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    Basic oxazine dyestuffs and process for their preparation
    2.
    发明授权
    Basic oxazine dyestuffs and process for their preparation 失效
    基本恶嗪染料及其制备方法

    公开(公告)号：US3928339A

    公开(公告)日：1975-12-23

    申请号：US43527774

    申请日：1974-01-21

    Applicant: HOECHST AG

    Inventor： MUNDLOS EBERHARD ,  HERZ LUIS ,  NEEB RUDOLF ,  MOHR REINHARD ,  OSTERMEIER JOHANN

    IPC: C09B19/00

    CPC classification number: C09B19/00

    Abstract: Basic oxazine dyestuffs of the formula I

    in which R stands for a lower alkyl group which may be substituted, R1 and R2 each stands for a hydrogen atom or a lower alkyl group which may be substituted and which may form together with the nitrogen atom also a heterocyclic radical, R3 stands for a hydrogen atom or a lower alkyl group which may be substituted, R4 stands for a hydrogen atom, a lower alkyl group which may be substituted, an aryl group which may be substituted, or together with the nitrogen atom and R3 or the benzene nucleus R4 may form a heterocyclic radical, and X stands for an anion, and the benzene nucleus a may carry further non ionic substituents or a fused benzene nucleus. The novel dyestuffs are suitable for the dyeing or printing of tannined cellulose fibers, silk, leather or fully synthetic fibers, such as acetate rayon, polyamide fibers or acid-modified polyamide or polyester fibers, especially of fibers containing polyacrylonitrile or polyvinylidene cyanide. The dyeings produced on these fibers are mostly very bright and have a good tinctorial strength as well as, in general, good fastness properties to light and wet processing, for example good fastness to washing, fulling, cross-dyeing, carbonizing, to the action of chlorine and to perspiration.

    Abstract translation: 式I的基本恶嗪染料，其中R表示可被取代的低级烷基，R 1和R 2各自表示氢原子或可以被取代的，可以与氮原子一起形成的低级烷基也是 杂环基，R 3表示氢原子或可被取代的低级烷基，R 4表示氢原子，可被取代的低级烷基，可被取代的芳基，或与氮原子一起 R3或苯核R4可以形成杂环基，X'代表阴离子，苯核a可以携带更多的非离子取代基或稠合的苯核。

    Basic ioninotriazole azoindole dyestuffs
    6.
    发明授权
    Basic ioninotriazole azoindole dyestuffs 失效
    基础离子喹诺酮类AZOINDOLE DYESTUFFS

    公开(公告)号：US3635942A

    公开(公告)日：1972-01-18

    申请号：US3635942D

    申请日：1969-02-10

    Applicant: HOECHST AG

    Inventor： MOHR REINHARD ,  OSTERMEIER JOHANN

    IPC: C09B44/18 ,  C09B29/00 ,  C09B29/36 ,  D06P1/08

    CPC classification number: C09B44/18 ,  Y10S8/922

    Abstract: BASIC AZO DYESTUFFS OF THE FORMULA:

    1-R1,2-R3,3-((1-R4,2-R5-INDOL-3-YL),4-R2,5-(HN=)-4,5-

    DIHYDRO-1H-1,2,4-TRIAZOLIUM X(-)

    WHEREIN R1 IS ARYL, R2 AND R3 ARE ALKYL OR ARALKYL, R4 AND R5 ARE HYDROGEN OR UNSUBSTITUTED OR SUBSTITUTED ALKYL OR ARYL, X$ IS AN ANION, AND IN WHICH THE BENZENE NUCLEUS A MAY CONTAIN NON-IONIC SUBSTITUENTS WHICH DYESTUFFS ARE SUITABLE FOR THE DYEING OR PRINTING OF TANNIN-TREATED CELLULOSE FIBERS, SILK, LEATHER OR FULLY SYNTHETIC FIBERS SUCH AS ACETATE RAYON, POLYAMIDE OR ACID-MODIFIED POLYESTER, ESPECIALLY FIBERS CONSISTING OF POLYACRYLONITRILE OR POLYVINYLIDENE CYANIDE, AND WHICH GIVE IN THE MAJORITY OF CASES DYEINGS WITH VERY CLEAR AND DEEP COLOURS AND GOOD FASTNESS TO LIGHT, FULLING, CROSS-DYEING, CARBONIZING, CHLORINATING, PERSPIRATION, DECATIZING, STEAMING, IRONING, RUBBING AND SOLVENTS.

    Basic triazole containing mono-azo dyestuffs
    7.
    发明授权
    Basic triazole containing mono-azo dyestuffs 失效
    含有单胺氧基的基本三唑

    公开(公告)号：US3597412A

    公开(公告)日：1971-08-03

    申请号：US3597412D

    申请日：1969-01-08

    Applicant: HOECHST AG

    Inventor： MOHR REINHARD ,  OSTERMEIER JOHANN

    IPC: C09B44/18 ,  C09B29/06 ,  D06P1/02

    CPC classification number: C09B44/18 ,  Y10S8/927

    Abstract: BASIC AZO DYESTUFFS OF THE FORMULA:

    (1-R1,2-HN=,3-R2,4-R5-N(-R4)-B-N=N-,5-R3-1,2-DIHYDRO-4H-1,

    2,4-TRIAZOLE)(+) X(-)

    WHEREIN R1 IS ARYL, R2 AND R3 ARE ALKYL OR ARALKYL, R4 AND R5 ARE UNSUBSTITUTED OR SUBSTITUTED ALKYL OR ARALKYL OR ARE JOINED TOGETHER TO FORM A RING, B IS A DIVALENT BENZENE OR NAPHTHALENE RADICAL AND X- IS AN ANION.

    Basic quinaldiniumazoindole dyestuffs
    8.
    发明授权
    Basic quinaldiniumazoindole dyestuffs 失效
    基本喹喔啉IN LE。。。。。

    公开(公告)号：US3562245A

    公开(公告)日：1971-02-09

    申请号：US3562245D

    申请日：1968-04-04

    Applicant: HOECHST AG

    Inventor： MOHR REINHARD ,  OSTERMEIER JOHANN

    IPC: C09B44/12 ,  C09B29/36 ,  D06P1/04 ,  D06P1/10

    CPC classification number: C09B44/126 ,  Y10S8/922

    Abstract: AZO-DYESTUFFS OF THE FORMULA

    1-R1,2-R2,4-((1-R4,2-R3,R5-3-INDOLYL)-N=N-)QUINOLINIUM

    X(-)

    WHEREIN R1 REPRESENTS METHYL OR ETHYL, R2 REPRESENTS METHYL, R3 REPRESENTS HYDROGEN, METHYL OR PHENYL, R4 REPRESENTS HYDROGEN OR METHYL, R5 REPRESENTS HYDROGEN, FLUORINE, CHLORINE, BROMINE, LOWER ALKYL, LOWER ALKOXY, CYANO OR NITRO, AND X- REPRESENTS AN ANION, SAID DYESTUFFS BEING SUITABLE FOR THE DYEING OR PRINTING OF TANNED CELLULOSE FIBRES, SILK, LEATHER OR FULLY SYNTHETIC FIBRES AND YIELDING DYEINGS OR PRINTS OF A VERY GOOD TINCTORIAL STRENGTH AND OF VERY GOOD FASTNESS PROPERTIES TO LIGHT AND TO WET PROCESSING.

    Basic azo dyestuffs of the 2,6-diamino-pyridine series
    9.
    发明授权
    Basic azo dyestuffs of the 2,6-diamino-pyridine series 失效
    2,6-二氨基 - 吡啶系列的碱性偶氮染料

    公开(公告)号：US3899478A

    公开(公告)日：1975-08-12

    申请号：US35660873

    申请日：1973-05-02

    Applicant: HOECHST AG

    Inventor： FLECKENSTEIN ERWIN ,  MOHR REINHARD ,  HEINRICH ERNST

    IPC: C07D213/74 ,  C07D213/80 ,  C07D213/82 ,  C07D213/85 ,  C09B29/42 ,  C09B44/00 ,  C09B44/08 ,  C09B44/10 ,  C09B29/36

    CPC classification number: C09B29/3639 ,  C09B44/08 ,  C09B44/105

    Abstract: A basic azo dyestuff of the formula

    WHEREIN A is an aromatic or heterocyclic diazo component, R1 and R2 each is primary, secondary or tertiary amino or hydrazino, R3 is cyano, carbo lower alkoxy, carbamoyl, lower alkyl carbamoyl, di lower alkyl carbamoyl, lower alkylsulfonyl or phenylsulfonyl, R4 is lower alkyl, substituted lower alkyl or phenyl, m is 1 or 2 and X is an anion and at least one of the groups A, R1, R2 and R4 contain a quaternary ammonium group of the formula

    wherein Y1 and Y2 are hydrogen, lower alkyl, benzyl or cyclohexyl, Y3 is hydrogen, lower alkyl, benzyl, cyclohexyl, lower alkoxy or amino or the nitrogen atom forms together with Y1 and Y2 or Y3 a heterocyclic ring. The novel dyestuffs are suitable for the preparation of writing and stamping inks or ball pen pastes and can be used for rubber printing. They are also suitable for the dyeing, printing or mass dyeing of tannined cellulose fibers, silk, hair, leather, coco fibers, jute, sisal or synthetic fibers, such as acetate silk, polyamide fibers or acid modified polyolefin, polyamide or polyester fibers, especially, however, of fibers containing polyacrylonitrile or polyvinylidene cyanide. The dyeings obtained on these fibers have, mostly, a high tinctorial strength and, in general, good fastnesses to light and to wet processing.

    Abstract translation: 式（Ⅰ）的碱性偶氮染料AN = N m X（I）m其中A是芳族或杂环重氮组分，R1和R2分别是伯，仲或叔氨基或肼基，R3是氰基 ，低级烷氧基，氨基甲酰基，低级烷基氨基甲酰基，二低级烷基氨基甲酰基，低级烷基磺酰基或苯基磺酰基，R4为低级烷基，取代的低级烷基或苯基，m为1或2，X为阴离子，基团A至 R1，R2和R4含有式Y1 | - + N-Y2 | Y3的季铵基，其中Y1和Y2为氢，低级烷基，苄基或环己基，Y3为氢，低级烷基，苄基，环己基， 低级烷氧基或氨基或氮原子与Y1和Y2或Y3一起形成杂环。

    3-amino-1h-pyrazolo(3,4-b)pyridines
    10.
    发明授权
    3-amino-1h-pyrazolo(3,4-b)pyridines 失效
    3-氨基-1H-吡唑并（3,4-B）吡啶

    公开(公告)号：US3872133A

    公开(公告)日：1975-03-18

    申请号：US37376673

    申请日：1973-06-26

    Applicant: HOECHST AG

    Inventor： FLECKENSTEIN ERWIN ,  MOHR REINHARD

    IPC: C07D213/85 ,  C07D471/04 ,  C09B29/036 ,  C09B44/14 ,  C07D31/42

    CPC classification number: C07D471/04 ,  C09B29/0029 ,  C09B44/14

    Abstract: IN WHICH Z1 stands for an optionally substituted alkyl or aralkyl group, K for the radical of a coupling component and A for an anion, and X, Y and Z are defined as further above. These dyestuffs, which are especially suitable for dyeing polyacrylonitrile, have a high tinctorial strength and generally afford good fastness properties.

    WHEREIN X is amino, alkylamino with 1 - 6 carbon atoms, lower alkoxy- lower alkylamino, hydroxy- lower alkylamino, amino- lower alkylamino, di-lower alkylamino - lower alkylamino, cyclohexylamino, benzylamino, furfurylamino, pyridylamino, pyridylmethylamino, phenylamino, lower alkoxy-phenylamino, dilower alkylamino, di-hydroxy lower alkylamino, lower alkyl hydroxy lower alkylamino, lower alkyl phenylamino, hydroxy lower alkyl cyclohexylamino, hydroxy lower alkyl lower alkoxyamino, lower alkyl lower alkoxyamino, morpholyl, piperidyl, N- lower alkyl piperazinyl, pyrrolidinyl, morpholyl- lower alkylamino; hydrazino, lower alkylhydrazino, di-lower alkylhydrazino, trilower alkylhydrazino, phenylhydrazino, N-piperidylamino, Nmorpholyalmino, N-pyrrolidinylamino,- lower alkoxy, lower alkoxy - lower alkoxy, cyclohexyloxy, phenoxy, benzyloxy, hydroxy lower alkoxy; lower alkylthio, phenylthio; Y is hydrogen, lower alkyl, hydroxy -lower alkyl, di-lower alkylamino -lower alkyl, cyclohexyl, benzyl, phenyl, chlorophenyl, furyl, pyridyl-methyl and Z is hydrogen or lower alkyl and ''''lower'''' means groups with one to four carbon atoms. These compounds are valuable intermediate products for the preparation of dyestuffs, especially of azo dyestuffs of the formula

    A 3-amino-1H-pyrazolo(3,4-b)pyridine of the formula

    Abstract translation: 具有式WHEREIN X的3-氨基-1H-吡唑并[3,4-b]吡啶是氨基，具有1-6个碳原子的烷基氨基，低级烷氧基 - 低级烷基氨基，羟基 - 低级烷基氨基，氨基 - 低级烷基氨基， 低级烷基氨基 - 低级烷基氨基，环己基氨基，苄基氨基，糠基氨基，吡啶基氨基，吡啶基甲基氨基，苯基氨基，低级烷氧基 - 苯基氨基，二低级烷基氨基，二羟基低级烷基氨基，低级烷基羟基低级烷基氨基，低级烷基苯基氨基，羟基低级烷基环己基氨基，羟基 低级烷基低级烷氧基氨基，低级烷基低级烷氧基氨基，吗啉基，哌啶基，N-低级烷基哌嗪基，吡咯烷基，吗啉基 - 低级烷基氨基; 肼基，低级烷基肼基，二低级烷基肼基，三低级烷基肼基，苯基肼基，N-哌啶基氨基，N-形式缩水甘油基，N-吡咯烷基氨基， - 低级烷氧基，低级烷氧基 - 低级烷氧基，环己氧基，苯氧基，苄氧基，羟基低级烷氧基。 低级烷硫基，苯硫基; Y是氢，低级烷基，羟基低级烷基，二低级烷基氨基 - 低级烷基，环己基，苄基，苯基，氯苯基，呋喃基，吡啶基 - 甲基，Z是氢或低级烷基，“低级” 碳原子。

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