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公开(公告)号：JP2010018629A
公开(公告)日：2010-01-28
申请号：JP2009236899
申请日：2009-10-14
Applicant: Basf Se , ビーエーエスエフ ソシエタス・ヨーロピアBasf Se
Inventor： GENGER THOMAS , OOST CARSTEN , SNOECK JOOST-WILLEM , STROEZEL MANFRED , BECKER JENS , BERNING WILFRIED
IPC: C07C27/12 , B01D3/00 , B01D3/34 , B01J10/00 , B01J19/00 , C07B61/00 , C07C29/50 , C07C35/08 , C07C45/33 , C07C45/34 , C07C45/35 , C07C45/36 , C07C49/403 , C07C51/215 , C07C51/25 , C07C51/265 , C07C407/00 , C07C409/14 , C07C409/16
CPC classification number: C07C51/252 , B01J2219/00103 , B01J2219/00108 , B01J2219/0011 , C07C29/50 , C07C45/33 , C07C45/34 , C07C45/35 , C07C45/36 , C07C51/215 , C07C51/265 , C07C407/00 , C07C409/14 , C07C2601/14 , Y02P20/582 , C07C49/04 , C07C49/403 , C07C47/22 , C07C35/08
Abstract: PROBLEM TO BE SOLVED: To provide a method for easily oxidizing a starting material, particularly an organic starting material, using an oxidant so as to obtain a product by a technically easy, economical method.
SOLUTION: The method for obtaining a product mixture containing cyclohexanol and cyclohexanone by oxidizing cyclohexane using an oxidant comprises a step of carrying out oxidation in a rectifying column, which has a bottom region at its lower end, a top region at its upper end and a reaction zone between the top and bottom regions and has a separation performance of 10-100 in terms of the number of theoretical plates, a step of maintaining the reaction mixture in a boiling state in the reaction zone, and a step of introducing the oxidant into the reaction zone in at least two sub-streams. Here, the oxidation is carried out under a condition wherein the average retention time of a reaction mixture on each plate of the column is 1-120 min and the number of theoretical plates in the upper region of the rectifying column is 5-50.
COPYRIGHT: (C)2010,JPO&INPITAbstract translation: 要解决的问题：提供一种使用氧化剂容易地氧化原料，特别是有机原料的方法，以便通过技术上容易和经济的方法获得产物。 解决方案：使用氧化剂通过氧化环己烷获得含有环己醇和环己酮的产物混合物的方法包括在精馏塔中进行氧化的步骤，该精馏塔在其下端具有底部区域，在其上部具有顶部区域 末端和顶部和底部区域之间的反应区域，并且根据理论塔板数量具有10-100的分离性能，将反应混合物保持在反应区域中的沸腾状态的步骤，以及引入步骤 氧化剂在至少两个子流中进入反应区。 这里，在塔的每个板上的反应混合物的平均保留时间为1-120分钟，精馏塔上部区域的理论塔板数为5-50的条件下进行氧化。 版权所有（C）2010，JPO＆INPIT
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公开(公告)号：DE102008009992A1
公开(公告)日：2009-08-20
申请号：DE102008009992
申请日：2008-02-19
Applicant: BASF SE
Inventor： JAWOREK THOMAS , MILLER CHRISTIAN , STROEZEL MANFRED , ACHHAMMER GUENTHER , PAPKALLA THOMAS , BERNING WILFRIED
IPC: C07C51/245 , C07C51/44 , C07C55/02 , C07C55/14
Abstract: Process for producing dicarboxylic acid, comprises oxidation of cycloaliphatic alcohols and/or cycloaliphatic ketone with nitric acid, where the reaction and the separation of the components are carried out in a fractionating-, reaction-, and/or rectification-column.
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公开(公告)号：BRPI0719676A2
公开(公告)日：2013-12-24
申请号：BRPI0719676
申请日：2007-11-30
Applicant: BASF SE
Inventor： OOST CARSTEN , ROHDE WOLFGANG , MILLER CHRISTIAN , STROEZEL MANFRED , THOME ALFRED , BERNING WILFRIED
Abstract: A process is proposed for reprocessing the exhaust gas from a plant for producing hydroxylamine or hydroxylammonium salts by catalytic reduction of nitrogen monoxide with hydrogen for the purpose of utilization of at least a part of the nitrogen monoxide and if appropriate hydrogen present in the exhaust gas for producing hydroxylamine or hydroxylammonium salts, which comprises, in a first separation stage, selectively separating off nitrogen monoxide from the exhaust gas of the plant for producing hydroxylamine or hydroxylammonium salts.
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公开(公告)号：DE102007050713A1
公开(公告)日：2009-04-23
申请号：DE102007050713
申请日：2007-10-22
Applicant: BASF SE
Inventor： JAWOREK THOMAS , MILLER CHRISTIAN , STROEZEL MANFRED , ACHHAMMER GUENTHER , PAPKALLA THOMAS , BERNING WILFRIED
Abstract: Process for producing dicarboxylic acid comprises oxidation of cycloaliphatic alcohols and/or cycloaliphatic ketone with nitric acid, where the reaction and the separation of the components are carried out in a fractionating-, reaction-, and/or rectification-column.
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