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11.发明申请公开(公告)号：US20180022666A1
公开(公告)日：2018-01-25
申请号：US15216382
申请日：2016-07-21
Applicant: PHILLIPS 66 COMPANY
Inventor： Jianhua Yao , Bruce B. Randolph
CPC classification number: C01B39/026 , B01J29/40 , B01J37/06 , C01B39/38 , C10G50/00 , C10L1/06 , C10L2200/0423 , C10L2270/023
Abstract: A process for post synthesis treatment of ZSM-5 catalyst for converting ethylene to liquid fuel products providing substantially improved catalyst life. The treatment comprises either a base treatment, an acid treatment or a two-step treatment where one is with an acid and the other is with a base. The base treatment is provided by a weak sodium hydroxide such as less than 1 Molar concentration. The acid treatment is stronger acid where, for example, a hydrogen chloride solution at greater than 2 Molar concentration is used.
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12.发明授权Process scheme for catalytic production of renewable hydrogen from oxygenate feedstocks 有权从含氧化合物原料催化生产可再生氢的工艺方案公开(公告)号：US09452931B2
公开(公告)日：2016-09-27
申请号：US14076321
申请日：2013-11-11
Applicant: PHILLIPS 66 COMPANY
Inventor： Uchenna P. Paul , Bruce B. Randolph , Jon M. Nelson , Kristi A. Fjare , Danielle K. Smith , Mark Rumel Cragun , Richard D. Sadok
IPC: C01B3/32
CPC classification number: C01B3/323 , C01B2203/0233 , C01B2203/0405 , C01B2203/0415 , C01B2203/043 , C01B2203/1041 , C01B2203/1058 , C01B2203/1076 , C01B2203/1082 , C01B2203/1094 , C01B2203/1211 , C01B2203/1217 , C01B2203/1223 , C01B2203/1229
Abstract: A process is described for flowing an oxygenate feed over a catalyst in an adiabatic fixed bed reactor to product a reactor effluent and heat. The reaction inside the adiabatic fixed bed reactor occurs at a reaction temperature from about 200° C. to about 375° C. The reactor effluent is then condensed to separate the liquid products and the gaseous products. A separation step then separates the gaseous products into hydrogen and off-gas.
Abstract translation: 描述了一种将含氧化合物进料在绝热固定床反应器中的催化剂上流动以产生反应器流出物和热量的方法。 绝热固定床反应器中的反应在约200℃至约375℃的反应温度下进行。然后将反应器流出物冷凝以分离液体产物和气态产物。 然后分离步骤将气态产物分离成氢气和废气。
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公开(公告)号：US20160101409A1
公开(公告)日：2016-04-14
申请号：US14872171
申请日：2015-10-01
Applicant: PHILLIPS 66 COMPANY
Inventor： William Chadwick Ellis , Uchenna Paul , Danielle Smith , Bruce B. Randolph , Neal D. McDaniel , Jon Nelson , Larry Johnston
IPC: B01J23/89 , C01B3/40 , B01J23/83 , B01J23/755 , B01J23/78
CPC classification number: C01B3/40 , B01J23/002 , B01J23/755 , B01J23/78 , B01J23/80 , B01J23/83 , B01J23/894 , B01J2523/00 , C01B2203/0233 , C01B2203/0283 , C01B2203/043 , C01B2203/0475 , C01B2203/048 , C01B2203/0811 , C01B2203/0816 , C01B2203/1235 , C01B2203/1241 , C01B2203/1247 , C01B2203/148 , Y02P20/52 , B01J2523/13 , B01J2523/17 , B01J2523/19 , B01J2523/25 , B01J2523/31 , B01J2523/3712 , B01J2523/847 , B01J2523/22 , B01J2523/27
Abstract: A catalyst for steam reforming. The catalyst comprises an active site of NiCu or NiCuZn, from about 15 wt % to about 25 wt % of the catalyst, a composition comprising at least one promoter and at least one support modifier, from about 5 wt % to about 30 wt % of the catalyst, and a support.
Abstract translation: 蒸汽重整用催化剂。 催化剂包含NiCu或NiCuZn的活性位点，约15重量％至约25重量％的催化剂，包含至少一种助催化剂和至少一种载体改性剂的组合物，约5重量％至约30重量％ 催化剂和支持物。
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14.发明申请公开(公告)号：US20200339489A1
公开(公告)日：2020-10-29
申请号：US16855333
申请日：2020-04-22
Applicant: PHILLIPS 66 COMPANY
Inventor： Anthony O. Baldridge , Neal D. McDaniel , James A. Suttil , Jianhua Yao , Edward C. Weintrob , Matthew J. Wulfers , Bruce B. Randolph , Maziar Sardashti
Abstract: Processes for producing liquid transportation fuels by converting a hydrocarbon feed stream comprising both isopentane and n-pentane. The hydrocarbon feed stream is separated into a first fraction that predominantly comprises isopentane and a second fraction that predominantly comprises n-pentane and some C6 paraffins. The first fraction is catalytically activated to produce an activation effluent comprising olefins and aromatics, while the second fraction is isomerized to convert at least a portion of the n-pentane to isopentane, then combined with the hydrocarbon feed stream to allow the newly-produced isopentane to be separated into the first fraction. Finally, the activation effluent is oligomerized. The process produced increased yields of products that meet specifications for a blend component of liquid transportation fuels.
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公开(公告)号：US10400182B2
公开(公告)日：2019-09-03
申请号：US15871614
申请日：2018-01-15
Applicant: PHILLIPS 66 COMPANY
Inventor： Jianhua Yao , Hong Xie , Bruce B. Randolph , Steven E. Lusk , Dhananjay B. Ghonasgi , Jonathan R. Marda
Abstract: The present disclosure relates generally processes and systems for converting a mixture of light hydrocarbons to liquid transportation fuels by first cracking the light hydrocarbons to an intermediate comprising olefins, which is converted by contacting with a catalyst comprising at least one zeolite in two separate conversion stages with an intervening recovery of liquid product. The first stage conversion favors oligomerization of larger olefins to form diesel range products that are collected prior to directing unconverted smaller olefins to be oligomerized in a second stage conversion conducted at a higher temperature and lower pressure.
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Patent Agency Ranking
公开(公告)号：US09266755B2
公开(公告)日：2016-02-23
申请号：US14020388
申请日：2013-09-06
Applicant: PHILLIPS 66 COMPANY
Inventor： Mark A. Hughes , Charles J. Lord, III , Bruce B. Randolph , Joe B. Cross , Sumod Kalakkunnath , Mike K. Corbett , Roger K. Goenner , Larry E. Reed
IPC: B01D15/00 , C02F1/42 , C02F1/58 , C02F9/00 , B01J20/08 , B01J20/20 , B01J20/32 , B01J20/02 , B01J20/10 , C02F1/02 , C02F1/24 , C02F1/28 , C02F1/38 , C02F1/44 , C02F1/463 , C02F1/52 , C02F101/10 , C02F101/20 , C02F101/32 , C02F1/00 , C02F1/40 , C02F1/469 , C02F1/66 , C02F1/70 , C02F103/00 , C02F103/10 , C02F103/36
CPC classification number: C02F1/58 , B01J20/0262 , B01J20/08 , B01J20/103 , B01J20/20 , B01J20/3204 , B01J20/3236 , C02F1/004 , C02F1/02 , C02F1/24 , C02F1/281 , C02F1/283 , C02F1/285 , C02F1/288 , C02F1/38 , C02F1/40 , C02F1/42 , C02F1/441 , C02F1/442 , C02F1/463 , C02F1/4693 , C02F1/5236 , C02F1/66 , C02F1/70 , C02F9/00 , C02F2001/007 , C02F2101/101 , C02F2101/103 , C02F2101/106 , C02F2101/20 , C02F2101/32 , C02F2101/325 , C02F2103/001 , C02F2103/10 , C02F2103/365 , C02F2301/08
Abstract: Methods and apparatus relate to treating fluid to at least reduce selenium content within the fluid. The treating includes conditioning stages to alter a composition of the fluid prior to removal of the selenium content from the fluid. The composition of the fluid after the conditioning stages facilitates the removal of the selenium content or at least limits detrimental impact to selenium removal efficiency.
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公开(公告)号：US20140110271A1
公开(公告)日：2014-04-24
申请号：US14047084
申请日：2013-10-07
Applicant: PHILLIPS 66 COMPANY
Inventor： Mahaprasad Kar , Sourabh Pansare , John T. Gorke , Edgar Lotero , Neal D. McDaniel , Danielle K. Smith , Dennis G. Schultz , Kristi A. Fjare , Bruce B. Randolph , Sikta Patnaik , Uchenna P. Paul , Madhu Anand
CPC classification number: C25B11/0415 , C25B1/02 , C25B11/0473
Abstract: The process describes performing electrolysis on an alkaline oxygenate mixture to produce hydrogen. In this process the electrolysis does not form any significant amounts of oxygen.
Abstract translation: 该方法描述了在碱性含氧化合物混合物上进行电解以产生氢。 在这个过程中，电解不会形成任何显着量的氧气。
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公开(公告)号：US20140042065A1
公开(公告)日：2014-02-13
申请号：US14020388
申请日：2013-09-06
Applicant: Phillips 66 Company
Inventor： Mark A. Hughes , Charles J. Lord III , Bruce B. Randolph , Joe B. Cross , Sumod Kalakkunnath , Mike K. Corbett , Roger K. Goenner , Larry E. Reed
IPC: C02F1/58
CPC classification number: C02F1/58 , B01J20/0262 , B01J20/08 , B01J20/103 , B01J20/20 , B01J20/3204 , B01J20/3236 , C02F1/004 , C02F1/02 , C02F1/24 , C02F1/281 , C02F1/283 , C02F1/285 , C02F1/288 , C02F1/38 , C02F1/40 , C02F1/42 , C02F1/441 , C02F1/442 , C02F1/463 , C02F1/4693 , C02F1/5236 , C02F1/66 , C02F1/70 , C02F9/00 , C02F2001/007 , C02F2101/101 , C02F2101/103 , C02F2101/106 , C02F2101/20 , C02F2101/32 , C02F2101/325 , C02F2103/001 , C02F2103/10 , C02F2103/365 , C02F2301/08
Abstract: Methods and apparatus relate to treating fluid to at least reduce selenium content within the fluid. The treating includes conditioning stages to alter a composition of the fluid prior to removal of the selenium content from the fluid. The composition of the fluid after the conditioning stages facilitates the removal of the selenium content or at least limits detrimental impact to selenium removal efficiency.
Abstract translation: 方法和装置涉及处理流体以至少降低流体内的硒含量。 处理包括在从流体中除去硒含量之前改变流体组成的调节阶段。 在调节阶段之后的流体组成促进了硒含量的去除，或至少限制了硒去除效率的有害影响。
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公开(公告)号：US20230382826A1
公开(公告)日：2023-11-30
申请号：US18314591
申请日：2023-05-09
Applicant: PHILLIPS 66 COMPANY
Inventor： Anthony O. Baldridge , Matthew J. Wulfers , Neal D. McDaniel , Robert M. Walston , Soumen Kundu , Bruce B. Randolph
CPC classification number: C07C6/10 , C07C7/09 , B01J8/0492 , B01D5/006 , B01D3/14 , C07C2529/40 , B01J2208/00017 , B01J2208/00539
Abstract: The present disclosure relates generally to processes and systems for producing liquid transportation fuels by converting a feed stream that comprises both isopentane and n-pentane, and optionally, some C6+ hydrocarbons. Isopentane and smaller hydrocarbons are separated to form a first fraction while n-pentane and larger components of the feed stock form a second fraction. Each fraction is then catalytically-activated in a separate reaction zone with a separate catalyst, where the conditions maintained in each zone maximize the conversion of each fraction to olefins and aromatics, while minimizing the production of C1-C4 light paraffins. In certain embodiments, the first fraction is activated at a lower temperature than the second fraction. Certain embodiments additionally comprise mixing at least a portion of the two effluents and contacting with either an oligomerization catalyst or alkylation catalyst to provide enhanced yields of upgraded hydrocarbon products that are suitable for use as a blend component of liquid transportation fuels or other value-added chemical products.
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公开(公告)号：US11406958B2
公开(公告)日：2022-08-09
申请号：US17095173
申请日：2020-11-11
Applicant: PHILLIPS 66 COMPANY
Inventor： Jianhua Yao , Neal D. McDaniel , Bruce B. Randolph , Robert M. Walston , Anthony O. Baldridge , James A. Suttil , Soumen Kundu , Hong Xie , Steven E. Lusk
Abstract: The present disclosure relates generally processes and systems for converting a C2-C7 light alkanes feed to liquid transportation fuels or value-added chemicals. The feed is contacted with an aromatization catalyst at a temperature and pressure that selectively converts C4 and larger alkanes to an intermediate product comprising monocyclic aromatics and olefins. Following separation of the aromatics and C5+ hydrocarbons from the intermediate product, unconverted C2-C3 alkanes are thermally-cracked to produce olefins that are subsequently oligomerized to produce a liquid transportation fuel blend stock or value-added chemicals.
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