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    Process and apparatus for a nanovoided article
    71.
    发明授权
    Process and apparatus for a nanovoided article 有权
    用于纳米复合制品的方法和装置

    公开(公告)号：US08808811B2

    公开(公告)日：2014-08-19

    申请号：US13262933

    申请日：2010-03-26

    Applicant: William Blake Kolb ,  Encai Hao ,  Brant U. Kolb ,  David L. Phillips

    Inventor： William Blake Kolb ,  Encai Hao ,  Brant U. Kolb ,  David L. Phillips

    IPC: B05D5/00 ,  C08F2/48 ,  C08J9/28

    CPC classification number: C08J9/28 ,  C08J2201/05 ,  C08J2333/06 ,  F26B13/10

    Abstract: A process and apparatus for producing a nanovoided article, a nanovoided coating, and a low refractive index coating is described. The process includes providing a first solution of a polymerizable material in a solvent; at least partially polymerizing the polymerizable material to form a composition that includes an insoluble polymer matrix and a second solution, wherein the insoluble polymer matrix includes a plurality of nanovoids that are filled with the second solution; and removing a major portion of the solvent from the second solution. An apparatus for the process is also described, and includes a webline, a coating section, a partial polymerization section, and a solvent removal section.

    Abstract translation: 描述了用于制备纳米复合制品，纳米复合涂层和低折射率涂层的方法和装置。 该方法包括在溶剂中提供可聚合材料的第一溶液; 至少部分地聚合所述可聚合材料以形成包含不溶性聚合物基质和第二溶液的组合物，其中所述不溶性聚合物基质包括填充有所述第二溶液的多个纳米泡; 并从第二溶液中除去大部分溶剂。 还描述了用于该方法的装置，并且包括纤维网，涂布部分，部分聚合部分和溶剂去除部分。

    POROUS ORGANIC POLYMERIC FILMS AND PREPARATION
    72.
    发明申请
    POROUS ORGANIC POLYMERIC FILMS AND PREPARATION 有权
    多孔有机聚合物膜和制备

    公开(公告)号：US20140147647A1

    公开(公告)日：2014-05-29

    申请号：US13686942

    申请日：2012-11-28

    Applicant: Mridula Nair ,  Tamara K. Jones

    Inventor： Mridula Nair ,  Tamara K. Jones

    IPC: C09D101/08

    CPC classification number: C08J9/28 ,  A61L15/225 ,  A61L15/425 ,  B05D3/02 ,  C08F2/32 ,  C08J5/18 ,  C08J9/0061 ,  C08J9/0071 ,  C08J9/283 ,  C08J2201/05 ,  C08J2367/04 ,  C08J2375/06 ,  C08J2401/10 ,  C08J2467/04 ,  C09D101/08 ,  Y10T428/249953 ,  Y10T428/249986

    Abstract: Porous organic polymeric films having multiple discrete cavities can be prepared using an water-in-oil emulsion that includes a cavity stabilizing hydrocolloid on the inner walls of the multiple discrete cavities. The multiple discrete cavities can also include organic catalytic materials for various catalytic reactions, markers materials for security applications, or the multiple discrete cavities can be used to increase opacity, hydrophobicity, or other desirable properties compared to nonporous organic polymeric films composed of the composition and dry thickness.

    Abstract translation: 具有多个离散空腔的多孔有机聚合物膜可以使用油包水乳液制备，其包括在多个分立空腔的内壁上的腔稳定水胶体。 多个分立的空腔还可以包括用于各种催化反应的有机催化材料，用于安全应用的标记材料或多个离散空腔可用于增加不透明度，疏水性或其它所需的性能，与由组合物组成的无孔有机聚合物膜相比， 干厚度。

    POROUS PARTICLES WITH IMPROVED FILTERING PERFORMANCE
    74.
    发明申请
    POROUS PARTICLES WITH IMPROVED FILTERING PERFORMANCE 审中-公开
    具有改进过滤性能的多孔颗粒

    公开(公告)号：US20120136080A1

    公开(公告)日：2012-05-31

    申请号：US12956022

    申请日：2010-11-30

    Applicant: Xiqiang Yang ,  James R. Bennett

    Inventor： Xiqiang Yang ,  James R. Bennett

    IPC: C08J9/28 ,  C08B15/00 ,  C08B37/02 ,  C08B3/00

    CPC classification number: C08J9/28 ,  C08B11/12 ,  C08J2201/05 ,  C08L1/284 ,  C08L1/286 ,  C08L5/02 ,  C08L33/26

    Abstract: A method of manufacturing porous polymer particles with improved filterability is described. One or more first water phases are formed comprising an anionic hydrocolloid with a mass-per-charge value of less than 600 and a relatively minor amount, compared to the anionic hydrocolloid, of at least one of a nonionic, cationic, zwitterionic, or weakly anionic water soluble or dispersible polymer, where the weakly anionic water soluble or dispersible polymer has a mass-per-charge value of larger than 600. A water-in-oil emulsion is formed by dispersing the one or more first water phases into an organic phase comprising at least one of either (i) preformed polymer dissolved in an organic solvent or (ii) polymerizable monomers, and homogenizing. A water-in-oil-in-water multiple emulsion is formed by dispersing the water-in-oil emulsion into a second water phase containing a stabilizing agent and homogenizing. The organic solvent is removed to precipitate the preformed polymer, or the polymerizable monomers are polymerized, to obtain a dispersion of porous polymer particles in an external aqueous phase, wherein individual porous particles each comprise a continuous polymer phase and internal pores containing an internal aqueous phase. The dispersion of porous polymer particles is filtered to remove the external aqueous phase. The method enables increased filtration rates of porous polymer particle dispersions containing water in the pores.

    Abstract translation: 描述了制造具有改进的过滤性的多孔聚合物颗粒的方法。 形成一个或多个第一水相，其包含阴离子水胶体，每批电荷值小于600，并且与阴离子水胶体相比，非离子，阳离子，两性离子或弱的至少一种 阴离子水溶性或可分散的聚合物，其中弱阴离子水溶性或可分散聚合物的每次电荷值大于600.通过将一个或多个第一水相分散到有机物中形成油包水乳液 包含（i）预先形成的聚合物溶解在有机溶剂中的至少一种或（ii）可聚合单体，并均化。 通过将油包水乳液分散到含有稳定剂的第二水相中并均化来形成水包油包水多重乳液。 去除有机溶剂以沉淀预制的聚合物，或聚合单体，得到多孔聚合物颗粒在外部水相中的分散体，其中各个多孔颗粒各自包含连续聚合物相和含有内部水相的内孔 。 过滤多孔聚合物颗粒的分散体以除去外部水相。 该方法能够增加在孔中含有水的多孔聚合物颗粒分散体的过滤速率。

    PROCESS FOR PRODUCING POROUS MATERIALS BASED ON POLYUREA
    75.
    发明申请
    PROCESS FOR PRODUCING POROUS MATERIALS BASED ON POLYUREA 有权
    基于聚氨酯生产多孔材料的工艺

    公开(公告)号：US20110319508A1

    公开(公告)日：2011-12-29

    申请号：US13169245

    申请日：2011-06-27

    Applicant: Marc Fricke ,  Mark Elbing

    Inventor： Marc Fricke ,  Mark Elbing

    IPC: C08G18/32 ,  C08J9/28

    CPC classification number: C08J9/28 ,  C08G18/3243 ,  C08G2101/0083 ,  C08G2101/0091 ,  C08J2201/05 ,  C08J2201/0502 ,  C08J2203/10 ,  C08J2205/024 ,  C08J2375/04

    Abstract: The present invention relates to a process for producing porous materials, which comprises reaction of at least one polyfunctional isocyanate with an amine component comprising at least one polyfunctional substituted aromatic amine and also water in the presence of a solvent.The invention further relates to the porous materials which can be obtained in this way and the use of the porous materials as insulation material and in vacuum insulation panels,

    Abstract translation: 本发明涉及一种生产多孔材料的方法，其包括至少一种多官能异氰酸酯与包含至少一种多官能取代的芳族胺的胺组分以及在溶剂存在下的水的反应。 本发明还涉及可以以这种方式获得的多孔材料以及多孔材料作为绝缘材料和真空绝热板的用途，

    METHOD OF MAKING POROUS PARTICLES
    79.
    发明申请
    METHOD OF MAKING POROUS PARTICLES 有权
    制造多孔颗粒的方法

    公开(公告)号：US20080268367A1

    公开(公告)日：2008-10-30

    申请号：US11739121

    申请日：2007-04-24

    Applicant: Mridula Nair ,  Xiqiang Yang ,  Tamara K. Jones ,  James G. Popowych

    Inventor： Mridula Nair ,  Xiqiang Yang ,  Tamara K. Jones ,  James G. Popowych

    IPC: G03G5/00

    CPC classification number: C08J3/14 ,  C08J9/28 ,  C08J2201/05 ,  G03G9/0806 ,  G03G9/0827

    Abstract: The present invention is a method for the preparation of porous particles that includes dissolving a polymer material in a first organic solvent and adding a second organic solvent and nonionic organic polymer particles to form an organic phase. The organic phase is dispersed in an aqueous phase that includes a particulate stabilizer to form a dispersion and the dispersion is homogenized. The first and second organic solvents are evaporated and the product is recovered.

    Abstract translation: 本发明是一种制备多孔颗粒的方法，其包括将聚合物材料溶解在第一有机溶剂中并加入第二有机溶剂和非离子有机聚合物颗粒以形成有机相。 将有机相分散在包含微粒稳定剂的水相中以形成分散体，并将分散体均化。 将第一和第二有机溶剂蒸发并回收产物。

    Preparation of hydrophobic organic aeorgels
    80.
    发明授权
    Preparation of hydrophobic organic aeorgels 失效
    疏水性有机物的制备

    公开(公告)号：US07291653B2

    公开(公告)日：2007-11-06

    申请号：US10927679

    申请日：2004-08-26

    Applicant: Theodore F. Baumann ,  Joe H. Satcher, Jr. ,  Alexander E. Gash

    Inventor： Theodore F. Baumann ,  Joe H. Satcher, Jr. ,  Alexander E. Gash

    IPC: C08J9/28

    CPC classification number: C08J9/28 ,  C08J2201/05 ,  C08J2203/08 ,  C08J2361/02 ,  Y02P20/544

    Abstract: Synthetic methods for the preparation of hydrophobic organics aerogels. One method involves the sol-gel polymerization of 1,3-dimethoxybenzene or 1,3,5-trimethoxybenzene with formaldehyde in non-aqueous solvents. Using a procedure analogous to the preparation of resorcinol-formaldehyde (RF) aerogels, this approach generates wet gels that can be dried using either supercritical solvent extraction to generate the new organic aerogels or air dried to produce an xerogel. Other methods involve the sol-gel polymerization of 1,3,5 trihydroxy benzene (phloroglucinol) or 1,3 dihydroxy benzene (resorcinol) and various aldehydes in non-aqueous solvents. These methods use a procedure analogous to the one-step base and two-step base/acid catalyzed polycondensation of phloroglucinol and formaldehyde, but the base catalyst used is triethylamine. These methods can be applied to a variety of other sol-gel precursors and solvent systems. These hydrophobic organics aerogels have numerous application potentials in the field of material absorbers and water-proof insulation.

    Abstract translation: 制备疏水性有机物气凝胶的合成方法。 一种方法涉及1,3-二甲氧基苯或1,3,5-三甲氧基苯与甲醛在非水溶剂中的溶胶 - 凝胶聚合。 使用类似于间苯二酚 - 甲醛（RF）气凝胶的制备方法，该方法产生湿凝胶，其可以使用超临界溶剂萃取干燥以产生新的有机气凝胶或空气干燥以产生干凝胶。 其他方法涉及在非水溶剂中1,3,5-三羟基苯（间苯三酚）或1,3-二羟基苯（间苯二酚）和各种醛的溶胶 - 凝胶聚合。 这些方法使用类似于间苯三酚和甲醛的一步碱和两步碱/酸催化缩聚的方法，但所用的碱催化剂是三乙胺。 这些方法可以应用于各种其他溶胶 - 凝胶前体和溶剂体系。 这些疏水性有机气凝胶在材料吸收体和防水绝缘领域具有许多应用潜力。

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