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    4.
    发明专利
    未知

    公开(公告)号：DE2413008A1

    公开(公告)日：1976-02-12

    申请号：DE2413008

    申请日：1974-03-18

    Applicant: HOECHST AG

    Inventor： STAEHLER GERHARD DR ,  EMMEL LUDWIG DR ,  BONIN WERNER DR

    IPC: A01N57/16 ,  A01N57/24 ,  A01N57/34 ,  C07F9/653 ,  C07F9/65 ,  A01N9/36

    Abstract: Mono- and dithiophosphonic acid esters of the formula I in which R is optionally substituted alkyl, cycloalkyl, cycloalkenyl, or optionally substituted phenyl, R' is optionally substituted alkyl, alkenyl, or cycloalkyl, R'' and R''' which are identical or different, are hydrogen, halogen, methyl, methoxy, nitro or trifluoromethyl, and X is oxygen or sulfur, are useful insecticides and acaricides.

    7.
    发明专利
    未知

    公开(公告)号：DE3002413A1

    公开(公告)日：1981-07-30

    申请号：DE3002413

    申请日：1980-01-24

    Applicant: HOECHST AG

    Inventor： STAEHLER GERHARD DR ,  WALTERSDORFER ANNA DR

    IPC: A01N47/18 ,  C07D231/28 ,  A01N43/56

    Abstract: Compounds of the formula I (I) in which R is hydrogen, (subst.) alkyl, cycloalkyl, benzyl, phenylethyl or (subst.) phenyl, R1, R2 and R3 are alkyl and X is oxygen or sulfur are effective insecticides and acaricides and especially suitable for combating plant lice.

    Phosphonic acid dihalides prodn - by catalytic halogenation with carbonyl or oxalyl halides
    8.
    发明专利
    Phosphonic acid dihalides prodn - by catalytic halogenation with carbonyl or oxalyl halides 未知

    公开(公告)号：DE2225547A1

    公开(公告)日：1973-12-06

    申请号：DE2225547

    申请日：1972-05-26

    Applicant: HOECHST AG

    Inventor： FINKE MANFRED DR ,  KLEINER HANS-JERG DR ,  STAEHLER GERHARD DR

    IPC: C07F9/42 ,  C07F9/48

    Abstract: Title cpds. of the formula: (where R is 1-18C alkyl, 4-8C cycloalkyl, 2-8C alkenyl, or 6-8C aryl, aralkyl, or alkyl-aryl, R opt. being substd by Cl, Br, CN, or lower acyloxy; and X is halogen) are prepd. by reacting phosphonic acid derivs. of the formula: R-P(O)(OR1)(OR2) (where R1 is H, a monovalent cation, 1-12C alkyl or haloalkyl or 4-8C cycloalkyl, and R2 is H or a monovalent cation) or corresponding pyrophosphonic acid derivs. or thio analogues of these derivs. with acid halides of the formula (CO)nX2 (where n is 1 or 2) in the presence of (a) cpds. contg. >=1 tertiary or quaternary N- or P-atom at least 3 valences of which are linked to is not >20C org. residues (2 of the valences opt. forming a double bond) or of (b) mono-, di- or tribasic org. or inorg. fully amidated acids of tri- or pentavalent phosphorus, the N-atoms of which are alkylated with is not >20C aliphatic residues and the organic residues of which contain is not >20C-atoms, opt. in the presence of an inert solvent.

    Phosphonic acid dihalides - from (thio) phosphonic acids and a carbonyl halide
    9.
    发明专利
    Phosphonic acid dihalides - from (thio) phosphonic acids and a carbonyl halide 未知

    公开(公告)号：DE2129584A1

    公开(公告)日：1972-12-21

    申请号：DE2129584

    申请日：1971-06-15

    Applicant: HOECHST AG

    Inventor： FINKE MANFRED DR ,  KLEINER HANS-JERG DR-ING ,  STAEHLER GERHARD DR

    IPC: C07F9/42

    Abstract: In a process for cpds. (I): (where R is 1-18C alkyl, 4-8C cycloalkyl, 2-18C-alkenyl, Ph, phenylalkyl oralkylphenyl (of 6-8C), all opt. substd. by Cl, Br, CN or acyloxy, and X is halogen) cpds. (II) or their salts or functional derivs. (where Y = O or S) are reacted with cpds. (III): (where n is 1 or 2) in the presence of cpds. having at least 1 Natom or tri- or penta-valent P which is linked (in the case of N) by 1-4 valencies or (in the case of P) by at least 3 valencies to organic radicals having up to 20C, two of the valencies may form a double bond or in the presence of amidated mono-, di- or tri-acids of tri- or pentavalent-P, the N atoms of which may carry 1-20C alkyl groups and whose organic radicals may contain up to 20C and optionally in the presence of a solvent. Intermediates for plant protection agents, ripening agents, ignifuges. Esp. intermediates for 2-chloroethane phosphonic acid and its derivs. and vinylphosphonic acid which may be used in its polymerised form to prevent corrosion in metals. Increased yields without purification of intermediates.

    10.
    发明专利
    未知

    公开(公告)号：DE1770936A1

    公开(公告)日：1972-02-17

    申请号：DE1770936

    申请日：1968-07-20

    Applicant: HOECHST AG

    Inventor： SCHERER OTTO DR ,  STAEHLER GERHARD DR

    IPC: A01N57/16 ,  C07F9/653 ,  C07F9/16

    Abstract: 1,262,675. Phosphorus-containing isoxazole derivatives. FARBWERKE HOECHST A.G. 21 July, 1969 [20 July, 1968], No. 36587/69. Heading C2P. Novel compounds of the general formula in which R is methyl or ethyl and X is O or S are obtained by reacting (RO) 2 P(X)SMe, where Me is ammonium or an alkali metal or alkaline earth metal with. The reaction is preferably carried-out in a polar solvent and the two isomeric chlpromethyl isoxazoles may be used separately or in admixture. The products have pesticidal, especially systemic insecticidal and acaricidal, properties and may be used in admixture with solid or liquid carriers. The compositions may contain wetting agents, dispersing agents, adhesives or grinding auxiliaries and may be in the form of wettable powders, emulsions, suspensions, dusting powders or granules.

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