Sight window assembly and method of forming same
    131.
    发明授权
    Sight window assembly and method of forming same 失效
    视窗组装及其形成方法

    公开(公告)号:US5974877A

    公开(公告)日:1999-11-02

    申请号:US641541

    申请日:1996-05-01

    CPC classification number: B01J3/004 B23P11/025

    Abstract: A sight window assembly and a method of making same, the assembly being comprised of a windowpane panel mounted directly and under radial compression within an annular window-opening of a vessel wall panel and having cooperative annular peripheral portions which are complementary in shape to the window-opening defining portions of the wall panel, said panels having cooperative, mechanical, annular, positive interlocking elements. The method is comprised of providing the wall panel with the annular opening-defining portions, and the light-permeable windowpane panel, shaped to conform to the shape of the opening, and being slightly larger radially under predetermined equilibrium thermal conditions, and effecting a change in the equilibrium conditions to cause an increase in the radial differential of the wall panel opening and windowpane panel so as to permit the windowpane panel to be inserted within the opening in closing relation, inserting the windowpane panel in substantially such closing relation while maintaining said change in conditions, and maintaining the windowpane panel in such opening-closing position while permitting the wall panel and windowpane panel to return to a condition approaching such equilibrium conditions.

    Abstract translation: 视窗组件及其制造方法,该组件包括直接安装在径向压缩下的容器壁板的环形窗口内的窗玻璃面板,并具有与窗口形状互补的协作环形周边部分 打开限定壁板的部分,所述面板具有协作,机械,环形,正互锁元件。 该方法包括为壁板提供环形开口限定部分和透光性窗玻璃板,其形状适合于开口的形状,并且在预定平衡热条件下径向略微增大,并且实现改变 在平衡条件下,导致壁板开口和窗玻璃板的径向差异增加,以便窗玻璃板以关闭关系插入开口内,将窗玻璃板以基本上这样的关闭关系插入,同时保持所述变化 并且将窗玻璃板保持在这样的打开关闭位置,同时允许墙板和窗玻璃板返回到接近这种平衡条件的状态。

    Method and apparatus for producing nanoparticles at a high rate
    132.
    发明授权
    Method and apparatus for producing nanoparticles at a high rate 失效
    高速生产纳米粒子的方法和装置

    公开(公告)号:US5958329A

    公开(公告)日:1999-09-28

    申请号:US965469

    申请日:1997-11-06

    Inventor: Donald Lee Brown

    Abstract: A method and apparatus for producing nanoparticles at a high rate is provided. The system uses two chambers separated by a narrow duct. Contained within the lower chamber is the source material, preferably heated with an electron gun and fed with a continuous feeder for extended nanoparticle production runs. The upper chamber is used to nucleate the nanoparticles, the nanoparticles formed when the source vapor collides with a gas contained within the upper chamber. Depending upon the desired nanoparticles, the gas within the upper chamber is either inert or reactive. The duct connecting the upper and lower chambers is narrow enough to allow differential pumping of the chambers. Furthermore the vapor stream flowing though the duct at high speed provides a pumping action which helps to maintain the differential pressures within the two chambers. At least a portion of the top surface of the upper chamber is cooled, thus providing a condensation site for the nanoparticles. Periodically one or more scrappers remove the condensed nanoparticles from the condensation surface, allowing them to collect within particle collection containers surrounding the duct.

    Abstract translation: 提供了一种高速生产纳米粒子的方法和装置。 该系统使用由狭窄的管道隔开的两个室。 包含在下腔室内的是源材料,优选用电子枪加热,并且用连续进料器供给以延长纳米粒子生产运行。 上室用于使纳米颗粒成核,当源蒸气与包含在上室内的气体碰撞时形成纳米颗粒。 取决于所需的纳米颗粒,上部室内的气体是惰性或反应性的。 连接上部和下部腔室的管道足够窄以允许腔室的差动泵送。 此外,高速流过管道的蒸汽流提供了有助于保持两个室内的压差的泵送作用。 上室的顶表面的至少一部分被冷却,从而提供纳米颗粒的冷凝位置。 定期地,一个或多个刮板从冷凝表面去除凝结的纳米颗粒,使其能够收集在围绕管道的颗粒收集容器内。

    High pressure relief for microwave digestion vessel assembly
    133.
    发明授权
    High pressure relief for microwave digestion vessel assembly 失效
    用于微波消解容器组件的高压释放

    公开(公告)号:US5948307A

    公开(公告)日:1999-09-07

    申请号:US868756

    申请日:1997-06-04

    Abstract: A high pressure and temperature microwave digestion vessel assembly with enhanced safety features is disclosed. The assembly includes a membrane that is rupturable for pressure relief, and a secondary pressure relief mechanism including a seal cap with an annular stress relief region that shears or fractures when excess pressure is in the vessel interior. The membrane is positioned on a post extending from the seal cap into the inner liner. The diameter of the venting orifice may be adjusted to vary the desired pressure relief. The assembly also includes a piercing mechanism for venting the vessel after digestion is completed.

    Abstract translation: 公开了具有增强的安全特征的高压和高温微波消解容器组件。 组件包括可破裂的用于压力释放的膜,以及次级压力释放机构,包括具有环形应力消除区域的密封盖,当超负荷在容器内部时,所述环形应力释放区域被剪切或断裂。 膜位于从密封帽延伸到内衬里的柱上。 排气孔的直径可以调节以改变所需的压力释放。 组件还包括用于在消化完成之后使容器排气的穿孔机构。

    Solid acid supercritical alkylation reactions using carbon dioxide
and/or other co-solvents
    134.
    发明授权
    Solid acid supercritical alkylation reactions using carbon dioxide and/or other co-solvents 失效
    使用二氧化碳和/或其他共溶剂的固体酸超临界烷基化反应

    公开(公告)号:US5907075A

    公开(公告)日:1999-05-25

    申请号:US872865

    申请日:1997-06-11

    Abstract: Improved isoparaffin-olefin alkylation solid catalyst processes are provided which are characterized by low coke laydown and catalyst deactivation rates and production of valuable branched chain, high octane number alkylates. The processes of the invention involve providing a starting reactant mixture comprising an isoparaffin, an olefin and a co-solvent or diluent (carbon dioxide in molar excess, methane, hydrogen or mixtures thereof), and contacting the reactant mixture with an alkylation catalyst at near-critical or preferably supercritical conditions for the reaction mixture. The carbon dioxide serves as a co-solvent and reduces the critical temperature (T.sub.c) of the reaction mixture, thereby allowing lower reaction temperatures. The isoparaffin and olefin reactants are preferably pretreated to minimize moisture, peroxide and oxygenate impurities therein.

    Abstract translation: 提供改进的异链烷烃烯烃烷基化固体催化剂方法,其特征在于低焦炭沉淀和催化剂失活速率和有价值的支链高辛烷值烷基化物的生产。 本发明的方法包括提供起始反应物混合物,其包含异链烷烃,烯烃和共溶剂或稀释剂(摩尔过量的二氧化碳,甲烷,氢气或其混合物),并将反应混合物与烷基化催化剂接近 重要或优选超临界条件。 二氧化碳用作助溶剂并降低反应混合物的临界温度(Tc),由此允许较低的反应温度。 优选对异链烷烃和烯烃反应物进行预处理,以使其中的水分,过氧化物和含氧化合物的杂质最小化。

    Vacuum extrusion system and method
    136.
    发明授权
    Vacuum extrusion system and method 失效
    真空挤压系统及方法

    公开(公告)号:US5753161A

    公开(公告)日:1998-05-19

    申请号:US696472

    申请日:1996-08-14

    Abstract: A horizontal vacuum extrusion line includes a fixed bulkhead, a die inside the bulkhead, a telescoping vacuum chamber section and a fixed chamber section. A dam in the fixed section forms a pond for immersion cooling of the extrudate. A truss extends from the dam to the bulkhead supporting, shaping and calibration equipment and extends through the telescoping section. Fluid pressurizable seals at each end of the telescoping section are operable after the telescoping section is closed against the bulkhead and the telescoping and fixed sections are locked together. The telescoping section provide a more compact line and easier access to the complex equipment downstream of the die. The extrudate from the die passes down into the pond and then through an orifice in a hood projecting from the chamber into a lower level portion of the pond exposed to atmosphere. The hood also includes a tractor drive to push the extrudate through the underwater orifice. The hood and its contents are accessible through the atmospheric pond. A tractor haul-off and the tractor drive in the hood are the only extrudate drives between the calibration equipment and atmosphere. The higher level of the pond within the chamber downstream of the dam is controlled by a valve in turn controlling the output of a pump. The valve control senses the pond level and operates independently of the vacuum controls.

    Abstract translation: 卧式真空挤压生产线包括固定隔板,隔板内的模具,伸缩真空室部分和固定室部分。 固定部分的坝形成了用于浸渍冷却挤出物的池。 桁架从大坝延伸到隔板支撑,成型和校准设备,并延伸穿过伸缩部分。 伸缩部分的每端处的流体可加压密封件在伸缩部分相对于舱壁关闭并且伸缩和固定部分被锁定在一起之后是可操作的。 伸缩部分提供更紧凑的生产线,更容易进入模具下游的复杂设备。 来自模具的挤出物向下流入池塘,然后穿过从室中突出的罩中的孔口,暴露于大气中的池塘的下部。 发动机罩还包括一个拖拉机驱动器,用于将挤出物推出水下孔口。 罩及其内容物可通过大气池进入。 拖拉机牵引车和牵引车的驱动器是校准设备和大气之间唯一的挤出机。 坝下游的池塘中的较高水位由阀门控制,从而控制泵的输出。 阀门控制检测池水位,独立于真空控制器运行。

    Protective collar for vacuum seal in a plasma etch reactor
    139.
    发明授权
    Protective collar for vacuum seal in a plasma etch reactor 失效
    用于等离子体蚀刻反应器中真空密封的保护套环

    公开(公告)号:US5722668A

    公开(公告)日:1998-03-03

    申请号:US235602

    申请日:1994-04-29

    Abstract: A vacuum seal assembly that can be used in a plasma etch reactor to seal the chamber interior from the outside environment consists of a protective collar that is injection molded or machined of a high strength, high temperature and corrosion resistant thermoplastic material, the collar has an elastomeric gasket installed therein and is used in combination with a second elastomeric gasket to achieve a fluid-tight seal between two rigid surfaces made of silicon and quartz, respectively.

    Abstract translation: 可用于等离子体蚀刻反应器以将室内部与外部环境密封的真空密封组件包括由高强度,耐高温和耐腐蚀的热塑性材料注射成型或加工的保护套圈,所述套环具有 安装在其中的弹性垫圈并且与第二弹性垫圈组合使用以分别在由硅和石英制成的两个刚性表面之间实现流体密封。

    Method for hydrothermal oxidation
    140.
    发明授权
    Method for hydrothermal oxidation 失效
    水热氧化法

    公开(公告)号:US5674405A

    公开(公告)日:1997-10-07

    申请号:US509504

    申请日:1995-07-08

    CPC classification number: C02F1/025 C02F11/086 F01K3/188 Y02P20/582

    Abstract: A method of continuous flow hydrothermal oxidation which provides for a low cost means of reaction initiation and propagation. The aqueous-organic feedstock and oxidant are introduced to a small reaction chamber and allowed to mix with the hot, partially reacted contents thereof. This backmixing serves to initiate the reaction of the incoming feedstock. Optionally, the contents of the chamber then pass to a second reactor located downstream, in order to allow for completion of the oxidation reaction.

    Abstract translation: 连续流动水热氧化方法,其提供反应开始和传播的低成本手段。 将含水有机原料和氧化剂引入到小的反应室中,并与其部分反应的热的物质混合。 该回混用于引发进料的反应。 任选地,室的内容物然后传递到位于下游的第二反应器,以便完成氧化反应。

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