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    MANUFACTURE OF HIGHLY FUNCTIONAL WATER-ABSORPTIVE RESIN
    1.
    发明专利
    MANUFACTURE OF HIGHLY FUNCTIONAL WATER-ABSORPTIVE RESIN 失效

    公开(公告)号：JPS6036534A

    公开(公告)日：1985-02-25

    申请号：JP14625783

    申请日：1983-08-10

    Applicant: KAO CORP

    Inventor： KOBAYASHI TAKATOSHI ,  YAMAZAKI SEIZOU ,  TSUNODA YUUZOU

    IPC: C08J3/24 ,  C08J3/00 ,  C08J7/04

    Abstract: PURPOSE:To obtain titled resin effectively carrying on its surface highly reactive functional group without any reduction in its water absorptivity, by crosslinking reaction following impregnation of a carboxyl group-contg. resin of specific water content with reactive functional group-contg. hydrophilic monomer. CONSTITUTION:(A) A carboxyl (or carboxylate) group-contg. highly water-absorptive resin with a water content regulated below 50wt% (pref. to 10-40wt%) is impregnated with (B) a reactive functional group-contg. hydrophilic monomer [pref. (meth)acrylamide] followed by crosslinking using a crosslinking agent (pref. polyglycidyl ether) to coat the surface of said resin. The above resin (A) is preferably an acrylic acid (alkali metal salt) (co)polymer prepared by reversed- phase suspension polymerization of an aqueous solution of carboxyl group, etc.- contg. hydrophilic monomer in the presence of water-soluble initiator. USE:As hygienic materials, antisweating agent, phase-transfer catalyst, etc.

    Manufacture of molded article of antistatic polymer
    2.
    发明专利
    Manufacture of molded article of antistatic polymer 失效
    抗静电聚合物成型制品的制造

    公开(公告)号：JPS59117542A

    公开(公告)日：1984-07-06

    申请号：JP22953782

    申请日：1982-12-24

    Applicant: Kao Corp ,  Takeo Saegusa ,  Unitika Ltd

    Inventor： SAEGUSA TAKEO ,  SANO YOSHIYUKI ,  KIMURA YOSHIHARU ,  TSUNODA YUUZOU ,  YAMAZAKI HARUMASA ,  SHINONOME OSAMI ,  TOKUSAWA TAROU

    IPC: C08J7/04 ,  D06M13/02 ,  D06M13/165 ,  D06M101/00 ,  D06M101/16 ,  D06M101/30 ,  D06M101/32

    Abstract: PURPOSE: To impart remarkable antistatic effect and excellent durability to a molded article made of a polyester polymer, by etching the article with an alkaline solution, and treating with a specific polyalkylene oxide compound.
    CONSTITUTION: A molded article made of a polyester or a polymer composition containing a polyester is etched with an alkaline solution and then treated with a polyalkylene oxide cmpound containing at least one epoxy group. The polyester is preferably the one containing 5-alkali metal sulfoisophthalate component or polyalkylene oxide component as a copolymerized component. A molded article of a polymer having polyester and tertiary amine structure is also preferable. The molded article is preferably fiber or film.
    COPYRIGHT: (C)1984,JPO&Japio

    Abstract translation: 目的：通过用碱性溶液蚀刻制品，并用特定的聚环氧烷化合物处理，赋予由聚酯聚合物制成的模制品显着的抗静电效果和优异的耐久性。 构成：用聚酯或含有聚酯的聚合物组合物制成的模制品用碱性溶液蚀刻，然后用含有至少一个环氧基的聚环氧烷烃化处理。 聚酯优选为含有作为共聚成分的5-碱金属磺基间苯二甲酸酯成分或聚环氧烷成分的聚酯。 具有聚酯和叔胺结构的聚合物的成型体也是优选的。 模制品优选是纤维或薄膜。

    PREPARATION OF WATER-ABSORBING MATERIAL HAVING IMPROVED WATER ABSORPTION PROPERTY
    6.
    发明专利
    PREPARATION OF WATER-ABSORBING MATERIAL HAVING IMPROVED WATER ABSORPTION PROPERTY 失效

    公开(公告)号：JPS5832607A

    公开(公告)日：1983-02-25

    申请号：JP13067081

    申请日：1981-08-20

    Applicant: KAO CORP

    Inventor： YAMAZAKI HARUMASA ,  TSUNODA YUUZOU ,  HARADA SHIYOUICHIROU

    IPC: C08F2/00 ,  A61L15/60 ,  C08F2/32 ,  C08F20/00 ,  C08F20/02 ,  C08F220/00 ,  C08F220/04

    Abstract: PURPOSE:In polymerizing an aqueous solution of a water-soluble ethylenic unsaturated monomer, to obtain a water-absorbing material useful as a water- retaining agent for agriculture, sanitary material, etc., having improved water- absorbing rate for a salt solution or the blood, by adding a surface active agent to the polymerization system during polymerization or after polymerization. CONSTITUTION:An aqueous solution of a water-soluble ethylenic unsaturated monomer (e.g., acrylic acid, etc.) is dispersed or suspended in a hydrocarbon or a halogenated hydrocarbon in the presence of an oil-soluble cellulose or cellulose ester, and polymerized with a water-soluble radical polymerization initiator. In the polymerization, an aqueous and/or water-dispersed surface active agent (preferably nonionic surface active agent and anionic surface active agent having >=7; HLB polyoxyethylene alkyl ether, sodium oleate, etc.) is added to the polymerization system during polymerization or after polymerization, to give a water-absorbing material having improved water absorption properties.

    PREPARATION OF CROSSLINKED AMPHOLYTIC POLYMER
    7.
    发明专利
    PREPARATION OF CROSSLINKED AMPHOLYTIC POLYMER 失效

    公开(公告)号：JPS5813609A

    公开(公告)日：1983-01-26

    申请号：JP11257581

    申请日：1981-07-17

    Applicant: KAO CORP

    Inventor： TSUSHIMA RIKIO ,  TSUNODA YUUZOU

    IPC: C08F20/00 ,  C08F20/34 ,  C08F20/52 ,  C08F220/34 ,  C08F220/60

    Abstract: PURPOSE:To obtain the titled polymer capable of dispersing a water-insoluble solid fine particle substance stably independtly of pH and the presence or absence of soluble salts, by copolymerizing a mixture of an ampholytic monomer with a crosslinkable monomer in the presence of a radical polymerization initiator. CONSTITUTION:95-99.99mol% ampholytic monomer[e.g., 3-dimethyl(acryloxyethyl)ammonium ethanecarboxylate, etc.]shown by the formula (R1, R4 and R5 are H or merhyl; R2 and R3 are methyl or ethyl; A is -O- or -NH-; X is -CO2-, -SO3, -PHO3; m and n=1-3) is copolymerized with 0.01-5mol% crosslinkable monomer (e.g., methylene bisacrylamide, etc.) in the presence of about 0.01- 5wt% radical polymerization initiator (e.g., sodium persulfate, etc.) at 20-120 deg.C (preferably at 35-80 deg.C), to give the desired copolymer. USE:A viscosity builder, dispersant, etc. for perfume, cosmetic, drug, emulsion etc.

    Production of water-soluble bead polymer
    8.
    发明专利
    Production of water-soluble bead polymer 失效
    生产水溶性珠粒聚合物

    公开(公告)号：JPS5774309A

    公开(公告)日：1982-05-10

    申请号：JP15045480

    申请日：1980-10-27

    Applicant: Kao Corp

    Inventor： YAMAZAKI HARUMASA ,  FUKUZAKI HIROSHI ,  TSUNODA YUUZOU

    IPC: C08F2/00 ,  C08F2/20 ,  C08F2/32 ,  C08F10/02

    Abstract: PURPOSE: To prevent a phenomenon of formation of films on the wall or a like area of a polymerization vessel, by using a specified copolymer as a protective colloid in the production of the title polymer by subjecting an aqueous solution of an ethylenically unsaturated monomer to a reversed phase suspension polymerization.
    CONSTITUTION: A water-soluble bead polymer is produced by subjecting an aqueous solution of an ethylenically unsaturated monomer, e.g., methacrylic acid or acrylamide, to a reversed phase suspension polymerization using a water-soluble radical polymerization initiator such as potassium persulfate, in an unpolymerizable hydrophobic liquid, e.g., hexane. In this polymerization, a phenomenon of formation of films on the wall or a like area of a polymerization vessel is prevented by using, as a protective colloid, a copolymer of a 16W60C α-olefin and an α, β- unsaturated carboxylic acid anhydride, .g., maleic anhydride or itaconic anhydride, or a derivative of the copolymer, e.g., partially esterified product or partially amidated product.
    COPYRIGHT: (C)1982,JPO&Japio

    Abstract translation: 目的：为了防止在聚合容器的壁或类似区域上形成膜的现象，通过在制备标题聚合物中使用指定的共聚物作为保护胶体，使烯键式不饱和单体的水溶液 反相悬浮聚合。 构成：水溶性珠粒聚合物是通过将烯键式不饱和单体（例如甲基丙烯酸或丙烯酰胺）的水溶液以不可聚合的水溶性自由基聚合引发剂如过硫酸钾的水溶性自由基聚合引发剂 疏水性液体，例如己烷。 在该聚合中，通过使用16-60℃的α-烯烃与α，β-不饱和羧酸的共聚物作为保护胶体来防止在聚合容器的壁或类似区域上形成膜的现象 酸酐，例如马来酸酐或衣康酸酐，或共聚物的衍生物，例如部分酯化产物或部分酰化产物。

    PREPARATION OF HIGHLY WATER ABSORBING POLYMER
    10.
    发明专利
    PREPARATION OF HIGHLY WATER ABSORBING POLYMER 失效

    公开(公告)号：JPS60186506A

    公开(公告)日：1985-09-24

    申请号：JP4172784

    申请日：1984-03-05

    Applicant: KAO CORP

    Inventor： KOBAYASHI TAKATOSHI ,  YAMAZAKI HARUMASA ,  SAKURAI AKIRA ,  ITOU OSAMU ,  TSUNODA YUUZOU

    IPC: A61F13/53 ,  A61F13/15 ,  A61F13/472 ,  A61F13/49 ,  A61L15/60 ,  C08F2/00 ,  C08F2/32 ,  C08F8/00 ,  C08F20/02 ,  C08F120/04 ,  C08G59/00 ,  C08G59/40 ,  C08L33/00 ,  C08L33/02 ,  C08L63/00

    Abstract: PURPOSE:To obtain the titled polymer, having improved salt resistance and high water absorption rate, and useful for sanitary materials, etc., by dispersing or suspending an aqueous solution containing a carboxyl group-containing monomer in a hydrocarbon, etc. in the presence of an oil-soluble cellulose ester, etc., polymerizing the monomer, adjusting the water content, and crosslinking the resultant polymer. CONSTITUTION:An aqueous solution of a carboxyl group-containing water-soluble ethylenically unsaturated monomer, e.g. acrylic acid, is dispersed or suspended in a hydrocarbon, e.g. cyclohexane, or a halogenated aromatic hydrocarbon, and polymerized. In the process, a cellulose ester, e.g. cellulose acetate, or cellulose ether, e.g. ethyl cellulose, which is soluble in oil at the polymerization temperature is used as a protective colloid, and the water content is adjusted to 10-40wt% after the polymerization. The resultant polymer is then crosslinked with a crosslinking agent, e.g. ethylene glycol diglycidyl ether, having two or more functional groups reactive with carboxyl groups or carboxylate groups to give the aimed polymer.

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