Process for the production of niobium and/or tantalum powder with large surface area
    31.
    发明申请
    Process for the production of niobium and/or tantalum powder with large surface area 审中-公开
    用于生产具有大表面积的铌和/或钽粉末的方法

    公开(公告)号:US20060096418A1

    公开(公告)日:2006-05-11

    申请号:US10533791

    申请日:2003-08-27

    Inventor: Solon Tagusagawa

    Abstract: The present invention refers to a process for production of a powder of niobium and/or tantalum having high purity, large specific surface area, controlled contents of oxygen and nitrogen, and a morphology that is adequate for use in the manufacture of capacitors, characterized by including one sole step of reduction of a controlled layer of niobium and/or tantalum oxide (NbxOy, and/or TaxOy, where x=1 to 2 and y=1 to 5) deliberately formed over particles of metallic niobium and/or tantalum and/or hydrides thereof of adequate purity, by alkali metals or earth alkali metals and/or hydrides thereof in a bath of molten salts followed by a step of dissolution of the salt in an aqueous solution for recovery of the niobium and/or tantalum powder. These particles produced using the said process have a small size, large surface area and a sponge-like morphology, being thereby adequate for the production of capacitors.

    Abstract translation: 本发明涉及一种生产具有高纯度,大比表面积,受控含氧量和氮含量的铌和/或钽粉末的方法,以及足以用于制造电容器的形态,其特征在于: 包括在金属铌和/或钽的颗粒上故意形成的铌和/或氧化钽(Nb x O y和/或TaxO y,其中x = 1至2和y = 1至5)受控层的还原的唯一步骤, 碱金属或碱土金属和/或其氢化物在熔盐浴中浸渍,然后将盐溶解在用于回收铌和/或钽粉末的水溶液中的步骤。 使用所述方法制造的这些颗粒具有小尺寸,大的表面积和海绵状形态,从而足以用于制造电容器。

    Method of making a fecraI material and such material
    32.
    发明申请
    Method of making a fecraI material and such material 有权
    制作fecraI材料和这种材料的方法

    公开(公告)号:US20030089198A1

    公开(公告)日:2003-05-15

    申请号:US10168860

    申请日:2002-10-16

    Abstract: A method of producing an FeCrAl material by gas atomization, wherein in addition to containing iron (Fe), chromium (Cr) and aluminium (Al) the material also contains minor fractions of one or more of the materials molybdenum (Mo), hafnium (Hf), zirconium (Zr), yttrium (Y), nitrogen (N), carbon (C) and oxygen (O). The invention is characterized by causing the smelt to be atomized to contain 0.05-0.50 percent by weight tantalum (Ta) and, at the same time, less than 0.10 percent by weight titanium (Ti). According to one highly preferred embodiment, nitrogen gas (N2) is used as an atomizing gas to which a given amount of oxygen gas (O2) is added, said amount of oxygen gas being such as to cause the atomized powder to contain 0.02-0.10 percent by weight oxygen (O) at the same time as the nitrogen content of the powder is 0.01-0.06 percent by weight. The invention also relates to a high temperature material.

    Abstract translation: 通过气体雾化生产FeCrAl材料的方法,其中除了含有铁(Fe),铬(Cr)和铝(Al)外,该材料还含有一种或多种钼(Mo),铪(Mo Hf),锆(Zr),钇(Y),氮(N),碳(C)和氧(O)。 本发明的特征在于使熔体雾化含有0.05-0.50重量%的钽(Ta),同时小于0.10重量%的钛(Ti)。 根据一个高度优选的实施方案,使用氮气(N 2)作为添加了给定量的氧气(O 2)的雾化气体,所述氧气量使得雾化粉末含有0.02-0.10 在粉末的氮含量的同时,氧(O)的重量百分比为0.01-0.06重量%。 本发明还涉及高温材料。

    Undercooled liquid metallic droplets having a protective shell

    公开(公告)号:US12030126B2

    公开(公告)日:2024-07-09

    申请号:US17383150

    申请日:2021-07-22

    CPC classification number: B22F9/06 B22F2201/01 B22F2201/03

    Abstract: A droplet comprises a core including an alloy comprising a majority of a first metallic element and a minority of a second element, wherein the core is in a liquid state below a solidus temperature of the alloy. A shell is arranged to enclose the core and includes an exterior surface comprising a majority of the second element and a minority of the first metallic element, wherein the shell is in a solid state below the solidus temperature of the alloy. The alloy can comprise a solder material that can be used to form solder connections below a solidus temperature of the alloy.

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