Abstract:
PROBLEM TO BE SOLVED: To improve a method of purifying a raw melt of at least one monomer by crystallization. SOLUTION: There is provided the method for the purification of a crude melt of at least one monomer by crystallization, in which the crude melt to be purified is subjected to a suspension crystallization, the monomer crystals produced during the suspension crystallization and suspended in the residual melt are separated from the residual melt by using a first mechanical separation operation and, in at least one further crystallization stage, the residual melt remaining after the first mechanical separation operation and/or the monomer crystals which have been separated off and if necessary washed are further purified after they have been melted, wherein the residual melt and/or the remelted monomer crystals are subjected to at least one further mechanical solid/liquid separation operation on their way into the one or more further crystallization stages. COPYRIGHT: (C)2010,JPO&INPIT
Abstract:
The invention describes a process for the isolation of pure N-vinylpyrrolidone from N-vinylpyrrolidone-containing crude products, comprising a single-stage or multistage crystallization process, which comprises passing the mother liquor from the first crystallization stage either to a distillative and/or extractive purification, or returning it to an N-vinylpyrrolidone-containing product stream of the preparation process.
Abstract:
Method for extracting alcoholate through crystallization from the corresponding alcohol solution comprises crystallizing alcoholate at an absolute pressure of at least 3 bar and a temperature of at least 120[deg]C.
Abstract:
Disclosed is an absorbent for eliminating carbon dioxide from gas flows. Said absorbent contains an aqueous solution of an amine of formula (I) HNR2, wherein one or both radicals R represent (II) while the other radical R represents hydrogen. The inventive absorbent is characterized by particularly great resistance to oxidation.