公开(公告)号：US20230049400A1

公开(公告)日：2023-02-16

申请号：US17873493

申请日：2022-07-26

Applicant: PHILLIPS 66 COMPANY

Inventor： Kan Huang ,  Liang Zhang ,  Christopher J. LaFrancois ,  Brian J. Worfolk

IPC: H01M4/587 ,  C01B32/05 ,  C10G27/04

Abstract: Embodiments of the present disclosure generally relate to methods for preparing carbon materials which can be used in battery electrodes. In one or more embodiments, a method for preparing an anode carbon material is provided and includes combining a liquid refinery hydrocarbon product and a solvent to produce a first mixture, combining the first mixture and a first oxidizing agent containing an acid to produce a second mixture containing the liquid refinery hydrocarbon product, the solvent, and the first oxidizing agent, and heating the second mixture to produce a reaction mixture containing an oxidized solid product during an oxidation process. The method also includes separating the oxidized solid product from the reaction mixture during a separation process and carbonizing the oxidized solid product to produce a hard carbon product during a carbonization process.

公开(公告)号：US20210020903A1

公开(公告)日：2021-01-21

申请号：US16929222

申请日：2020-07-15

Applicant: PHILLIPS 66 COMPANY

Inventor： Zhenhua Mao ,  Nan Li ,  Corey W. Tropf ,  Dachuan Shi ,  Christopher J. LaFrancois

IPC: H01M4/133 ,  H01M10/0525

Abstract: The disclosure relates to a carbon-based electrode material that has been graphitized to hold ions in the electrode of a battery and more particularly include carbide or carbide and nitride surfaces that protect the graphite core. The preferred batteries include metal ion such as lithium ion batteries where the carbon-based electrode is the anode although the carbon-based electrode may also serve in dual ion batteries where both electrodes may comprise the graphitized carbon-based electrodes. The electrodes are more amorphous than conventional graphite electrodes and include a carbide or nitride containing surface treatment.

公开(公告)号：US20140205536A1

公开(公告)日：2014-07-24

申请号：US14220661

申请日：2014-03-20

Applicant: PHILLIPS 66 COMPANY

Inventor： Roland Schmidt ,  Christopher J. LaFrancois

IPC: C01B3/26

CPC classification number: C01B3/26 ,  B01J23/90 ,  B01J38/06 ,  B01J38/40 ,  C01B3/323 ,  C01B3/326 ,  C01B3/48 ,  C01B2203/1047 ,  C01B2203/1052 ,  C01B2203/1058 ,  C01B2203/1064 ,  C01B2203/107 ,  C10J3/02 ,  C10J3/463 ,  C10J2300/0916 ,  C10J2300/0923 ,  C10J2300/0943 ,  C10J2300/0959 ,  C10J2300/0976 ,  C10J2300/0986 ,  C10J2300/0993 ,  C10K3/04 ,  Y02P20/145 ,  Y02P20/52 ,  Y02P20/584

Abstract: There is provided herein a method for producing hydrogen gas, comprising: sorbing a liquid hydrocarbon fuel to a gasification catalyst to form a sorbed hydrocarbon fuel; heating said sorbed hydrocarbon fuel to a first temperature for a first period of time sufficient to form coke; and gasifying said coke at a second temperature at a pressure for a second period of time in the presence of water and/or oxygen, so as to produce hydrogen gas and carbon monoxide and to regenerate said catalyst. In particular, the hydrocarbon fuel can be a liquid biomass, such pyrolysis oil, and the method can be CO2 neutral.

Abstract translation: 本文提供了一种生产氢气的方法，包括：将液体烃燃料吸附到气化催化剂以形成吸附的烃燃料; 将所述吸附的烃燃料加热至第一温度持续足以形成焦炭的第一时间段; 以及在第二个温度下在水和/或氧的存在下在第二时间段内将所述焦炭气化，以产生氢气和一氧化碳，并再生所述催化剂。 特别地，烃燃料可以是液体生物质，这种热解油，并且该方法可以是二氧化碳中性的。

公开(公告)号：US20210020904A1

公开(公告)日：2021-01-21

申请号：US16929248

申请日：2020-07-15

Applicant: PHILLIPS 66 COMPANY

Inventor： Zhenhua Mao ,  Nan Li ,  Corey W. Tropf ,  Dachuan Shi ,  Christopher J. LaFrancois

IPC: H01M4/133 ,  H01M10/0525

Abstract: The disclosure relates to a carbon-based electrode material that has been graphitized to hold ions in the electrode of a battery and more particularly include carbide or carbide and nitride surfaces that protect the graphite core. The preferred batteries include metal ion such as lithium ion batteries where the carbon-based electrode is the anode although the carbon-based electrode may also serve in dual ion batteries where both electrodes may comprise the graphitized carbon-based electrodes. The electrodes are more amorphous than conventional graphite electrodes and include a carbide or nitride containing surface treatment.

公开(公告)号：US08817241B2

公开(公告)日：2014-08-26

申请号：US14051492

申请日：2013-10-11

Applicant: Phillips 66 Company

Inventor： Christopher J. LaFrancois ,  James F. Stewart ,  Gregory C. Allred ,  Marion Ash

IPC: G01N33/28 ,  G01J3/00 ,  G01N33/18 ,  G01N21/35 ,  G01N21/33 ,  G01N21/41 ,  G01N21/64

CPC classification number: G01N33/1833 ,  G01N21/33 ,  G01N21/35 ,  G01N21/3577 ,  G01N21/41 ,  G01N21/64

Abstract: An oil in water analyzer for measuring the concentration of hydrocarbons in an effluent stream. The oil in water analyzer has a valve system for acquiring a sample from an effluent stream. An extraction device is used for mixing a known volume of a solvent and the sample to produce a hydrocarbon/solvent mixture. A second valve is used for transporting the hydrocarbon/solvent mixture to a spectroscopic cell. It is at the spectroscopic cell where the concentration of hydrocarbons in the hydrocarbon/solvent mixture is evaluated.

Abstract translation: 用于测量流出物流中碳氢化合物浓度的水分析仪。 水分析仪具有用于从流出物流中获取样品的阀系统。 提取装置用于混合已知体积的溶剂和样品以产生烃/溶剂混合物。 第二个阀用于将烃/溶剂混合物输送到分光单元。 在烃/溶剂混合物中的烃浓度被评估的分光池中。