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    CHARGE IMBALANCED POLYELECTROLYTE COMPOSITION
    2.
    发明申请
    CHARGE IMBALANCED POLYELECTROLYTE COMPOSITION 审中-公开
    电荷不均匀聚电解质组合物

    公开(公告)号：WO1993019102A1

    公开(公告)日：1993-09-30

    申请号：PCT/US1993000790

    申请日：1993-01-28

    Applicant: ISP INVESTMENTS INC.

    Inventor： ISP INVESTMENTS INC. ,  CHAUDHURI, Ratan, K. ,  ANDERSON, Lowell, R. ,  LOGIN, Robert, B.

    IPC: C08F08/32

    CPC classification number: C08F8/12 ,  C08F2810/50 ,  C08F222/06 ,  C08F216/18 ,  C08F8/48 ,  C08F8/32

    Abstract: A charge imbalanced composition comprising: (a) about 10 to 90 mole % of a mixture of amphoteric copolymers having formulas (I) and (II) where A is present in an amount of about 0.1-0.8 mole, and B is present in an amount of about 0.05-0.4 mole, and where A is 2-6 times B, where R=C1-C4, n=1-6, R1 and R2 are independently C1-C6, R3 is H or lower alkyl, and R4=C12-C24; (b) about 10 to 90 mole % of a polymeric diacid having formula (III) where R is as defined above, and (c) about 0-20 mole % of by-product salts which are the dialkylaminoalkylamine and alkylamine salts of (a) and (b). The composition described above is made by: reacting 1 mole of an anhydride compound having formula (IV) where R is as defined above, with less than 1 mole of a mixture of about 0.1-0.8 mole of a compound having formula (A) where n, R1, R2 and R3 are as defined above, and about 0.05-0.4 of a compound having formula (B) where R4 is as defined above, and where A is 2-6 times B, isolating the product, and hydrolyzing any residual anhydride compound in water to the corresponding diacid compound.

    Abstract translation: 一种电荷不平衡组合物，其包含：（a）约10至90摩尔％的具有式（I）和（II）的两性共聚物的混合物，其中A以约0.1-0.8摩尔的量存在，B存在于 量为约0.05-0.4摩尔，其中A为2-6倍B，其中R = C1-C4，n = 1-6，R1和R2独立地为C1-C6，R3为H或低级烷基，R4 = C12-C24; （b）约10至90摩尔％的具有式（III）的聚合二酸，其中R如上所定义，和（c）约0-20摩尔％的副产物盐，其是二烷基氨基烷基胺和（a ）和（b）。 上述组合物是通过使1摩尔具有式（Ⅳ）的式（Ⅳ）的酸酐化合物（其中R如上定义）与少于1摩尔约0.1-0.8摩尔具有式（A）的化合物的混合物反应，其中 n，R 1，R 2和R 3如上定义，和约0.05-0.4的具有式（B）的化合物，其中R 4如上所定义，并且其中A是2-6倍B，分离产物，并水解任何残余物 水中的酸酐化合物与相应的二酸化合物。

    CHARGE IMBALANCED POLYELECTROLYTE COMPOSITION
    3.
    发明申请
    CHARGE IMBALANCED POLYELECTROLYTE COMPOSITION 审中-公开
    电荷不均匀聚电解质组合物

    公开(公告)号：WO1993011170A1

    公开(公告)日：1993-06-10

    申请号：PCT/US1992008251

    申请日：1992-09-30

    Applicant: ISP INVESTMENTS INC.

    Inventor： ISP INVESTMENTS INC. ,  CHAUDHURI, Ratan, K. ,  LOGIN, Robert, B. ,  ANDERSON, Lowell, R. ,  TAZI, Mohammed

    IPC: C08F08/32

    CPC classification number: C08F8/12 ,  C08F2810/50 ,  C08F8/48 ,  C08F8/32 ,  C08F222/06 ,  C08F216/18

    Abstract: A charge imbalanced composition comprising: (a) about 10 to 90 mole % of an amphoteric copolymer having formula (I) where R = alkyl C1-C4, n = 1-6, R1 and R2 are independently alkyl C1-C6, and R3 is H; (b) about 10 to 90 mole % of a polymeric diacid having formula (II) where R is as defined above, and (c) less than about 8 mole % of by-product salts which are the dialkylaminoalkylamine salts of (a) and (b). The composition described above is made by: reacting 1 mole of an anhydride compound having formula (III) where R is as defined above, with less than 1 mole of a compound having formula (IV) where n, R1 and R2 are as defined above, and R3 is H, isolating the product, and hydrolyzing residual anhydride compound in water to the corresponding diacid compound.

    PROCESS FOR MAKING SUBSTANTIALLY HOMOGENEOUS COPOLYMERS OF VINYL PYRROLIDONE AND N-3,3-DIMETHYLAMINOPROPYL METHACRYLAMIDE FOR PERSONAL CARE APPLICATIONS
    4.
    发明申请
    PROCESS FOR MAKING SUBSTANTIALLY HOMOGENEOUS COPOLYMERS OF VINYL PYRROLIDONE AND N-3,3-DIMETHYLAMINOPROPYL METHACRYLAMIDE FOR PERSONAL CARE APPLICATIONS 审中-公开
    制备乙烯吡咯烷酮和N-3,3-二甲基氨基丙烯酰胺甲基丙烯酰胺用于个人护理应用的大量均质共聚物的方法

    公开(公告)号：WO1996019967A1

    公开(公告)日：1996-07-04

    申请号：PCT/US1995015973

    申请日：1995-12-11

    Applicant: ISP INVESTMENTS INC.

    Inventor： ISP INVESTMENTS INC. ,  LIU, Kou-Chang ,  ANDERSON, Lowell, R. ,  HARDY, Eugene, E. ,  REUVEN, Yakir

    IPC: A61K07/11

    CPC classification number: C08F220/60 ,  A61K8/8182 ,  A61Q5/06 ,  C08F2/10 ,  C08F226/10

    Abstract: A process is described for making substantially homogeneous copolymers comprising 20-99 % of vinyl pyrrolidone (VP) and 1-80 % of N-3,3-dimethylaminopropyl methacrylamide (DMAPMA), preferably 50-95 % VP and 5-50 % DMAPMA, and, most preferably, about 80:20, by weight, having a weight average molecular weight of about 200,000 to 1,500,000, as a clear, low viscosity aqueous solution of the homogeneous copolymer, at a 5-20 % solids level, preferably about 10-15 %, by weight of the solution, having a viscosity of about 5,000 to 80,000 cps, preferably about 10,000 to 70,000 cps. The solution obtained herein has lower viscosity and better clarity, and provides hair care products with enhanced curl retention (hold), when compared to non-homogeneous copolymers of the same composition, or related existing commercial products.

    Abstract translation: 描述了一种制备基本上均匀的共聚物的方法，其包含20-99％的乙烯基吡咯烷酮（VP）和1-80％的N-3,3-二甲基氨基丙基甲基丙烯酰胺（DMAPMA），优选50-95％VP和5-50％DMAPMA ，最优选约80:20重量％，重均分子量为约200,000至1,500,000，作为均匀共聚物的透明低粘度水溶液，固含量为5-20％，优选约为 10-15％（重量）的溶液，其粘度为约5,000至80,000cps，优选约10,000至70,000cps。 本文获得的溶液具有较低的粘度和更好的透明度，并且与相同成分的非均相共聚物或相关的现有商品相比，提供具有增强的卷曲保持性（保持）的护发产品。

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