ， - N =，或-N（C 1-6烷基） - 已被取代，并任选地用选自苯基，C 1-6烷基，O-C基团独立地选择的一个或多个另外的取代基取代 是1-6烷基，NH-C 1-6烷基，N（C 1-6烷基）2，OH和NH 2基团; 且其中相对于具有取代基R的碳环，所述肟衍生物具有过量的至少10％的R或S形式的。

    8.
    发明专利
    未知

    公开(公告)号：AT493522T

    公开(公告)日：2011-01-15

    申请号：AT07786853

    申请日：2007-06-27

    Applicant: BASF SE

    Inventor： GRIESBACH ULRICH ,  WALDVOGEL SIEGFRIED R ,  KULISCH JOERG ,  MALKOWSKY ITAMAR

    IPC: C25B3/25

    Abstract: The present invention relates to a process for preparing an amine, which comprises the step cathodic reduction of a corresponding oxime derivative of the general formula (I) where R is C1-6-alkyl or C2-6-alkenyl which is optionally substituted by one or more substituents selected independently from the group consisting of phenyl, O—C1-6-alkyl, NH—C1-6-alkyl, N(C1-6-alkyl)2, OH and NH2; R1 is H; C1-6-alkyl or C(O)—C1-6-alkyl and A is a 5-, 6- or 7-membered hydrocarbon ring which is saturated or has a double bond and in which at least one CH2 group may, if appropriate, be replaced by —O—, —S——NH—, —N═ or —N(C1-6-alkyl)- and which may optionally be substituted by one or more further substituents selected independently from the group consisting of phenyl, C1-6-alkyl, O—C1-6-alkyl, NH—C1-6-alkyl, N(C1-6-alkyl)2, OH and NH2; wherein, based on the ring carbon bearing the substituent R, the oxime derivative has an excess of the R or S form of at least 10%.

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