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    Process for the preparation of tertiary methyl-phosphine oxides
    5.
    发明授权
    Process for the preparation of tertiary methyl-phosphine oxides 失效
    叔甲基膦氧化物的制备方法

    公开(公告)号：US3928463A

    公开(公告)日：1975-12-23

    申请号：US46013374

    申请日：1974-04-11

    Applicant: HOECHST AG

    Inventor： REUTER MARTIN ,  RUPP WALTER

    IPC: C07F9/53 ,  C08G18/38 ,  C07D105/02

    CPC classification number: C08G18/388 ,  C07F9/53

    Abstract: A process is provided for the catalytic preparation of tertiary methylphosphine oxides which comprises mixing hydroxymethylalkylphosphines with at least 1 weight % of carbon tetrachloride or carbon tetrabromide at a temperature of from -10* to +120*C, and, after the reaction is complete, isolating the tertiary methylphosphine oxide by distilling off the carbon tetrahalide.

    Abstract translation: 提供用于催化制备叔甲基氧化膦的方法，其包括在-10至+ 120℃的温度下将羟甲基 - 烷基膦与至少1重量％的四氯化碳或四溴化碳混合，并且在反应之后 通过蒸馏除去四卤化碳来分离叔甲基氧化膦。

    Process for the preparation of bis-hydroxymethyl-methylphosphine
    6.
    发明授权
    Process for the preparation of bis-hydroxymethyl-methylphosphine 失效
    制备双羟甲基 - 甲基膦的方法

    公开(公告)号：US3927112A

    公开(公告)日：1975-12-16

    申请号：US46015174

    申请日：1974-04-11

    Applicant: HOECHST AG

    Inventor： REUTER MARTIN ,  BEERMANN CLAUS

    IPC: C07F9/53 ,  C08G18/38 ,  C07D105/02

    CPC classification number: C08G18/388 ,  C07F9/53

    Abstract: A process is provided for the catalytic preparation of bis(hydroxymethyl)-methylphosphine oxide, which comprises mixing tris-(hydroxymethyl)-phosphine with at least 1 weight % of carbon tetrachloride or carbon tetrabromide at temperatures of from 10* to +120*C, and, after completed reaction, isolating the bis(hydroxymethyl)-methylphosphine oxide so obtained by distilling off the carbon tetrahalide.

    Abstract translation: 提供用于催化制备双（羟甲基） - 甲基氧化膦的方法，其包括在-10℃至+ 120℃的温度下将三 - （羟甲基） - 膦与至少1重量％的四氯化碳或四溴化碳混合 DEG，并且在完成反应后，通过蒸馏出四卤化碳分离得到的双 - （羟甲基） - 甲基氧化膦。

    Process for the preparation of methylphosphine oxides
    7.
    发明授权
    Process for the preparation of methylphosphine oxides 失效
    甲基膦氧化物的制备方法

    公开(公告)号：US3927113A

    公开(公告)日：1975-12-16

    申请号：US46015374

    申请日：1974-04-11

    Applicant: HOECHST AG

    Inventor： REUTER MARTIN ,  RUPP WALTER

    IPC: C07F9/53 ,  C08G18/38 ,  C07D105/02

    CPC classification number: C07F9/53 ,  C08G18/388

    Abstract: A process is provided for the catalytic preparation of tertiary methylphosphine oxides, which comprises mixing hydrohydroxymethyl-alkylphosphines with at least 1 weight % of a carbon tetrahalide of the formula C(Hal1)(Hal2)(Hal3), Hal4, where Hal1 is fluorine, chlorine or bromine, and Hal2, Hal3 and Hal4 each is chlorine or bromine, only three of the radicals Hal1 to Hal4 being the same at temperatures of from -10* to +120*C and, after completed reaction, isolating the methylphosphine oxide of formula (I) so obtained by distilling off the carbon tetrahalide.

    Abstract translation: 提供用于催化制备叔甲基氧化膦的方法，其包括将羟基甲基 - 烷基膦与至少1重量％的式C（Hal1）（Hal2）（Hal3），Hal4的四卤化物（其中Hal1为 氟，氯或溴，Hal2，Hal3和Hal4各自为氯或溴，在-10至+120℃的温度下，只有3个Hal1至Hal4的基团相同，反应完成后，将甲基膦 通过蒸馏掉四卤化物得到的式（I）氧化物。

    PRODUCTION OF TERTIARY METHYLPHOSPHINE OXIDES
    9.
    发明专利
    PRODUCTION OF TERTIARY METHYLPHOSPHINE OXIDES 未知

    公开(公告)号：CA1042467A

    公开(公告)日：1978-11-14

    申请号：CA222498

    申请日：1975-03-19

    Applicant: HOECHST AG

    Inventor： LIPPSMEIER BERND ,  HESTERMANN KLAUS ,  REUTER MARTIN

    IPC: B01J27/00 ,  C07B61/00 ,  C07F9/50 ,  C07F9/53

    Abstract: Production of tertiary methylphosphine oxides of the general formula (I) in which R and R' each stand for identical or different, alkyl groups other than a hydroxymethl group, having from 1 to 6 carbon atoms. The compounds are produced by subjecting tertiary hydroxymethylphosphines of the general formula (II) in which R and R1 have the meanings given above, to a thermal rearrangement reaction at temperatures higher than about 90.degree.C or, in the presence of BF3.etherate as catalyst, at temperatures within the range -10 and.250.degree.C.

    PROCESS FOR PROVIDING CELLULOSE FIBRE MATERIAL WITH A FLAME-PROOF FINISH
    10.
    发明专利
    PROCESS FOR PROVIDING CELLULOSE FIBRE MATERIAL WITH A FLAME-PROOF FINISH 未知

    公开(公告)号：CA960921A

    公开(公告)日：1975-01-14

    申请号：CA121549

    申请日：1971-08-27

    Applicant: HOECHST AG

    Inventor： REUTER MARTIN ,  BEERMANN CLAUS ,  LINKE FRITZ

    IPC: C07F9/40 ,  D06M13/288

    Abstract: 1364700 Derivatives of urethanoalkyl phosphonic acid esters FARBWERKE HOECHST AG 25 Aug 1971 [29 Aug 1970] 39846/71 Addition to 1311906 Heading C2P [Also in Division D1] Novel compounds of the general formula wherein each of R, R 1 and R 11 are alkyl, preferably C 1 -C 4 alkyl, and Y is H or a methylol group, are obtained by reacting a compound of the formula with formaldehyde. The products are useful as flame-proofing agents for cellulosic fibrous materials. The compounds (II) may be obtained by reacting a compound with phosgene to form and then treating the latter with ammonia, or by reacting III with chlorosulphonyl isocyanate and then hydrolysing the main reaction product.

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