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    Process for the manufacture of alkane phosphonic acid diesters
    2.
    发明授权
    Process for the manufacture of alkane phosphonic acid diesters 失效
    碱性磷酸钙制品的制备方法

    公开(公告)号：US3812222A

    公开(公告)日：1974-05-21

    申请号：US9805270

    申请日：1970-12-14

    Applicant: HOECHST AG

    Inventor： KLEINER H ,  RITTNER S

    IPC: C07F9/38 ,  C07F9/40

    CPC classification number: C07F9/3808 ,  C07F9/4006

    Abstract: The known production of alkane phosphonic acid diesters from olefins and dialkylphosphites in the presence of free radical generators is improved by using Alpha -olefins having an extremely low content of sulfur. Thus high yields and pure products are obtained within short reaction times. The known products are foam depressants, anticorrosives, oiladditives, dyeing adjuvants and organic intermediates, expecially for plant protecting agents.

    Antistatic thermoplastic moulding compositions
    3.
    发明授权
    Antistatic thermoplastic moulding compositions 失效
    防静电热塑性成型组合物

    公开(公告)号：US3709852A

    公开(公告)日：1973-01-09

    申请号：US3709852D

    申请日：1971-03-09

    Applicant: HOECHST AG

    Inventor： VAN SPANKEREN U ,  GORDON W ,  KLEINER H

    IPC: C08K5/5397 ,  C08F15/00 ,  C08F45/00

    CPC classification number: C08K5/5397 ,  Y10S260/16 ,  Y10S524/912

    Abstract: THEERMOPLASTIC MOULDING COMPOSITIONS FOT THE MAKING OF ANTISTATIC SHAPED ARTICLES ARE DISCLOSEED. COMPOUNDS OF THE FORMULA

    R1-P(=O)-R2(-R3)

    WHEREIN R1 IS AN ALKYL RADICAL OF 8 TO 24 CARBON ATOMS AND R2 AND R3 ARE ALLKYL RADICALS OF 1 TO 3 CARBON ATOMS HAVE PROVED TO BE ESPECIALLY EFFICIENT ANTISTATIC AGENTS, PARTICULARLY IN VIEW OF THEIR ADVANTAGEOUS TOXICOLOGICAL PROPERTIES AMD OF THE FACT THAT OTHER FAVOURABLE PROPERTIES OF HE PLASTIC MATERIALS, IN WHICH THEY ARE CONTAINED, ARE NOT ADVERSELY AFECTED.

    (hydroxy or alkanoyloxy alkylene)dihydrocarbyl phosphine oxides
    4.
    发明授权
    (hydroxy or alkanoyloxy alkylene)dihydrocarbyl phosphine oxides 失效
    （羟基或烷基亚烷基亚烷基）二氢氧化膦氧化物

    公开(公告)号：US3790638A

    公开(公告)日：1974-02-05

    申请号：US3790638D

    申请日：1971-08-12

    Applicant: HOECHST AG

    Inventor： KLEINER H

    IPC: C07F9/53 ,  C07F9/6506 ,  C07F9/50

    CPC classification number: C07F9/65061 ,  C07F9/5304

    Abstract: TERTIARY PHOSPHINE OXIDES ARE OBTAINED BY ADDING OLEFINS HAVING A TERMINAL HYDROXY OR AMINO GROUP OR FUNCTIONAL DERIVATIVES THEREOF TO SECONDARY PHOSPHINE OXIDES. THE ADDUCTS ARE USEFUL AS INTERMEDIATES IN THE PREPARATION OF FLAME-RETARDANT AGENTS, ANTI-CORROSIVE AGENTS, PESTICIDES, PHARMACEUTICALS AND DETERGENTS.

    Process for the preparation of dialkyl phosphites from alcohols and phosphorous acid
    7.
    发明授权
    Process for the preparation of dialkyl phosphites from alcohols and phosphorous acid 失效
    从醇和磷酸中制备二磷酸磷酸盐的方法

    公开(公告)号：US3725515A

    公开(公告)日：1973-04-03

    申请号：US3725515D

    申请日：1970-03-04

    Applicant: HOECHST AG

    Inventor： SCHIMMELSCHMIDT K ,  KLEINER H

    IPC: C07F9/142 ,  C07F9/08

    CPC classification number: C07F9/142

    Abstract: Improved process for the preparation of dialkyl phosphites by means of refluxing phosphorous acid with alcohols under azeotropic separation of the reaction water formed, wherein primary or secondary straight-chained or branched aliphatic alcohols having at least 4 carbon atoms are reacted in an excess of at least 45 percent over the stoichiometrical amount with phosphorous acid in the absence of an inert solvent until the amount of acid in the reaction mixture is as low as possible. In comparison to known processes the dialkyl phosphites are obtained according to the instant process in higher yields and with higher purity. The dialkyl phosphites are valuable intermediates. Owing to their high purity, they are especially suitable as starting materials for such reactions catalyzed by radicals.

    Abstract translation: 通过在形成的反应水的共沸分离下通过使亚磷酸与醇回流来制备亚磷酸二烷基酯的改进方法，其中具有至少4个碳原子的伯或仲直链或支链脂族醇至少过量反应 在不存在惰性溶剂的情况下，亚磷酸的化学计量比例为45％，直到反应混合物中酸的量尽可能低。 与已知方法相比，亚磷酸二烷基酯以本发明方法获得，产率更高，纯度更高。 亚磷酸二烷基酯是有价值的中间体。 由于它们的高纯度，它们特别适用于由自由基催化的这种反应的起始原料。

    Process for the preparation of tertiary phosphine oxides using high energy radiation
    8.
    发明授权
    Process for the preparation of tertiary phosphine oxides using high energy radiation 失效
    使用高能量辐射制备精细磷酸盐氧化物的方法

    公开(公告)号：US3714009A

    公开(公告)日：1973-01-30

    申请号：US3714009D

    申请日：1970-03-04

    Applicant: HOECHST AG

    Inventor： KLEINER H ,  ROSSINGER S

    IPC: A61K8/55 ,  A61Q17/00 ,  A61Q19/10 ,  C07F9/53 ,  C11D1/79 ,  B01J1/10

    CPC classification number: A61Q17/005 ,  A61K8/55 ,  A61Q19/10 ,  C07F9/5304 ,  C11D1/79

    Abstract: Improved process for the preparation of tertiary phosphine oxides by reacting dialkyl phosphine oxides with Alpha olefins, wherein the reaction is carried out in the presence of high-energy radiation. In comparison with known processes the tertiary phosphine oxides are obtained according to the instant process within a shorter reaction time, with higher purity and with higher yields. The reaction products can be used as intermediates, surfactants, detergents and cleaning agents, especially in cosmetic products.

    Abstract translation: 通过使二烷基氧化膦与α-烯烃反应制备叔氧化膦的改进方法，其中反应在高能量辐射的存在下进行。 与已知方法相比，根据本发明方法在更短的反应时间内获得了叔膦氧化物，具有较高的纯度和较高的收率。 反应产物可用作中间体，表面活性剂，洗涤剂和清洁剂，特别是在化妆品中。

    10.
    发明专利
    未知

    公开(公告)号：BR7407703D0

    公开(公告)日：1975-07-29

    申请号：BR770374

    申请日：1974-09-16

    Applicant: HOECHST AG

    Inventor： KLEINER H ,  FINKE M ,  BOLLERT U

    IPC: C08G63/00 ,  C07F9/6571 ,  C08G63/20 ,  C08G63/692 ,  C08G79/04 ,  D01F6/84 ,  C08G63/16 ,  C08K5/51

    Abstract: Flame-repellant linear polyesters are obtained by incorporating by condensation phosphorus-compounds having the formula O &uarr& HO-P-R-COOH, ¦ R1 wherein R and R1 are organic radicals which may also contain hereto atoms into the linear polyesters, preferably those from terephthalic acid and ethylene glycol. These polyesters are materials of which flame-repellent filaments, fibers, sheets, press-moulded and injection-moulded articles may be made. Products of the invention can be used whereever especially acute risks of ignition and fire exist.

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