2.
    发明专利
    未知

    公开(公告)号:DE59602429D1

    公开(公告)日:1999-08-19

    申请号:DE59602429

    申请日:1996-05-25

    Applicant: DEGUSSA

    Abstract: Precipitated silicic acid has a BET surface area of 100-130m /g (DIN 66131); a DBP absorption (water-free (DIN53601) ASTM D244 of plus or minus 275g/100g, a dry loss (2 hrs./105 degrees C) of 3.5-5.5 wt.% (DIN ISO787/11,ASTM D280, JISK5101/21), and a sieve residue with ALPINE air sieve of plus or minus 10;0 wt.% (

    10.
    发明专利
    未知

    公开(公告)号:DE2651446A1

    公开(公告)日:1978-05-24

    申请号:DE2651446

    申请日:1976-11-11

    Applicant: DEGUSSA

    Abstract: Silicon dioxide containing waste flue dust from the producton of silicon metal and silicon alloys is converted to crystalline zeolite molecular sieves of Type Y by (1) dissolving the flue dust in alkali metal hydroxide solution with the formation of alkali metal silicate solution having the module (SiO2:MeI2O) in the range of 4.0:1 to 5.0:1 at a temperature of 60 DEG -110 DEG C.; (2) purifying the thus obtained alkali metal silicate solution from organic constituents by treatment with activated carbon and/or an oxidizing agent and separating the non-decomposable residue from the solution; and (3) reacting alkali metal aluminate solution present at room temperature with the diluted, purified alkali metal silicate solution with a module (SiO2:MeI2O) of 4.0:1 to 5.0:1 obtained by steps (1) and (2) and subsequently crystallizing the reaction mixture (SiO2:Al2O3=4-7:1, MeI2O:SiO2=0.4-0.7, H2O:MeI2O=30-50:1) at a temperature of 75 DEG -100 DEG C. with stirring for a period of 8-48 hours, subsequently filtering to remove the product from the mother liquor, washing and drying to recover a zeolite molecular sieve of Type Y with a Faujasite structure having a degree of whiteness according to Berger (A. Berger, Die Farbe, 8 Nr. 4/6 (1959) 187-202) at 460 mu in the range of 90-95%.

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