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公开(公告)号:JPH03146606A
公开(公告)日:1991-06-21
申请号:JP28427089
申请日:1989-10-31
Applicant: WATANABE RYUZO , KAWASAKI AKIRA , NAT AEROSPACE LAB , ISHIKAWAJIMA HARIMA HEAVY IND
Inventor: WATANABE RYUZO , KAWASAKI AKIRA , SHINNO MASAYUKI , YUKI MASAHIRO , MURAYAMA TOSHIICHI , IRISAWA TOSHIO
Abstract: PURPOSE:To easily manufacture a gradated functional material constituted with intermediate layer continuously varying composition thereof by repeatedly executing heating and sintering process, in which powder is arranged on surface of a base material and irradiated with laser beam, at the suitable sintering temp. according to the composition of each arranged powder. CONSTITUTION:For example, at the time of manufacturing the gradated functional material, in which the front face is ceramic 11 and the back face is metal 12 and the intermediate layer is continuously varied with these compositions, at first, the base material 13, which can be separated with the metal 12, is prepared. The metal powder 14 is thinly arranged on this base material 13 with a nozzle 15 and irradiated with the laser beam 16 and heated and sintered at the suitable sintering temp. of the metal powder 14 to form sintered layer having 100% metal. Successively, the powder mixing the ceramic powder 13 into the metal powder 14 on the sintered layer is arranged with the nozzle 15 and heated and sintered at the suitable temp. with the laser beam 16. The operation is repeatedly executed while gradually increasing the mixed rate of ceramic powder 21 and finally, the sintered layer having 100% ceramic is formed. By this method, the gradated functional material composed of the ceramic 11 at the first face and the metal 12 at the back face is easily obtd.
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公开(公告)号:JPH03146607A
公开(公告)日:1991-06-21
申请号:JP28426889
申请日:1989-10-31
Applicant: WATANABE RYUZO , KAWASAKI AKIRA , NAT AEROSPACE LAB , ISHIKAWAJIMA HARIMA HEAVY IND
Inventor: WATANABE RYUZO , KAWASAKI AKIRA , SHINNO MASAYUKI , YUKI MASAHIRO , MURAYAMA TOSHIICHI , IRISAWA TOSHIO
Abstract: PURPOSE:To enable joining with the wall-known welding method by varying composition to joining end direction in a material and allowing the most outer end part to be a weldable composition. CONSTITUTION:Raw material powder 31 of ceramic 12, raw material powder 32 of metal 13 and binder 33 are prepared and composition ratio is adjusted with each composition ratio control valve 34, and they are mixed with a mixing nozzle 35 and injected and filled up into a metallic mold 36. Then, the metallic mold 36 is shifted to X-Y direction and they are filled up so that the front face 11a is the ceramic 12 and the back face 11b and the joining end part 11c are the metal 13 and the composition toward the end part 11c from the center part continuously varies in binary condition, and pressurized and formed to the prescribed shape to make the gradated functional material 11. Successively, the material 11 is heated under the condition of giving the temp. gradation corresponding to the gradation of composition in the raw material powder by using a device combining a sintering furnace and laser beam heating device for uniform heating and held to the sintering temp. for each composition. By this method, the metal 13 having 100% at the joining end part 11c is obtd. and the metal- made structural materials can be joined respectively.
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公开(公告)号:JPH03146603A
公开(公告)日:1991-06-21
申请号:JP28426989
申请日:1989-10-31
Applicant: WATANABE RYUZO , KAWASAKI AKIRA , NAT AEROSPACE LAB , ISHIKAWAJIMA HARIMA HEAVY IND
Inventor: WATANABE RYUZO , KAWASAKI AKIRA , SHINNO MASAYUKI , YUKI MASAHIRO , MURAYAMA TOSHIICHI , IRISAWA TOSHIO
Abstract: PURPOSE:To manufacture a gradated functional material having different property at the front and the back by heating the surface of a powder green compact with laser beam after heating it near to starting temp. of sintering, cooling the back face and sintering while giving temp. gradation. CONSTITUTION:For example, the powder green compact W composed of ceramic on the front face and metal on the back face, is set on a cooling device 25 in a sintering furnace 13 and the inner part of the furnace is made to an inert gas atmosphere with a vacuum suction device 18 and gas introducing hole 19. Successively, after uniformly heating in the sintering furnace 13 near to the starting temp. of sintering to the powder green compact W with an electric heating device 11, the powder green compact W is irradiated with the laser beam in a laser beam heating device 22 through a laser beam irradiating aperture 21 to heat the surface thereof. Simultaneously, cooling gas is supplied from a cooling device 25 to cool the back face of powder green compact W, and the sintering is executed under the condition of existence of the temp. inclination between the front and the back. By this method, as coming from the front face to the back face, the gradated functional material continuously varying the property at atomic and molecular level, is obtd.
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公开(公告)号:JPS62156938A
公开(公告)日:1987-07-11
申请号:JP29704285
申请日:1985-12-28
Applicant: NAT AEROSPACE LAB , HIRAI TOSHIO , WATANABE RYUZO , DAIKIN IND LTD , SUMITOMO ELECTRIC INDUSTRIES
Inventor: SHINNO MASAYUKI , SUZUKI AKIO , HIRAI TOSHIO , WATANABE RYUZO , HIRANO TORU , KUROISHI ATSUSHI
IPC: B32B18/00 , B22F3/11 , B22F7/02 , B32B7/04 , B32B15/04 , C23C4/02 , C23C4/06 , C23C14/02 , C23C14/06 , C23C14/22 , C23C16/02 , C23C16/30 , C23C16/44
Abstract: The present invention relates to a method of producing a functionally gradient material whose components and structure are continuously adjusted by the coating, plating and powder metallurgy techniques to change its function in turn and provides a method of producing a functionally gradient material superior in heat-resistance, corrosion-reistance and resistance to thermal fatigue by distributing a third component having a lower Young's modulus or formed of high-strength material sufficiently durable to the fracture strength among ceramics as a first component and metals or other ceramics as a second component to change the function.
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公开(公告)号:DE3679975D1
公开(公告)日:1991-08-01
申请号:DE3679975
申请日:1986-12-23
Applicant: NAT AEROSPACE LAB , HIRAI TOSHIO , WATANABE RYUZO , DAIKIN IND LTD , SUMITOMO ELECTRIC INDUSTRIES
Inventor: NIINO MASAYUKI , SUZUKI AKIO , NIRAI TOSHIO , WATANABE RYUZO , HIRANO TOHRU , KUROISHI NOBUHITO
IPC: B32B18/00 , B22F3/11 , B22F7/02 , B32B7/04 , B32B15/04 , C23C4/02 , C23C4/06 , C23C14/02 , C23C14/06 , C23C14/22 , C23C16/02 , C23C16/30 , C23C16/44 , C23C4/12
Abstract: The present invention relates to a method of producing a functionally gradient material whose components and structure are continuously adjusted by the coating, plating and powder metallurgy techniques to change its function in turn and provides a method of producing a functionally gradient material superior in heat-resistance, corrosion-reistance and resistance to thermal fatigue by distributing a third component having a lower Young's modulus or formed of high-strength material sufficiently durable to the fracture strength among ceramics as a first component and metals or other ceramics as a second component to change the function.
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公开(公告)号:DE3320556A1
公开(公告)日:1983-12-08
申请号:DE3320556
申请日:1983-06-07
Applicant: NAT AEROSPACE LAB
Inventor: NIINO MASAYUKI , YATSUYANAGI NOBUYUKI , KUMAKAWA AKINAGA , SUZUKI AKIO , GOMI HIROMI , SAKAMOTO HIROSHI , SASAKI MASAKI , MASUDA YOSHIMICHI , WATANABE RYUZO , TAKEKAWA JUN JIRO , OHTSUKI ETSUO , ISAGO TERASHI
Abstract: In the cooling wall of a regenerative cooling rocket combustion chamber, the throat portion thereof in which the heat load is highest is formed of a porous material having a perspiring cooling action. The other portion in which the heat load is relatively low is designed to be cooled by conventional forced convection. By such a composite cooling system, a high cooling effect is provided and yet the pressure loss in the cooling passages is small and light weight and long life of the engine are attained concurrently.
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公开(公告)号:DE3320557A1
公开(公告)日:1983-12-08
申请号:DE3320557
申请日:1983-06-07
Applicant: NAT AEROSPACE LAB
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