POLYSACCHARIDE MONOLITHIC STRUCTURE AND MANUFACTURING METHOD THEREFOR
    11.
    发明申请
    POLYSACCHARIDE MONOLITHIC STRUCTURE AND MANUFACTURING METHOD THEREFOR 审中-公开
    多晶体单晶结构及其制造方法

    公开(公告)号:US20140311984A1

    公开(公告)日:2014-10-23

    申请号:US14258456

    申请日:2014-04-22

    Abstract: A problem is to provide a monolithic structure that is a porous body formed of a polysaccharide being a naturally-occurring polymer, and has continuous pores having an average pore diameter suitable for biomolecule separation to allow formation into an arbitrary shape, and a manufacturing method therefor. A solution is to manufacture the polysaccharide monolithic structure by a method including a first step for dissolving a polysaccharide into a mixed solvent including a solvent into which the polysaccharide is soluble and a solvent into which the polysaccharide is insoluble, at a temperature lower than a boiling point of the mixed solvent, to give a polysaccharide solution, and a second step for cooling the polysaccharide solution to give the polysaccharide monolithic structure. The polysaccharide monolithic structure obtained is a porous body having continuous pores having an average pore diameter of 0.01 to 20 micrometers and a thickness of 100 micrometers or more.

    Abstract translation: 问题在于提供作为天然存在的聚合物的多糖形成的多孔体的整体结构,并且具有适于生物分子分离以使形成任意形状的平均孔径的连续孔及其制造方法 。 解决方案是通过包括第一步骤的方法来制造多糖整体结构,该方法包括将多糖溶解在包含多糖可溶性的溶剂的混合溶剂中,以及多糖不溶于其中的溶剂,在低于沸点 的混合溶剂,得到多糖溶液,第二步是冷却多糖溶液,得到多糖整体结构。 获得的多糖整体结构是具有平均孔径为0.01〜20微米,厚度为100微米以上的连续孔的多孔体。

    Method for making a porous polymeric material

    公开(公告)号:US20140227338A1

    公开(公告)日:2014-08-14

    申请号:US14253695

    申请日:2014-04-15

    Abstract: Porous polymers having a plurality of openings or chambers that are highly convoluted, with each chamber being defined by multiple, thin, flat partitions are produced by a new gel enhanced phase separation technique. In a preferred embodiment, a second liquid is added to a polymer solution, the second liquid causing the solution to increase in viscosity. With sufficient polymer and second liquid present, the increase in viscosity can be up to that of a gel. The gel can then be shaped as needed. Subsequent solvent extraction leaves the porous polymeric body of defined shape. The porous polymers have utility as medical prostheses, the porosity permitting ingrowth of neighboring tissue. A second material may be incorporated into the chambers, thereby creating a microstructure filling the voids of the macrostructure. A porous polymeric body manufactured by this process may incorporate biologically active agents, and which agents may be delivered in a time-staged delivery manner, where differing drugs may be delivered over differing periods.

    Method for making a porous polymeric material
    13.
    发明申请
    Method for making a porous polymeric material 有权
    制造多孔聚合材料的方法

    公开(公告)号:US20050075408A1

    公开(公告)日:2005-04-07

    申请号:US10948486

    申请日:2004-09-23

    Abstract: Porous polymers having a plurality of openings or chambers that are highly convoluted, with each chamber being defined by multiple, thin, flat partitions are produced by a new gel enhanced phase separation technique. In a preferred embodiment, a second liquid is added to a polymer solution, the second liquid causing the solution to increase in viscosity. With sufficient polymer and second liquid present, the increase in viscosity can be up to that of a gel. The gel can then be shaped as needed. Subsequent solvent extraction leaves the porous polymeric body of defined shape. The porous polymers have utility as medical prostheses, the porosity permitting ingrowth of neighboring tissue. A second material may be incorporated into the chambers, thereby creating a microstructure filling the voids of the macrostructure. A porous polymeric body manufactured by this process may incorporate biologically active agents, and which agents may be delivered in a time-staged delivery manner, where differing drugs may be delivered over differing periods.

    Abstract translation: 通过新的凝胶增强相分离技术产生多孔聚合物,其具有高度卷曲的多个开口或室,每个室由多个薄的平坦隔板限定。 在优选的实施方案中,将第二液体加入到聚合物溶液中,使第二液体溶液增加粘度。 当存在足够的聚合物和第二液体时,粘度的增加可以达到凝胶的增加。 然后可以根据需要成型凝胶。 随后的溶剂萃取离开具有限定形状的多孔聚合物体。 多孔聚合物可用作医用假体,孔隙度允许相邻组织向内生长。 可以将第二材料并入室中,从而产生填充宏观结构的空隙的微结构。 通过该方法制造的多孔聚合体可以并入生物活性剂,并且哪些试剂可以按时间递送方式递送,其中不同的药物可以在不同的时期内递送。

    Non-degradable porous materials with high surface areas
    14.
    发明申请
    Non-degradable porous materials with high surface areas 失效
    具有高表面积的不可降解多孔材料

    公开(公告)号:US20030071383A1

    公开(公告)日:2003-04-17

    申请号:US10271622

    申请日:2002-10-16

    Inventor: Peter X. Ma

    CPC classification number: B29C67/20 C08J9/28 C08J2201/048 C08J2201/054

    Abstract: A method for preparing a highly porous, high surface area non-degradable material, comprises the steps of mixing a non-degradable polymer with a solvent or mixture of solvents; gelling the mixture; and treating the gel under conditions whereby a substantially solvent free porous structure is created having a porosity greater than about 80%. The resultant material is mechanically strong and has an architecture comprising at least one of nano fibrous, micro fibrous, non fibrous, complex porous structure with nano fibrous architecture, and mixtures thereof.

    Abstract translation: 一种制备高度多孔,高表面积不可降解材料的方法,包括将不可降解聚合物与溶剂或溶剂混合物混合的步骤; 凝胶混合物 并在条件下处理凝胶,由此产生具有大于约80%的孔隙率的基本上无溶剂的多孔结构。 所得到的材料是机械强度的并且具有包括具有纳米纤维结构的纳米纤维,微纤维,非纤维,复合多孔结构及其混合物中的至少一种的结构。

    Low-density microcellular foam and method of making same
    16.
    发明授权
    Low-density microcellular foam and method of making same 失效
    低密度微孔泡沫及其制备方法

    公开(公告)号:US4012265A

    公开(公告)日:1977-03-15

    申请号:US609641

    申请日:1975-09-02

    Applicant: James A. Rinde

    Inventor: James A. Rinde

    Abstract: Low-density microcellular foam having a cell size of not greater than 2 .mu.m and method of making by dissolving cellulose acetate in an acetone-based solvent, gelling the solution in a water bath maintained at 0.degree.-10.degree. C for a selected period of time to allow impurities to diffuse out, freezing the gel, and then freeze-drying wherein water and solvents sublime and the gel structure solidifies into low-density microcellular foam. The foam has a density of 0.065 to 0.6.times.10.sup.3 kg/m.sup.3 and cell size of about 0.3 to 2 .mu.m. The small cell size foam is particularly applicable for encapsulation of laser targets.

    Abstract translation: 细胞尺寸不大于2μm的低密度微孔泡沫体和通过将乙酸纤维素溶解在丙酮类溶剂中制备的方法,将溶液凝胶保持在0-10℃的水浴中选定的时间 的时间以允许杂质扩散出来,冷凝凝胶,然后冷冻干燥,其中水和溶剂升华,凝胶结构固化成低密度微孔泡沫。 泡沫体的密度为0.065〜0.6×10 3 kg / m 3,电池尺寸为0.3〜2μm左右。 小泡沫泡沫特别适用于激光靶材的封装。

    Method of preparation of a porous thermosetting resin
    17.
    发明授权
    Method of preparation of a porous thermosetting resin 失效
    多孔热固性树脂的制备方法

    公开(公告)号:US3825506A

    公开(公告)日:1974-07-23

    申请号:US35096073

    申请日:1973-04-13

    Inventor: CARTER E

    CPC classification number: C08J9/28 C08G59/18 C08J9/32 C08J2201/054

    Abstract: POROUS OPEN-CELL THERMOSETTING RESIN AND PROCESS FOR PREPARING SAME. THE PROCESS INVOLVES THE INITIAL FORMATION OF AN EMULSION HAVING A LIQUID RESIN BLEND AS THE CONTINUOUS PHASE AND A HARDENER SOLUTION OR DISPERSION AS THE DISCONTINUOUS PHASE. THE RESIN BLEND PHASE INITIALLY CONTAINS AN AMOUNT OF HARDENER LESS THAN THAT REQUIRED FOR A STOICHIOMETRIC CURE OF THE RESIN. THE HARDENER SOLUTION OR DISPERSION INITIALLY CONTAINS AN ADDITIONAL AMOUNT OF HARDENER TO SUPPLEMENT THE BLEND AND CURE THE RESIN. THE LIQUID OF THE NON-RESIN PHASE IS SELECTED TO BE SUBSTNTIALLY A NON-SOLVENT WITH RESPECT TO THE RESIN. AS THE POLYMERIZATION OF THE EMULSION PROCEEDS HARDENER IS LEACHED OUT OF THE SOLUTION PHASE WHICH IS THE DISCONTINUOUS PHASE,

    RESULTING IN A PHASE INVERSION AFTER PARTIAL GELATION WITH THE NON-RESIN LIQUID SOLUTION PHASE BECOMING THE CONTINUOUS PHASE ND THE NON-GELLED RESIN BLEND BECOMING THE DISCONTINUOUS PHASE. AFTER POLYMERIZATION IS COMPLETED AND THE RESIN SOLIDIFIED, THE LIQUID OF THE NON-RESIN PHASE IS REMOVED BY EXTRACTION OR EVAPORATION. THE RESULT IS A RESIN HAVING A NETWORK OF INTERCONNECTED PORES. AN IMPORTANT ASPECT OF THE INVENTION IS THAT IT PERMITS CONTROL OF THE PORE SIZE OF THE PRODUCT.

    AEROGEL POWDER MANUFACTURING METHOD AND THERMAL INSULATION MATERIAL USING THE SAME

    公开(公告)号:US20230357525A1

    公开(公告)日:2023-11-09

    申请号:US18028543

    申请日:2021-06-04

    Abstract: A manufacturing method of an aerogel powder of the present invention includes: a mixing process of mixing a silicon alkoxide (TEOS (tetraethoxysilane)) and a solvent (methanol) to form a sol on hydrolysis; a gelling process of gelling the sol obtained in the mixing process; an aging process of aging the gel obtained in the gelling process to obtain a wet gel (alkogel); a solvent exchanging process of replacing the solvent of the wet gel with a predetermined replacement solvent (hexane); a modifying process of modifying a surface of a network structure of the wet gel with a predetermined organic group using TMCS; a process of washing the modified wet gel obtained in the wet gel generating process; drying the washed and modified wet gel; and crushing the dried, washed and modified wet gel. It is possible to provide aerogel powder with reduced manufacturing cost per unit bulk volume and excellent in thermal insulation.

Patent Agency Ranking