Dual crosslinkable emulsion polymers at ambient conditions
    42.
    发明授权
    Dual crosslinkable emulsion polymers at ambient conditions 有权
    双重交联乳液聚合物在环境条件下

    公开(公告)号:US06426121B1

    公开(公告)日:2002-07-30

    申请号:US09816305

    申请日:2001-03-23

    Abstract: This invention relates to a dual crosslinkable polymer/crosslinking system particularly suited for use in preparing high quality nonwoven products. The polymeric binders incorporate at least two different but reactive functionalities, i.e., hydroxy and carboxyl, and which are capable of reacting with two other multifunctional reactants, i.e., polyaldehydes and aziridines, each of which reacts with at least one of the functionalities present in the polymer. This selection of reactive functionality coupled with the selection of crosslinking agents permits ambient temperature cure.

    Abstract translation: 本发明涉及特别适用于制备高品质非织造布产品的双交联聚合物/交联体系。 聚合物粘合剂包含至少两种不同但反应性的官能团,即羟基和羧基,并且它们能够与另外两种多官能反应物反应,所述多官能反应物即聚醛和氮丙啶各自与至少一种官能团反应 聚合物。 反应性功能的选择与交联剂的选择相结合允许环境温度固化。

    Tartaric acid diesters as biodegradable surfactants
    43.
    发明授权
    Tartaric acid diesters as biodegradable surfactants 失效
    酒石酸二酯作为可生物降解的表面活性剂

    公开(公告)号:US06423376B1

    公开(公告)日:2002-07-23

    申请号:US09544671

    申请日:2000-04-06

    Abstract: This invention provides water-based compositions which are essentially free of hydrocarbon solvents, particularly coating, ink, fountain solution, adhesive and agricultural compositions, manifesting reduced equilibrium and dynamic surface tension by the incorporation of a surface tension reducing amount of certain tartrate diester compounds of the structure where R1 and R2 are C4 to C6 alkyl groups.

    Abstract translation: 本发明提供了基本上不含烃溶剂,特别是涂料,油墨,润版液,粘合剂和农业组合物的水基组合物,通过结合表面张力降低量的某些酒石酸二酯化合物表现出减少的平衡和动态表面张力 其中R1和R2是C4-C6烷基的结构。

    Method of preparing low-temperature-cure polymer composition
    45.
    发明授权
    Method of preparing low-temperature-cure polymer composition 失效
    制备低温固化聚合物组合物的方法

    公开(公告)号:US06416819B1

    公开(公告)日:2002-07-09

    申请号:US09608289

    申请日:2000-06-30

    Abstract: A method of preparing a composition containing a fluorocarbon thermoplastic random copolymer comprising the steps of: (A) providing a mixture having: (i) a fluorocarbon thermoplastic random copolymer having subunits of: —(CH2CF2)x—, —(CF2CF(CF3)y—, and —(CF2 CF2)z—,  wherein x is from 1 to 50 or 60 to 80 mole percent, y is from 10 to 90 mole percent, z is from 10 to 90 mole percent, x+y+z equals 100 mole percent; (ii) a filler comprising zinc oxide; (iii) a curable amino functional polydimethyl siloxane copolymer comprising aminofunctional units selected from the group consisting of (aminoethylaminopropyl) methyl, (aminopropyl) methyl and (aminopropyl) dimethyl; and (iv) antimony-doped tin oxide particles; (v) a bisphenol residue curing agent; and (B) curing the mixture for 5 to 10 hours at a temperature in the range of 25° C. to 275° C.

    Abstract translation: 一种制备含有碳氟化合物热塑性无规共聚物的组合物的方法,包括以下步骤:(A)提供具有以下物质的混合物:(i)具有亚基的氟碳热塑性无规共聚物,其中x为1至50或60至80摩尔% y为10至90摩尔%,z为10至90摩尔%,x + y + z为100摩尔%;(ii)包含氧化锌的填料;(iii)可固化的氨基官能的聚二甲基硅氧烷共聚物,其包含氨基官能单元 选自(氨基乙基氨基丙基)甲基,(氨基丙基)甲基和(氨基丙基)二甲基; 和(iv)锑掺杂氧化锡颗粒;(v)双酚残余固化剂; 和(B)在25℃至275℃的温度下固化混合物5至10小时。

    Method for making surfactant-templated thin films
    47.
    发明授权
    Method for making surfactant-templated thin films 有权
    制备表面活性剂模板薄膜的方法

    公开(公告)号:US06387453B1

    公开(公告)日:2002-05-14

    申请号:US09517873

    申请日:2000-03-02

    CPC classification number: B82Y30/00

    Abstract: An evaporation-induced self-assembly method to prepare a porous, surfactant-templated, thin film by mixing a silica sol, a solvent, a surfactant, and an interstitial compound, evaporating a portion of the solvent to form a liquid, crystalline thin film mesophase material, and then removal of the surfactant template. Coating onto a substrate produces a thin film with the interstitial compound either covalently bonded to the internal surfaces of the ordered or disordered mesostructure framework or physically entrapped within the ordered or disordered mesostructured framework. Particles can be formed by aerosol processing or spray drying rather than coating onto a substrate. The selection of the interstitial compound provides a means for developing thin films for applications including membranes, sensors, low dielectric constant films, photonic materials and optical hosts.

    Abstract translation: 通过混合硅溶胶,溶剂,表面活性剂和间隙化合物制备多孔表面活性剂模板化薄膜的蒸发诱导自组装方法,蒸发溶剂的一部分以形成液体,晶体薄膜 中间相材料,然后除去表面活性剂模板。 涂覆在基材上产生薄膜,其中间隙化合物共价键合到有序或无序的介观结构框架的内表面或物理地截留在有序或无序的介观结构框架内。 颗粒可以通过气溶胶处理或喷雾干燥形成,而不是涂覆在基材上。 间隙化合物的选择提供了一种用于开发用于包括膜,传感器,低介电常数膜,光子材料和光学主体的薄膜的薄膜的方法。

    Compositions and methods to protect calcitic and/or siliceous materials
    49.
    发明授权
    Compositions and methods to protect calcitic and/or siliceous materials 失效
    保护方解石和/或硅质材料的组合物和方法

    公开(公告)号:US06383569B2

    公开(公告)日:2002-05-07

    申请号:US09782109

    申请日:2001-02-13

    Abstract: Calcitic and/or siliceous particulate materials are provided with increased resistance to penetration by water, oil or grease damage from water, oil or grease by a process which comprises treating said materials with an aqueous composition containing: (A) from about 0.1 to 4% by weight on a 100% solids basis of an aqueous solution or self-dispersed emulsion or dispersion of a copolymer which is a reaction product of monomers containing fluorinated groups, cationic groups and nonionic groups, optionally (B) an effective amount of a penetration assistant, and (C) water to make up 100%.

    Abstract translation: 方解石和/或硅质颗粒材料通过包括用含有以下组分的水性组合物处理所述材料的方法提供了对水,油或油脂的水,油或油脂损伤的渗透性的增加的抵抗力:(A)约0.1至4% 以100%固体为基准的水溶液或自分散乳液或作为含氟化基团,阳离子基团和非离子基团的单体的反应产物的共聚物的分散体,任选地(B)有效量的渗透助剂 ,(C)水补足100%。

    Method of coating fuser member with thermoplastic containing zinc oxide and aminosiloxane
    50.
    发明授权
    Method of coating fuser member with thermoplastic containing zinc oxide and aminosiloxane 失效
    用含氧化锌和氨基硅氧烷的热塑性涂层定影器构件的方法

    公开(公告)号:US06361829B1

    公开(公告)日:2002-03-26

    申请号:US09607418

    申请日:2000-06-30

    Abstract: A method of making a fuser member having a support comprising the steps of: a) providing a support; b) coating from an organic solvent onto said support a coating composition comprising a fluorocarbon thermoplastic random copolymer, a curing agent having a bisphenol residue, a particulate filler containing zinc oxide, and an aminosiloxane, the fluorocarbon thermoplastic random copolymer having subunits of: —(CH2CF2)x—, —(CF2CF(CF3)y—, and —(CF2CF2)z—, wherein  x is from 1 to 50 or 60 to 80 mole percent,  y is from 10 to 90 mole percent,  z is from 10 to 90 mole percent,  x+y+z equals 100 mole percent; and (c) curing the coating composition for 3 to 10 hours at a temperature in the range of 220° C. to 280° C. and for an additional 2 to 10 hours at a temperature in the range of 250° C. to 270° C.

    Abstract translation: 一种制造具有支撑体的定影器构件的方法,包括以下步骤:a)提供支撑体; b)将有机溶剂涂覆到所述载体上,所述涂料组合物包含氟碳热塑性无规共聚物,具有双酚残基的固化剂, 含有氧化锌的颗粒填料和氨基硅氧烷,所述氟碳热塑性无规共聚物具有亚单位:其中x为1至50或60至80摩尔%,y为10至90摩尔%,z为10至90摩尔% ,x + y + z等于100摩尔% 和(c)在220℃至280℃的温度范围内将涂料组合物固化3至10小时,并在250℃至270℃的温度下再固化2至10小时 C。

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