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公开(公告)号：US09970120B2
公开(公告)日：2018-05-15
申请号：US14997636
申请日：2016-01-18
Applicant: Integran Technologies Inc.
Inventor： Klaus Tomantschger , Diana Facchini , Francisco Gonzalez , Jonathan McCrea , John Kratochwil , Dan Woloshyn , Yusuf Bismilla , Nandakumar Nagarajan , Mioara Neacsu
Abstract: A method for electrodepositing a coating/free-standing layer on a workpiece in an electrolytic cell includes moving the workpiece and an anode applicator tool having a consumable anode insert relative to each other; anodically dissolving a metal from the insert and cathodically depositing the metal on the workpiece; providing flow of electrolyte solution through the insert to ensure that greater than 90% of the anodic reaction is represented by dissolution of the metal; recirculating collected electrolyte solution exiting the electrolytic cell through the insert; applying an electric current to the electrolytic cell; maintaining a concentration of the anodically dissolved metal within ±25% of each Ampere-hour per liter of electroplating solution; and creating a cathodic electrodeposit on the workpiece which includes the anodically dissolved metal, the chemical composition of the deposit varying by less than 25% in the deposition direction over a selected thickness of up to 25 microns of the deposit.
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公开(公告)号：US20130337288A1
公开(公告)日：2013-12-19
申请号：US13975696
申请日：2013-08-26
Applicant: Integran Technologies Inc.
Inventor： Diana Facchini , Francisco Gonzalez , Jonathan McCrea , Mike Uetz , Gino Palumbo , Klaus Tomantschger , Nandakumar Nagarajan , Jared J. Victor , Uwe Erb
IPC: B32B15/01
Abstract: Free standing articles or articles at least partially coated with substantially porosity free, fine-grained and/or amorphous Co-bearing metallic materials optionally containing solid particulates dispersed therein, are disclosed. The electrodeposited metallic layers and/or patches comprising Co provide, enhance or restore strength, wear and/or lubricity of substrates without reducing the fatigue performance compared to either uncoated or equivalent thickness Cr coated substrate. The fine-grained and/or amorphous metallic coatings comprising Co are particularly suited for articles exposed to thermal cycling, fatigue and other stresses and/or in applications requiring anti-microbial and hydrophobic properties.
Abstract translation: 公开了至少部分地涂覆有基本上无孔隙的细颗粒和/或无定形的含Co金属材料的任选地含有分散在其中的固体颗粒的独立制品或制品。 包含Co的电沉积金属层和/或贴剂提供，增强或恢复基材的强度，磨损和/或润滑性，而不降低与未涂覆或等效厚度的Cr涂覆的基材相比的疲劳性能。 包含Co的细晶粒和/或无定形金属涂层特别适用于暴露于热循环，疲劳和其他应力的物品和/或需要抗微生物和疏水性质的应用中。
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3.发明授权Electrodeposited metallic coatings comprising cobalt with enhanced fatigue properties 有权包含钴的电沉积金属涂层具有增强的疲劳性能公开(公告)号：US08663819B2
公开(公告)日：2014-03-04
申请号：US13673017
申请日：2012-11-09
Applicant: Integran Technologies, Inc.
Inventor： Francisco Gonzalez , Diana Facchini , Jonathan McCrea , Mike Uetz , Gino Palumbo , Klaus Tomantschger
CPC classification number: C25D7/00 , B32B15/01 , B32B15/013 , B32B15/017 , C22C19/07 , C23C30/00 , C25D3/12 , C25D3/562 , C25D5/18 , C25D5/50 , C25D7/04 , C25D15/00 , Y10T428/12458 , Y10T428/12493 , Y10T428/12625 , Y10T428/12729 , Y10T428/1275 , Y10T428/12778 , Y10T428/12861 , Y10T428/12882 , Y10T428/1291 , Y10T428/12937 , Y10T428/12944 , Y10T428/12951 , Y10T428/12972 , Y10T428/12979 , Y10T428/13 , Y10T428/24942 , Y10T428/24967 , Y10T428/26 , Y10T428/263 , Y10T428/264 , Y10T428/265
Abstract: Free standing articles or articles at least partially coated with substantially porosity free, fine-grained and/or amorphous Co-bearing metallic materials optionally containing solid particulates dispersed therein, are disclosed. The electrodeposited metallic layers and/or patches comprising Co provide, enhance or restore strength, wear and/or lubricity of substrates without reducing the fatigue performance compared to either uncoated or equivalent thickness chromium coated substrate. The fine-grained and/or amorphous metallic coatings comprising Co are particularly suited for articles exposed to thermal cycling, fatigue and other stresses and/or in applications requiring anti-microbial properties.
Abstract translation: 公开了至少部分地涂覆有基本上无孔隙的细颗粒和/或无定形的含Co金属材料的任选地含有分散在其中的固体颗粒的独立制品或制品。 包含Co的电沉积金属层和/或贴剂提供，增强或恢复基材的强度，磨损和/或润滑性，而不降低与未涂覆或等效厚度的铬涂覆的基材相比的疲劳性能。 包含Co的细粒和/或无定形金属涂层特别适用于暴露于热循环，疲劳和其它应力和/或需要抗微生物性能的应用中的制品。
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公开(公告)号：US20150111673A1
公开(公告)日：2015-04-23
申请号：US14513267
申请日：2014-10-14
Applicant: Integran Technologies Inc.
Inventor： Klaus Tomantschger , Jonathan McCrea , Nandakumar Nasarajan , Francisco Gonzalez , Gino Palumbo , Konstantinos Panagiotopoulos , Herath Katugaha , Diana Facchini , Jared Victor , Uwe Erb
IPC: C23C18/16 , C09J163/00 , A63B59/14
CPC classification number: C23C18/1641 , A63B59/70 , A63B2102/24 , B32B1/08 , B32B3/30 , B32B7/02 , B32B15/08 , B32B15/18 , B32B15/20 , B32B27/08 , B32B27/16 , B32B27/18 , B32B27/20 , B32B27/281 , B32B27/285 , B32B27/288 , B32B27/302 , B32B27/304 , B32B27/308 , B32B27/32 , B32B27/322 , B32B27/34 , B32B27/36 , B32B27/365 , B32B27/38 , B32B27/40 , B32B27/42 , B32B2255/06 , B32B2255/10 , B32B2255/20 , B32B2255/205 , B32B2262/101 , B32B2262/106 , B32B2264/02 , B32B2264/10 , B32B2264/12 , B32B2270/00 , B32B2307/202 , B32B2307/212 , B32B2307/30 , B32B2307/51 , B32B2307/538 , B32B2307/54 , B32B2307/718 , B32B2457/00 , B32B2509/00 , B32B2535/00 , B32B2597/00 , B32B2605/00 , C09J163/00 , C23C14/021 , C23C14/024 , C23C14/028 , C23C16/0227 , C23C16/0254 , C23C16/0272 , C23C18/1855 , C23C18/1893 , C23C18/1896 , C25D5/54 , Y10T428/12111 , Y10T428/12389 , Y10T428/12451 , Y10T428/12472 , Y10T428/12569 , Y10T428/12944 , Y10T428/1355 , Y10T428/24355 , Y10T428/24545 , Y10T428/24612 , Y10T428/26 , Y10T428/269
Abstract: The fine-grained and/or amorphous metallic coatings are particularly suited for strong and lightweight sporting goods exposed to thermal cycling although the coefficient of linear thermal expansion (CLTE) of the metallic layer and the substrate are mismatched.
Abstract translation: 细晶粒和/或非晶金属涂层特别适用于暴露于热循环的强和轻的运动用品，尽管金属层和基材的线性热膨胀系数（CLTE）不匹配。
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Patent Agency Ranking
5.发明授权Method of making articles with super-hydrophobic and/or self-cleaning surfaces 有权用超疏水和/或自清洁表面制造制品的方法公开(公告)号：US08784713B2
公开(公告)日：2014-07-22
申请号：US13906900
申请日：2013-05-31
Applicant: Integran Technologies Inc.
Inventor： Jared J. Victor , Uwe Erb , Klaus Tomantschger , Nandakumar Nagarajan , Diana Facchini , Mioara Neacsu
IPC: B29C33/42
CPC classification number: B29C59/02 , B29C37/0053 , B29C43/021 , B29C59/022 , B29C2043/025 , B29C2059/023 , Y10T428/139 , Y10T428/24355
Abstract: Super-hydrophobic and self-cleaning articles produced by imprinting exposed surfaces with suitable fine-grained and/or amorphous metallic embossing dies to transfer a dual surface structure, including ultra-fine features less than or equal to 100 nm embedded in and overlaying a surface topography with macro-surface structures greater than or equal to 1 micron are disclosed.
Abstract translation: 通过用合适的细粒和/或无定形金属压花模印制暴露表面而制造的超疏水和自清洁制品，以转移双表面结构，包括嵌入并覆盖表面的小于或等于100nm的超细特征 公开了具有大于或等于1微米的宏观表面结构的形貌。
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公开(公告)号：US08691397B2
公开(公告)日：2014-04-08
申请号：US13665052
申请日：2012-10-31
Applicant: Integran Technologies, Inc.
Inventor： Diana Facchini , Francisco Gonzalez , Jonathan McCrea , Mike Uetz , Gino Palumbo , Klaus Tomantschger
CPC classification number: C25D3/562 , C25D3/12 , C25D3/26 , C25D5/18 , C25D5/50 , C25D15/00 , Y10T428/12049 , Y10T428/12493 , Y10T428/12861 , Y10T428/12937 , Y10T428/12993 , Y10T428/13 , Y10T428/24942 , Y10T428/24967 , Y10T428/26 , Y10T428/263 , Y10T428/264 , Y10T428/265
Abstract: Free standing articles or articles at least partially coated with substantially porosity free, fine-grained and/or amorphous Co-bearing metallic materials optionally containing solid particulates dispersed therein, are disclosed. The electrodeposited metallic layers and/or patches comprising Co provide, enhance or restore strength, wear and/or lubricity of substrates without reducing the fatigue performance. The fine-grained and/or amorphous metallic coatings comprising Co are particularly suited for articles exposed to thermal cycling, fatigue and other stresses and/or in applications requiring anti-microbial properties.
Abstract translation: 公开了至少部分地涂覆有基本上无孔隙的细颗粒和/或无定形的含Co金属材料的任选地含有分散在其中的固体颗粒的独立制品或制品。 包含Co的电沉积金属层和/或贴剂提供，增强或恢复基底的强度，磨损和/或润滑性，而不降低疲劳性能。 包含Co的细粒和/或无定形金属涂层特别适用于暴露于热循环，疲劳和其它应力和/或需要抗微生物性能的应用中的制品。
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7.发明申请METHOD OF MAKING ARTICLES WITH SUPER-HYDROPHOBIC AND/OR SELF-CLEANING SURFACES 有权用超疏水和/或自清洁表面制造制品的方法公开(公告)号：US20130256944A1
公开(公告)日：2013-10-03
申请号：US13906900
申请日：2013-05-31
Applicant: Integran Technologies Inc.
Inventor： Jared J. Victor , Uwe Erb , Klaus Tomantschger , Nandakumar Nagarajan , Diana Facchini , Mioara Neacsu
IPC: B29C59/02
CPC classification number: B29C59/02 , B29C37/0053 , B29C43/021 , B29C59/022 , B29C2043/025 , B29C2059/023 , Y10T428/139 , Y10T428/24355
Abstract: Super-hydrophobic and self-cleaning articles produced by imprinting exposed surfaces with suitable fine-grained and/or amorphous metallic embossing dies to transfer a dual surface structure, including ultra-fine features less than or equal to 100 nm embedded in and overlaying a surface topography with macro-surface structures greater than or equal to 1 micron are disclosed.
Abstract translation: 通过用合适的细粒和/或无定形金属压花模印制暴露表面而制造的超疏水和自清洁制品，以转移双表面结构，包括嵌入并覆盖表面的小于或等于100nm的超细特征 公开了具有大于或等于1微米的宏观表面结构的形貌。
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8.发明授权公开(公告)号：US10286120B2
公开(公告)日：2019-05-14
申请号：US14826611
申请日：2015-08-14
Applicant: INTEGRAN TECHNOLOGIES, INC.
Inventor： Klaus Tomantschger , Gino Palumbo , Diana Facchini
Abstract: In-vivo biodegradable medical implants, containing at least in part at least partially fine-grained metallic materials provide a strong, tough, stiff and lightweight implant. The in-vivo biodegradable implants are used in a number of stent applications, for fracture fixation, sutures and the like. The in-vivo biodegradable medical implants enable the reduction of implant size and weight and consequently result in reducing the release of implant degradation products into the body.
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9.发明申请公开(公告)号：US20160130713A1
公开(公告)日：2016-05-12
申请号：US14997636
申请日：2016-01-18
Applicant: Integran Technologies Inc.
Inventor： Klaus Tomantschger , Diana Facchini , Francisco Gonzalez , Jonathan McCrea , John Kratochwil , Dan Woloshyn , Yusuf Bismilla , Nandakumar Nagarajan , Mioara Neacsu
Abstract: A method for electrodepositing a coating/free-standing layer on a workpiece in an electrolytic cell includes moving the workpiece and an anode applicator tool having a consumable anode insert relative to each other; anodically dissolving a metal from the insert and cathodically depositing the metal on the workpiece; providing flow of electrolyte solution through the insert to ensure that greater than 90% of the anodic reaction is represented by dissolution of the metal; recirculating collected electrolyte solution exiting the electrolytic cell through the insert; applying an electric current to the electrolytic cell; maintaining a concentration of the anodically dissolved metal within ±25% of each Ampere-hour per liter of electroplating solution; and creating a cathodic electrodeposit on the workpiece which includes the anodically dissolved metal, the chemical composition of the deposit varying by less than 25% in the deposition direction over a selected thickness of up to 25 microns of the deposit.
Abstract translation: 一种用于在电解池中将工件上的涂层/独立层电沉积的方法包括相对于彼此移动工件和具有可消耗阳极插入件的阳极施用工具; 将金属从插入物阳极溶解并将金属阴极沉积在工件上; 提供电解质溶液通过插入物的流动，以确保大于90％的阳极反应由金属的溶解表示; 通过插入物再循环离开电解池的收集的电解质溶液; 向电解槽施加电流; 将阳极溶解的金属的浓度保持在每升电镀溶液的每安培小时的±25％内; 并且在包括阳极溶解的金属的工件上产生阴极电沉积物，沉积物的沉积方向上的沉积物的化学成分在沉积方向上选择厚度高达25微米的选定厚度变化小于25％。
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