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公开(公告)号:JP2584495B2
公开(公告)日:1997-02-26
申请号:JP18774188
申请日:1988-07-27
Applicant: KAO CORP
Inventor: OOYA NAOHIRO , TOKUNAGA HIROSHI , YASUDA YUTAKA , MATSUI SADA
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公开(公告)号:JPH078927A
公开(公告)日:1995-01-13
申请号:JP14952493
申请日:1993-06-21
Applicant: KAO CORP
Inventor: MATSUI SADA , KINUTA MAMORU , SHIBATA MANABU
IPC: B08B3/12 , G11B23/03 , G11B23/113
Abstract: PURPOSE:To uniformly and certainly apply ultrasonic treatment to a large quantity of shutter members. CONSTITUTION:The ultrasonic washing device 1 for a shutter member such as a container for a recording medium subjected to punching processing and formed so as to be bent into an almost horizontal U-shape, is provided with a washing tank 3, a plurality of the ultrasonic vibrators 4 arranged on the bottom surface of the washing tank 3 and the shutter member receiving container arranged to the upper part within the area becoming shortest in peripheral length of the figure surrounding the arranged ultrasonic vibrators 4.
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公开(公告)号:JPS63218702A
公开(公告)日:1988-09-12
申请号:JP5147087
申请日:1987-03-06
Applicant: KAO CORP
Inventor: ISHII MASUKAME , MATSUI SADA , KATADA NAOKI
IPC: C08F2/18
Abstract: PURPOSE:To produce a highly water-absorbing polymer in high production efficiency, preventing the deposition of polymer particles in a reactor, by continuously carrying out polymerization reaction, control of water-content and crosslinking steps in individual reactors. CONSTITUTION:The objective highly water-absorbing polymer can be produced by continuously carrying out the following stage using one or more reactors for each stop. (1) A step to produce a slurry containing polymer phase by dissolving a water-soluble vinyl monomer (e.g. acrylic acid and itaconic acid) and a water-soluble polymerization initiator (e.g. potassium persulfate and sodium persulfate) in water, suspending the obtained aqueous solution in a hydrocarbon (e.g. n-pentane and cyclohexane) and subjecting the dispersion to suspension polymerization. (2) A step to remove water in the polymer phase of the slurry together with the hydrocarbon from the system. (3) A step to add a water-soluble crosslinking agent to the slurry containing the polymer phase and carry out crosslinking reaction in the polymer phase.
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公开(公告)号:JPH06346086A
公开(公告)日:1994-12-20
申请号:JP14219093
申请日:1993-06-14
Applicant: KAO CORP
Inventor: MATSUI SADA , KINUTA MAMORU , SHIBATA MANABU
IPC: C10M169/04 , C10N30/04 , C10N30/10 , C10N30/12 , C10N40/22
Abstract: PURPOSE:To obtain a cutting oil little in adverse effects on the environment and human body, ready to wash away from objects by simply using water, by admixing a cutting oil composition with a dicarboxylic ester-incorporated specific mixture. CONSTITUTION:This cutting oil can be obtained by admixing (A) an oil composition prepared by mixing (1) a mineral oil as the main component with (2) an antioxidant, (3) a rust-proofing agent, etc., with (B) a mixture of (4) a mineral oil and (5) a dicarboxylic ester with an aliphatic hydrocarbon as the main chain. The preferable amounts of the respective components to be used are as follows: component B: 5-100 pts.wt. per 100 pts.wt. of the component A; component 5: 0.1-15 pts.wt. per 100 pts.wt. of the component 4.
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公开(公告)号:JPH02163149A
公开(公告)日:1990-06-22
申请号:JP31801288
申请日:1988-12-16
Applicant: KAO CORP
Inventor: TORIMAE YASUHIRO , MATSUI SADA
Abstract: PURPOSE:To obtain a film having film strength and chemical resistance as a packaging material, soluble in cold water, comprising a polyvinyl alcohol-based polymer prepared by saponifying a copolymer having vinyl acetate and itaconic acid as essential monomer units. CONSTITUTION:A copolymer comprising 2-8mol% itaconic acid, 88-98mol% vinyl alcohol and 0-4mol% vinyl acetate is saponified to give a polyvinyl alcohol-based polymer having 10-45cPs viscosity at 4% aqueous solution, which is optionally blended with 5-20 pts.wt. based on 100 pts.wt. of the polymer of a plasticizer (preferably polyhydric plasticizer) and a surfactant (preferably nonionic surfactant having 7-20 HLB), molded into a film having 10-100mu preferably 20-50mu thickness by casting method and preferably embossed to give a film. A solid detergent is packaged with the film to give a packaged solid detergent.
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公开(公告)号:JPS63191804A
公开(公告)日:1988-08-09
申请号:JP2292787
申请日:1987-02-03
Applicant: KAO CORP
Inventor: KONDO AKIHIRO , IGARASHI TADASHI , TSUSHIMA RIKIO , MATSUI SADA
Abstract: PURPOSE:To continuously produce a (co)polymer of a water-soluble vinyl monomer with good efficiency and controllability, by forming a thin-film flow of an aqueous solution of a water-soluble vinyl monomer and a reductive sulfur- containing oxyacid salt on the inner wall of a reaction cylinder. CONSTITUTION:An aqueous solution of a water-soluble vinyl monomer (e.g., acrylamide) 1 except alpha,beta-unsaturated carboxylic acid monomers and a reductive sulfur-containing oxyacid salt (e.g., sodium hydrogensulfite) 3 is supplied into a reaction cylinder 10 comprising a (double)cylinder from an inlet 12. Simultaneously, an oxygen-containing gas 2 as a parallel flow to the aqueous solution is supplied into the reaction cylinder 10 from an inlet 11 to form a thin film flow of the aqueous monomer solution on the inner wall of the reaction cylinder 10 by a stream of the gas 2 to react. Then, the resulting (co)polymer of the water-soluble vinyl monomer is separated in a gas/liquid separation cooling part 4, cooled, and removed via an aging part 5 and a pH control part 6.
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公开(公告)号:JPS62121705A
公开(公告)日:1987-06-03
申请号:JP26225285
申请日:1985-11-21
Applicant: KAO CORP
Inventor: MATSUI SADA , HIDA HIDETAKA
Abstract: PURPOSE:To obtain a polymer of a narrow MW distribution and less coloration, by concurrently feeding an alpha,beta-unsaturated carboxylic acid monomer, etc., and an inert gas to one end of a reaction pipe to thereby form a stream of a thin film of the monomer on the inside wall of the pipe and reacting the monomer. CONSTITUTION:A monomer essentially consisting of an alpha,beta-unsaturated carboxylic acid (salt) (e.g., acrylic acid), previously prepared in a preparation part 1, is mixed with components which are necessary for the reaction (e.g., sodium hydrogensulfite) and are fed from a feed part 3, and the mixture is fed to a reaction pipe 10 comprising a pipe or a double pipe from its entrance 12. An inert gas, air or an oxygen gas 2 diluted with an inert gas is fed to the reaction pipe 10 from an entrance 11, and a stream of a thin film of the monomer is formed on the inside wall of the reaction pipe 10 by a stream of the gas while it is reacted. The reaction product is withdrawn from the top of the reaction pipe 10 and separated by cooling in a gas/liquid separation part 4 to obtain the purpose carboxylic acid polymer.
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公开(公告)号:JPS5759828A
公开(公告)日:1982-04-10
申请号:JP13548480
申请日:1980-09-29
Applicant: Kao Corp , Kawaken Fine Chem Co Ltd
Inventor: NAKAYAMA MUTSUO , KIMURA AKIO , EGUCHI KEN , MATSUI SADA
IPC: B01J10/00 , B01J19/26 , B01J23/00 , B01J23/44 , C07B61/00 , C07C51/00 , C07C51/235 , C07C59/01 , C07C59/10 , C07C59/105 , C07C59/285 , C07C67/00
CPC classification number: B01J19/26 , C07C51/235 , C07C59/105
Abstract: PURPOSE: To prepare a sugar oxide useful as a cleaning agent of metal or glass surface, concrete additive, pharmaceutical, food additive, etc., in high selectivity and yield, in a short time, by oxidizing a sugar using a specific gas-liquid contact process in the presence of a palladium-carbon catalyst.
CONSTITUTION: A sugar oxide is prepared by contacting an oxygen-containing gas with an alkaline aqueous dispersion obtained by dispersing a palladium-carbon catalyst in an aqueous soution of a sugar, and oxidizing the sugar. In the above process, the aqueous dispersion of the sugar and the palladium-carbon catalyst in the vessel 1 is circulated by the circulation pump 2 and the circulation pipe 3, and the O
2 - containing gas is introduced into the reactor 1 attached to the end of the circulation pipe 3 by the driving force of the circulating liquid, and is sucked through the gas intake port 7 by the injector 4 capable of sucking and mixing the gas by the injection of the circulating liquid and placed in the reactor 1. The O
2 -containing gas is mixed vigorously with the aqueous solution of the sugar containing suspended palladium-carbon catalyst, to effect the oxidation reaction.
COPYRIGHT: (C)1982,JPO&JapioAbstract translation: 目的:通过使用特定的气体液体氧化糖,以高选择性和高产率制备可用作金属或玻璃表面的清洁剂,混凝土添加剂,药物,食品添加剂等的糖氧化物 在钯 - 碳催化剂存在下进行接触。 构成:通过使含氧气体与通过将糖 - 碳催化剂分散在糖的水溶液中而获得的碱性水性分散体和氧化糖来制备糖氧化物。 在上述方法中,容器1中的糖和钯 - 碳催化剂的水分散体通过循环泵2和循环管3循环,将含O 2的气体引入附着在反应器1的反应器1中 通过循环液体的驱动力被循环管3吸入,并且通过喷射器4被吸入口7吸入,喷射器4能够通过注入循环液体吸入和混合气体并放置在反应器1中.O 2 含有气体与含糖悬浮钯 - 碳催化剂的水溶液剧烈混合,进行氧化反应。
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公开(公告)号:JPH06195922A
公开(公告)日:1994-07-15
申请号:JP34729592
申请日:1992-12-25
Applicant: KAO CORP
Inventor: MATSUI SADA , MATSUO YUZO , KOBAYASHI HIDEO , IKEDA HIROSHI
IPC: D04H1/4209 , G11B23/033 , G11B23/50 , D04H1/42
Abstract: PURPOSE:To impart an adequate cushion property to a liner material and to prevent a decrease in a cleaning effect by a liner with lapse of time by incorporating water into this liner material and sticking the liner material to the inner side of a container after drying. CONSTITUTION:Liquid having 50 to 200 deg.C b.p. is incorporated by an impregnating device 2 into the liner material 5 which is a non-woven fabric consisting of rayon fibers and nylon fibers, by which the non-woven fabric treated to contain 0.1% saturation quantity of the water is obtd. This non-woven fabric is stagnated and dried for about 2 seconds in the 120 to 150 deg.C atmosphere of a heating furnace 31, by which the treated non-woven fabric is obtd. The non- woven fabric is blanked to a prescribed shape to form the liner. The liner is ultrasonically welded to the inner side of the container and a magnetic disk is housed therein, by which a disk cartridge is obtd.
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公开(公告)号:JPH062770B2
公开(公告)日:1994-01-12
申请号:JP31801288
申请日:1988-12-16
Applicant: KAO CORP
Inventor: TORIMAE YASUHIRO , MATSUI SADA
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