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公开(公告)号:SG10201607435RA
公开(公告)日:2016-10-28
申请号:SG10201607435R
申请日:2013-02-06
Applicant: LUBRIZOL CORP
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公开(公告)号:CA2863950A1
公开(公告)日:2013-08-15
申请号:CA2863950
申请日:2013-02-06
Applicant: LUBRIZOL CORP
Inventor: WALKER GARY M , SOWERBY ROGER L , ROSKI JAMES P , PARSONS ROGER L , FRIEND CHRISTOPHER L , GRANGE ANDRE , CIOLLI CHRISTOPHER J , FAHMY MOHAMED G , PERERA JAYASOORIYA
IPC: C07G99/00 , C10M135/02 , C10M159/22
Abstract: A sulfurized alkaline earth metal (e.g., calcium) dodecylphenate is prepared by reacting (i) dodecylphenol with (ii) calcium hydroxide or calcium oxide in an amount of about 0.3 to about 0.7 moles per mole of dodecylphenol charged and (iii) an alkylene glycol in an amount of about 0.13 to about 0.6 moles per mole of dodecylphenol charged; and reacting the product of the first step with sulfur in an amount of about 1.6 to about 3 moles per mole of dodecylphenol charged; and thereafter optionally reacting the product with additional calcium hydroxide or calcium oxide and with carbon dioxide so as to form an overbased phenate. The product thus prepared has reduced levels of monomeric dodecylphenol.
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公开(公告)号:CA2863950C
公开(公告)日:2022-06-07
申请号:CA2863950
申请日:2013-02-06
Applicant: LUBRIZOL CORP
Inventor: WALKER GARY M , SOWERBY ROGER L , ROSKI JAMES P , PARSONS ROGER L , FRIEND CHRISTOPHER L , GRANGE ANDRE , CIOLLI CHRISTOPHER J , FAHMY MOHAMED G , PERERA JAYASOORIYA
IPC: C07G99/00 , C10M135/02 , C10M159/22
Abstract: A sulfurized alkaline earth metal (e.g., calcium) dodecylphenate is prepared by reacting (i) dodecylphenol with (ii) calcium hydroxide or calcium oxide in an amount of about 0.3 to about 0.7 moles per mole of dodecylphenol charged and (iii) an alkylene glycol in an amount of about 0.13 to about 0.6 moles per mole of dodecylphenol charged; and reacting the product of the first step with sulfur in an amount of about 1.6 to about 3 moles per mole of dodecylphenol charged; and thereafter optionally reacting the product with additional calcium hydroxide or calcium oxide and with carbon dioxide so as to form an overbased phenate. The product thus prepared has reduced levels of monomeric dodecylphenol.
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公开(公告)号:IN7290DEN2014A
公开(公告)日:2015-04-24
申请号:IN7290DEN2014
申请日:2014-08-29
Applicant: LUBRIZOL CORP
Inventor: WALKER GARY M , SOWERBY ROGER L , ROSKI JAMES P , PARSONS ROGER L , FRIEND CHRISTOPHER L , GRANGE ANDRE , CIOLLI CHRISTOPHER J , FAHMY MOHAMED G , PERERA JAYASOORIYA
IPC: C07G99/00 , C10M135/02 , C10M159/22
Abstract: A sulfurized alkaline earth metal (e.g. calcium) dodecylphenate is prepared by reacting (i) dodecylphenol with (ii) calcium hydroxide or calcium oxide in an amount of about 0.3 to about 0.7 moles per mole of dodecylphenol charged and (iii) an alkylene glycol in an amount of about 0.13 to about 0.6 moles per mole of dodecylphenol charged; and reacting the product of the first step with sulfur in an amount of about 1.6 to about 3 moles per mole of dodecylphenol charged; and thereafter optionally reacting the product with additional calcium hydroxide or calcium oxide and with carbon dioxide so as to form an overbased phenate. The product thus prepared has reduced levels of monomeric dodecylphenol.
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公开(公告)号:SG11201404656RA
公开(公告)日:2014-09-26
申请号:SG11201404656R
申请日:2013-02-06
Applicant: LUBRIZOL CORP , WALKER GARY M , SOWERBY ROGER L , ROSKI JAMES P , PARSONS ROGER L , FRIEND CHRISTOPHER L , GRANGE ANDRE , CIOLLI CHRISTOPHER J , FAHMY MOHAMED G , PERERA JAYASOORIYA
Inventor: WALKER GARY M , SOWERBY ROGER L , ROSKI JAMES P , PARSONS ROGER L , FRIEND CHRISTOPHER L , GRANGE ANDRE , CIOLLI CHRISTOPHER J , FAHMY MOHAMED G , PERERA JAYASOORIYA
IPC: C07G99/00 , C10M135/02 , C10M159/22
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