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公开(公告)号：US20230041090A1
公开(公告)日：2023-02-09
申请号：US17873536
申请日：2022-07-26
Applicant: PHILLIPS 66 COMPANY
Inventor： Kan Huang , Liang Zhang , Alexander Z. Wilbee , Brian J. Worfolk
Abstract: Embodiments of the present disclosure generally relate to carbon materials for battery electrodes and methods for preparing such carbon materials. More specifically, embodiments relate to methods for coating a carbon film onto nano-ordered carbon particles to produce carbon-coated particles which can be used as an anode material within a battery, such as a lithium-ion battery, a sodium-ion battery, other types of batteries. In one or more embodiments, a method for producing carbon-coated particles is provided and includes positioning nano-ordered carbon particles within a processing region of a processing chamber, purging the processing region containing the nano-ordered carbon particles with an inert gas, heating the nano-ordered carbon particles to a temperature of about 700° C. or greater during an annealing process, and depositing a carbon film on the nano-ordered carbon particles to produce carbon-coated particles during a vapor deposition process.
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公开(公告)号：US20230049400A1
公开(公告)日：2023-02-16
申请号：US17873493
申请日：2022-07-26
Applicant: PHILLIPS 66 COMPANY
Inventor： Kan Huang , Liang Zhang , Christopher J. LaFrancois , Brian J. Worfolk
Abstract: Embodiments of the present disclosure generally relate to methods for preparing carbon materials which can be used in battery electrodes. In one or more embodiments, a method for preparing an anode carbon material is provided and includes combining a liquid refinery hydrocarbon product and a solvent to produce a first mixture, combining the first mixture and a first oxidizing agent containing an acid to produce a second mixture containing the liquid refinery hydrocarbon product, the solvent, and the first oxidizing agent, and heating the second mixture to produce a reaction mixture containing an oxidized solid product during an oxidation process. The method also includes separating the oxidized solid product from the reaction mixture during a separation process and carbonizing the oxidized solid product to produce a hard carbon product during a carbonization process.
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公开(公告)号：US20230047084A1
公开(公告)日：2023-02-16
申请号：US17873422
申请日：2022-07-26
Applicant: PHILLIPS 66 COMPANY
Inventor： Dachuan Shi , Alexander Z. Wilbee , Paul M. Schmidt , Liang Zhang , Kan Huang , Jonathan R. Marda
Abstract: Embodiments of the present disclosure generally relate to methods for preparing carbon materials which can be used in battery electrodes. More specifically, embodiments relate to methods for preparing hard carbon materials used as anode materials in metal-ion batteries, such as a sodium-ion battery. In one or more embodiments, a method includes exposing a liquid refinery hydrocarbon product to a first functionalization agent containing sulfur to produce a first solid functionalized product containing sulfur during a first functionalization process. The method further includes purifying the first solid functionalized product during a purification process and exposing the first solid functionalized product to a second functionalization agent containing oxygen to produce a second solid functionalized product containing sulfur and oxygen during a second functionalization process. The method also includes carbonizing the second solid functionalized product to produce a hard carbon product during a carbonization process.
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