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公开(公告)号:YU33707B
公开(公告)日:1978-02-28
申请号:YU246370
申请日:1970-10-07
Applicant: DEGUSSA
Inventor: HANS PFLEGER , PFLEGER HANS , FRIEDRICH BITTNER , BITTNER FRIEDRICH , PAUL MEFFERT , MEFFERT PAUL
IPC: C01C3/20 , C07C161/02
Abstract: Alkali thiocyanates are prepared by reacting alkali cyanides with sulfur in the presence of alkali sulfide in a molar amount of 1:1000 to 1:2000 as a solubilizer for the sulfur. The reaction is carried out above the melting point of sulfur, preferably in an alkali thiocyanate solution. The alkali sulfide is then converted to the sulfate by oxidation with hydrogen peroxide.
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公开(公告)号:YU246370A
公开(公告)日:1977-08-31
申请号:YU246370
申请日:1970-10-07
Applicant: DEGUSSA
Inventor: PFLEGER HANS , HANS PFLEGER , BITTNER FRIEDRICH , FRIEDRICH BITTNER , MEFFERT PAUL , PAUL MEFFERT
IPC: C01C3/20 , C07C161/02
Abstract: Alkali thiocyanates are prepared by reacting alkali cyanides with sulfur in the presence of alkali sulfide in a molar amount of 1:1000 to 1:2000 as a solubilizer for the sulfur. The reaction is carried out above the melting point of sulfur, preferably in an alkali thiocyanate solution. The alkali sulfide is then converted to the sulfate by oxidation with hydrogen peroxide.
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