公开(公告)号：PL3041801T3

公开(公告)日：2022-09-12

申请号：PL14772004

申请日：2014-09-04

Applicant: CORNING INC

Inventor： HARPER BRIAN LEE ,  KHRAPKO ROSTISLAV RADIYEVICH ,  MISHRA SNIGDHARAJ KUMAR ,  RANEY SONYA MARIE ,  TANDON PUSHKAR

IPC: C03C13/04 ,  C03B37/014 ,  C03B37/018

公开(公告)号：WO2015034991A3

公开(公告)日：2015-04-30

申请号：PCT/US2014054001

申请日：2014-09-04

Applicant: CORNING INC

Inventor： HARPER BRIAN LEE ,  KHRAPKO ROSTISLAV RADIYEVICH ,  MISHRA SNIGDHARAJ KUMAR ,  RANEY SONYA MARIE ,  TANDON PUSHKAR

IPC: C03C13/04 ,  C03B37/014 ,  C03B37/018

CPC classification number: C03B37/01446 ,  C03B37/014 ,  C03B37/01453 ,  C03B2201/08 ,  C03B2201/12 ,  C03B2201/20 ,  C03B2201/31 ,  C03B2203/22 ,  C03B2203/23 ,  C03B2203/26 ,  C03C13/045 ,  C03C2201/11 ,  C03C2201/20

Abstract: One embodiment of the disclosure relates to a method of making an optical fiber comprising the steps of: (i) exposing a silica based preform with at least one porous glass region having soot density of r to a gas mixture comprising SiCl4 having SiCl4 mole fraction ySiCl4 (preferably of less than 0.03) at a doping temperature Tdop such that parameter X is larger than 0.03 to form the chlorine treated preform, wherein X is defined as a function of density r, doping temperature Tdop, SiCl4 mole fraction ySiCl4, and the density ps of the fully densified soot layer; and (ii) exposing the chlorine treated preform to temperatures above 1400 °C to completely sinter the preform to produce sintered optical fiber preform with a chlorine doped region; and (iii) drawing an optical fiber from the sintered optical preform.

Abstract translation: 本公开的一个实施方案涉及制造光纤的方法，其包括以下步骤：（i）将具有至少一个具有烟灰密度为r的多孔玻璃区域的二氧化硅基预成型件暴露于包含SiCl4的气体混合物，所述SiCl4具有SiCl4摩尔分数ySiCl4 （优选小于0.03），使得参数X大于0.03以形成经氯处理的预成型物，其中X被定义为密度r，掺杂温度T dop，SiCl 4摩尔分数y SiCl 4和密度 ps的完全致密的烟灰层; 和（ii）将氯处理的预成型件暴露于1400℃以上的温度以完全烧结预成型件以生产具有氯掺杂区域的烧结光纤预成型件; 和（iii）从烧结光学预制棒拉制光纤。