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公开(公告)号:KR860001885B1
公开(公告)日:1986-10-24
申请号:KR820002182
申请日:1982-05-19
Applicant: MITSUI TOATSU CHEMICALS
Inventor: MITA RYUICHI , HIKUCHI CHOJIRO , GAWASHIMA NOBUYUKI , KAWASHIMA NOBUHIRO
IPC: C07C227/14 , C07C101/30
Abstract: Compds. of the formula (I) [R1,R2=H, CH3, (un)substd. Ph. or pyridyl! were prepd. Thus, 160 ml of aq. soln. of 12.9 g 3-methylaziridine-2- carbonylethylester were subjected over cationexchange resin, Lewatit S-100(H-type) (Bayer Co.), washed with 60 ml distd. H2O and absorbed on the resin. The resin was heated 7 h at 80-85 ≦̸C in 100 ml of flask, packed on column, and eluted was concd. and dried to yield 11.4 g threonine(Yield 88.6%, Purity 92.5%).