公开(公告)号：WO1998006007A1

公开(公告)日：1998-02-12

申请号：PCT/US1997013677

申请日：1997-08-01

Applicant: LOCTITE (IRELAND) LIMITED ,  LOCTITE CORPORATION ,  MCARDLE, Ciaran, B. ,  BURKE, Joseph ,  WELCH, Edward, K.

Inventor： LOCTITE (IRELAND) LIMITED ,  LOCTITE CORPORATION

IPC: G03F07/00

CPC classification number: H05K3/323 ,  G03F7/34 ,  H01L2224/293 ,  H01L2924/01019 ,  H01L2924/01079 ,  H01L2924/07811 ,  H01L2924/10253 ,  H01R4/04 ,  H05K2201/083 ,  H05K2201/09945 ,  H05K2203/0769 ,  H05K2203/104 ,  Y10T428/26 ,  H01L2924/00

Abstract: The present invention provides a number of interrelated methods for the production of random and ordered arrays of particles and recesses, as well as films containing such arrays and recesses. The present invention also relates to the random and ordered arrays of particles and films prepared therefrom. The ordered arrays are obtained by the use of ferrofluid compositions which may be curable, solidifiable or non-curing/non-solidifiable. The arrays and films may contain electrically-conductive particles useful in electronic applications for effecting contact between leads or pads.

Abstract translation: 本发明提供了许多用于生产颗粒和凹槽的随机和有序排列的相关方法，以及含有这种阵列和凹槽的膜。 本发明还涉及由其制备的颗粒和膜的随机和有序阵列。 有序阵列通过使用可固化，可固化或不固化/不可固化的铁磁流体组合物获得。 阵列和膜可以包含可用于电子应用中的导电颗粒，以实现引线或焊盘之间的接触。

公开(公告)号：WO1995000869A1

公开(公告)日：1995-01-05

申请号：PCT/US1994007061

申请日：1994-06-22

Applicant: LOCTITE CORPORATION

Inventor： LOCTITE CORPORATION ,  WOODS, John, G. ,  RAKAS, Margaret, A. ,  JACOBINE, Anthony, F. ,  ALBERINO, Louis, M. ,  KROPP, Philip, L. ,  SUTKAITIS, Donna, M. ,  GLASER, David, M. ,  NAKOS, Steven, T.

IPC: G02B06/00

CPC classification number: G02B6/443 ,  B29C64/135 ,  C03C25/106 ,  C07D263/42 ,  C08F6/02 ,  C08G65/332 ,  C08G73/028 ,  C08G75/045 ,  C08G75/12 ,  C09D4/00 ,  G03F7/0037 ,  G03F7/0275 ,  Y10T428/2938 ,  C08F232/00

Abstract: A curable thiol-ene composition specially adapted for use as a primary coating on optical fibers comprises a polythiol and a compound having a plurality of norbornene groups thereon, are characterized in that one of either the compound having the plurality of norbornene groups or the polythiol has a backbone of a poly(tetramethylene oxide), or is an oligomer thereof, and the poly(tetramethylene oxide) has a molecular weight of between 250 and 5,000. The formulations are relatively low viscosity liquids at practical application temperatures and cure substantially completely with very low irradiation fluence. The formulations cure in ambient air. There is no need to exclude oxygen or to control humidity. The formulations of the invention can be cured using low intensity UV lamps which do not generate significant amounts of heat. The cured products have excellent low temperature flexibility, good humidity and water absorbtion resistance and good thermal oxidative stability. The formulations may be applied to optical fibers using conventional techniques and cured with UV-vis or EB irradiation.

Abstract translation: 特别适用于光纤上的初级涂层的可固化硫醇烯组合物包括多硫醇和其上具有多个降冰片烯基团的化合物，其特征在于具有多个降冰片烯基团的化合物或多硫醇中的一种具有 聚（四氢呋喃）氧化物的骨架或其低聚物，聚（四氢呋喃）的分子量为250-5,000。 制剂在实际应用温度下是相对低粘度的液体，并且以非常低的照射能量密度完全固化。 配方在环境空气中固化。 不需要排除氧气或控制湿度。 本发明的配方可以使用不产生大量热量的低强度UV灯来固化。 固化产物具有优异的低温柔韧性，良好的湿度和吸水性，良好的热氧化稳定性。 可以使用常规技术将制剂施用于光纤，并用UV-vis或EB辐照固化。

公开(公告)号：WO1992002306A1

公开(公告)日：1992-02-20

申请号：PCT/EP1991001372

申请日：1991-07-23

Applicant: LOCTITE CORPORATION ,  NKE S.R.L. ,  FIGINI, Aldo ,  BEYLIS, Renato

Inventor： LOCTITE CORPORATION ,  NKE S.R.L.

IPC: B05C11/10

CPC classification number: F04B43/1292 ,  B01D19/0036 ,  B05C11/10 ,  B05C11/1036

Abstract: The invention relates to a dispensing process particularly for a sealing/adhesive product (14) which comprises at least one step of pumping the sealing/adhesive product to allow a step of distribution thereof onto at least one part to be sealed, such as for example a motor-vehicle mechanical component (5), an intermediate step of deaeration of the sealing/adhesive product, so as to optimize its distribution on the part to be sealed, is provided between the pumping step and the distribution step. The apparatus for dispensing the sealing/adhesive product (14) comprises elements (2) for feeding the sealing/adhesive product to elements (4) for distributing it onto at least one part (5) to be sealed and sealing/adhesive product deaeration means (3) which cooperate with the pumping and distribution elements for the uniform deposition of the sealant/adhesive on the part.

Abstract translation: 本发明涉及一种特别用于密封/粘合剂产品（14）的分配方法，其包括至少一个步骤，泵送密封/粘合剂产品以允许将其分配到至少一个待密封部件上的步骤，例如 在泵送步骤和分配步骤之间提供机动车辆机械部件（5），密封/粘合产品的脱气的中间步骤，以便优化其在待密封部件上的分布。 用于分配密封/粘合剂产品（14）的装置包括用于将密封/粘合产品供给到元件（4）的元件（2），用于将其分配到要密封的至少一个部分（5）上，并且密封/粘合产品脱气装置 （3），其与泵送和分配元件协作以使密封剂/粘合剂均匀地沉积在部件上。

公开(公告)号：WO1989007623A1

公开(公告)日：1989-08-24

申请号：PCT/US1989000527

申请日：1989-02-09

Applicant: LOCTITE CORPORATION

Inventor： LOCTITE CORPORATION ,  BLAIN, Stephen, E.

IPC: C08K05/05

CPC classification number: C08F2/44 ,  C09J4/00 ,  C08F222/1006

Abstract: Polymerizable compositions comprising a liquid polymerizable continuous phase and a non-liquid, non-polymerizable dispersed discontinuous phase are stabilized agents density drift of the discontinuous phase by forming in-situ, throughout and within said polymerizable composition a crystalline matrix of sufficient density to effectively inhibit density drift.

Abstract translation: 包含液体可聚合连续相和非液体不可聚合分散的不连续相的可聚合组合是通过在所述可聚合组合物内部以及在所述可聚合组合物内原位形成具有足够密度的结晶基质以有效抑制的稳定剂的不连续相的密度漂移 密度漂移。

公开(公告)号：WO1985001947A1

公开(公告)日：1985-05-09

申请号：PCT/US1984001719

申请日：1984-10-23

Applicant: LOCTITE CORPORATION

Inventor： LOCTITE CORPORATION ,  WOODS, John ,  CASEY, Tadhg, Eisirt

IPC: C08L63/10

CPC classification number: G03F7/029 ,  C08F283/10 ,  C08G59/68 ,  C08F220/12

Abstract: A photocurable composition comprises (a) a (meth)acrylate functional monomer or prepolymer; (b) a cationically curable monomer or prepolymer; (c) a free-radical liberating, carbonyl containing, photoinitiator; and (d) an aromatic halonium salt whose anion is a complex metal halide. The composition solves difficulties in curing found in previous formulations and provides complete curing in air, thereby preventing tacky surfaces, as well as an accelerated cure rate and a more penetrating cure depth. Blending with between about 10% and 20% of a carboxyl-terminated nitrile rubber results in a composition suitable for bonding polybutyleneterephthalate.

Abstract translation: 光固化组合物包含（a）（甲基）丙烯酸酯官能单体或预聚物; （b）阳离子可固化的单体或预聚物; （c）自由基释放，含羰基的光引发剂; 和（d）阴离子是复合金属卤化物的芳族卤化盐。 该组合物解决了先前制剂中发现的固化困难，并且在空气中提供完全固化，从而防止粘性表面，以及加速的固化速率和更渗透的固化深度。 与约10％至20％的羧基封端的丁腈橡胶混合导致适用于粘合聚对苯二甲酸丁二酯的组合物。

公开(公告)号：WO1998014487A1

公开(公告)日：1998-04-09

申请号：PCT/US1997017463

申请日：1997-09-30

Applicant: LOCTITE CORPORATION

Inventor： LOCTITE CORPORATION

IPC: C08F08/02

CPC classification number: C08F8/02 ,  C08F12/24

Abstract: Cationically cureable adhesives and sealants with increased viscosities and improved rheological control and good storage stability are prepared using a cationically cureable monomer and a thickening polymer which is the alkylation reaction product of poly(4-hydroxystyrene) or poly(2-hydroxystyrene) with a compound RX where R is allyl, methallyl, crotyl or prenyl and X is Cl, Br or I. The cationically cureable monomer suitably includes at least one alkenyloxystyrene monomer. Such thickened adhesives are useful as edge sealants for flat panel display devices. A-stage curing of the adhesive with UV irradiation allows for near ambient temperature fixturing of the device assemblies and B-stage thermal curing of the adhesive can be conducted at much lower temperatures than are needed for glass frit sealants. The B-stage cured products have thermal resistance, outgassing and substrate adhesion properties adequate for flat panel display devices.

Abstract translation: 使用阳离子可固化单体和增稠聚合物制备具有增加的粘度和改善的流变控制和良好的储存稳定性的可阳离子可固化的粘合剂和密封剂，其是聚（4-羟基苯乙烯）或聚（2-羟基苯乙烯）与化合物的烷基化反应产物 RX，其中R是烯丙基，甲代烯丙基，巴豆基或异戊烯基，X是Cl，Br或I.可阳离子固化的单体适当地包括至少一种烯氧基苯乙烯单体。 这种增稠粘合剂可用作平板显示装置的边缘密封剂。 使用紫外线照射进行A级固化的粘合剂允许器件组件接近环境温度固定，粘合剂的B阶段热固化可在比玻璃料密封剂所需的温度低得多的温度下进行。 B阶固化产品具有适用于平板显示装置的耐热性，除气和基材粘合性能。

公开(公告)号：WO1995024356A1

公开(公告)日：1995-09-14

申请号：PCT/US1995002566

申请日：1995-03-01

Applicant: LOCTITE CORPORATION

Inventor： LOCTITE CORPORATION ,  MONTENIERI, Robert, E. ,  O'CONNELL, Maurice, T. ,  CRAMPTON, Alan, T. ,  SEYMOUR, Geoffrey, F. ,  EDSTROM, Richard, C. ,  BOURGEOIS, Bryon, J.

IPC: B67D47/00

CPC classification number: B65D50/06 ,  B65D11/04 ,  B65D11/20 ,  B65D41/0471 ,  B65D47/12 ,  B65D47/18 ,  B65D2251/065 ,  B65D2501/0081

Abstract: A package (10), with a nozzle (25), a chamber (35), a cap (15) which fits over the nozzle, and a pin (40) attached to the interior of the cap which fits into the opening (24) of the nozzle, for storing and dispensing a liquid, having an improved closure mechanism comprising at least one rectangular stopping member (55, 56) and at least one rectangular band (58) in the interior of the cap and at least one guide flange (29) on the nozzle. The package also has a plurality of guide ribs (26) located around the nozzle to aid in the proper placement of the cap. The package is designed to be leak proof, nonclogging, able to dispense the liquid precisely, and can be easily opened even when the pin has bonded to the opening of the nozzle without breaking or shearing the pin.

Abstract translation: 具有喷嘴（25）的封装（10），安装在喷嘴上方的腔室（35），盖子（15）以及安装在盖子的内部的销钉（40） ），用于存储和分配液体，其具有改进的封闭机构，该封闭机构包括至少一个矩形止动构件（55,56）和至少一个矩形带（58），并且至少一个导向凸缘 （29）在喷嘴上。 该包装还具有多个位于喷嘴周围的引导肋（26），以帮助盖的正确放置。 该包装被设计为防漏，不堵塞，能够精确地分配液体，即使当销已经结合到喷嘴的开口而不破坏或剪切销时也可以容易地打开。

公开(公告)号：WO1992017408A1

公开(公告)日：1992-10-15

申请号：PCT/JP1992000380

申请日：1992-03-27

Applicant: LOCTITE CORPORATION ,  YASUDA, Tohru

Inventor： LOCTITE CORPORATION

IPC: C02F01/44

CPC classification number: C02F1/444 ,  B01D61/145 ,  B01D61/147 ,  B01D61/16 ,  B01D2311/04 ,  C10M175/06

Abstract: A process for treating waste washing water, which is only slightly affected by the temperature and can dispense with any chemical and wherein the quality of treated water is not affected by a change in the waste water concentration. The process comprises conducting impregnation with an impregnant having a composition comprising triethylene glycol dimethacrylate, 2-hydroxyethyl methacrylate, lauryl methacrylate, nonionic surfactant and azobisisobutyronitrile, separating the impregnant thereafter, washing the surface of an impregnated article with water, and treating the waste water with a liquid obtained by filtering the liquid having the above composition though a filter having a retained particle diameter of 20 mu m or less.

Abstract translation: 一种处理废水清洗水的方法，其仅受温度的稍微影响，并且可以省去任何化学品，其中处理水的质量不受废水浓度变化的影响。 该方法包括用具有三甘醇二甲基丙烯酸酯，甲基丙烯酸2-羟乙酯，甲基丙烯酸月桂酯，非离子表面活性剂和偶氮二异丁腈的组合物的浸渍剂进行浸渍，然后用水分离浸渍剂，用水洗涤浸渍制品的表面，并用 通过过滤具有上述组成的液体而获得的液体通过保留粒径为20μm或更小的过滤器。

公开(公告)号：WO1989006666A1

公开(公告)日：1989-07-27

申请号：PCT/US1989000061

申请日：1989-01-09

Applicant: LOCTITE CORPORATION

Inventor： LOCTITE CORPORATION ,  CLARK, Paul, J. ,  JACOBINE, Anthony, F. ,  GLASER, David, M.

IPC: C08G75/04

CPC classification number: C08G75/045 ,  C08G75/12

Abstract: Compounds useful as adhesion promoters for thermally cured thiolene adhesives include (a) acrylic or norbornene acid phosphate esters such as (I) and (II); b) maleic, acrylic, methacrylic, norbornene dicarboxylic, and fumaric acids and half acid esters and peresters of maleic fumaric and norbornene dicarboxylic acids; and c) norbornene, acrylic or methacrylic silanes having two or three hydrolyzable groups bound to the silicon atom thereof, such as 5-(triacetoxysilyl)norbornene. The adhesion promoters may be employed as surface primers for conventional thiolene compositions. Alternatively the thiolene compositions themselves may be modified by addition of 0.1 to 10 % by weight of the adhesion promoter. Preferred thiolene compositions employ norbornene functional ene ingredients.

Abstract translation: 可用作热固化硫醇粘合剂的粘合促进剂的化合物包括（a）丙烯酸或降冰片烯酸性磷酸酯如（I）和（II）; b）马来酸，丙烯酸，甲基丙烯酸，降冰片烯二羧酸和马来酸富马酸和降冰片烯二羧酸的富马酸和半酸酯和过酸酯; 和c）具有两个或三个与其硅原子结合的可水解基团的降冰片烯，丙烯酸或甲基丙烯酸硅烷如5-（三乙酰氧基甲硅烷基）降冰片烯。 粘合促进剂可用作常规硫羟组合物的表面引物。 或者，硫醇组合物本身可以通过加入0.1至10重量％的粘合促进剂来改性。 优选的硫醇组合物采用降冰片烯功能烯成分。

公开(公告)号：WO1988002902A2

公开(公告)日：1988-04-21

申请号：PCT/US1987002618

申请日：1987-10-13

Applicant: LOCTITE CORPORATION

Inventor： LOCTITE CORPORATION ,  STEINKRAUS, Walter, J. ,  ROONEY, John, M. ,  GLASER, David, M. ,  WOODS, John ,  JACOBINE, Anthony, F.

IPC: G08G75/04

CPC classification number: C08G75/045 ,  C08G75/12

Abstract: A curable thiol-ene formulation comprising: a) a polythiol, b) a 'ene compound having a plurality of groups of formula (I), where Q is CH2, CHCH3, C(CH3)2, O, S, NR or SO2, R is H or alkyl, and m is 0-10, and c) an effective amount of a free radical initiator.

Abstract translation: 一种可固化的硫醇烯制剂，其包含：a）多硫醇，b）具有多个式（I）的基团的烯化合物，其中Q是CH 2，CHCH 3，C（CH 3）2，O，S，NR 1 >或SO 2，R 1是H或烷基，m是0-10，和c）有效量的自由基引发剂。