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    Reactors for forming foam materials from high internal phase emulsions, methods of forming foam materials and conductive nanostructures therein
    2.
    发明授权
    Reactors for forming foam materials from high internal phase emulsions, methods of forming foam materials and conductive nanostructures therein 有权
    用于从高内相乳液形成泡沫材料的反应器，其中形成泡沫材料的方法和导电纳米结构

    公开(公告)号：US08475616B2

    公开(公告)日：2013-07-02

    申请号：US12794693

    申请日：2010-06-04

    Applicant: Wilmot H. McCutchen

    Inventor： Wilmot H. McCutchen

    IPC: B65H69/02 ,  C08J9/00

    CPC classification number: B01D39/16 ,  B01D33/0006 ,  B01D33/0041 ,  B01D33/0087 ,  B01D33/15 ,  B01D33/21 ,  B01D33/23 ,  B01D39/083 ,  B01D39/14 ,  B01D39/1638 ,  B01D2239/025 ,  B01D2239/0258 ,  B01F7/00875 ,  B01J19/20 ,  C08F2/32 ,  C08J9/0066 ,  C08J9/0071 ,  C08J9/228 ,  C08J9/28 ,  C08J2201/028

    Abstract: An RF inductor such as a Tesla antenna splices nanotube ends together to form a nanostructure in a polymer foam matrix. High Internal Phase Emulsion (HIPE) is gently sheared and stretched in a reactor comprising opposed coaxial counter-rotating impellers, which parallel-align polymer chains and also carbon nanotubes mixed with the oil phase. Stretching and forced convection prevent the auto-acceleration effect. Batch and continuous processes are disclosed. In the batch process, a fractal radial array of coherent vortices in the HIPE is preserved when the HIPE polymerizes, and helical nanostructures around these vortices are spliced by microhammering into longer helices. A disk radial filter produced by the batch process has improved radial flux from edge to center due to its area-preserving radial vascular network. In the continuous process, strips of HIPE are pulled from the periphery of the reactor continuously and post-treated by an RF inductor to produce cured conductive foam.

    Abstract translation: 诸如特斯拉天线的RF电感器将纳米管接合在一起以在聚合物泡沫基质中​​形成纳米结构。 将高内相乳液（HIPE）在包括相对的同向反向旋转叶轮的反应器中轻轻地剪切和拉伸，其平行对准聚合物链以及与油相混合的碳纳米管。 拉伸和强制对流防止自动加速效应。 公开了批量和连续过程。 在间歇过程中，当HIPE聚合时，HIPE中的相干旋涡的分形径向阵列被保留，并且围绕这些涡流的螺旋纳米结构通过微型加工被剪接成更长的螺旋。 通过间歇法生产的盘式径向过滤器由于其面积保持的径向血管网络而具有从边缘到中心的径向通量。 在连续过程中，HIPE条被连续地从反应器的外围拉出，并由RF电感器进行后处理以产生固化的导电泡沫。

    Method for production of porous material
    6.
    发明授权
    Method for production of porous material 有权
    多孔材料的生产方法

    公开(公告)号：US06822010B2

    公开(公告)日：2004-11-23

    申请号：US10474950

    申请日：2003-10-14

    Applicant: Hirotama Fujimaru ,  Hiroki Inoue ,  Kenji Kadonaga ,  Kinya Nagasuna

    Inventor： Hirotama Fujimaru ,  Hiroki Inoue ,  Kenji Kadonaga ,  Kinya Nagasuna

    IPC: C08J928

    CPC classification number: C08J9/28 ,  C08F2/32 ,  C08J2201/028

    Abstract: A method for producing a porous material excelling in stability of preservation is produced. A method for the production of a porous material comprising a step for obtaining a porous polymer by polymerizing an HIPE containing a polymerizable monomer is disclosed, which method comprises a step for adding a compound capable of reacting with a polymerization initiator and/or a compound capable of reacting with an unsaturated double bond to said emulsion, said porous polymer and/or said porous material having a conversion of not less than 70%. According to this invention, it is made possible to produce a porous material excelling in stability in storage and to decrease the polymerization initiator and the residual monomer very simply.

    Abstract translation: 制造出具有良好的保存稳定性的多孔材料的制造方法。 公开了一种生产多孔材料的方法，其包括通过聚合含有可聚合单体的HIPE获得多孔聚合物的步骤，该方法包括添加能够与聚合引发剂和/或化合物反应的化合物的步骤 与所述乳液的不饱和双键反应，所述多孔聚合物和/或所述多孔材料具有不小于70％的转化率。 根据本发明，可以制备出具有良好的储存稳定性的多孔材料，并且非常简单地降低聚合引发剂和残留单体。

    Process for producing porous polymer
    7.
    发明授权
    Process for producing porous polymer 有权

    公开(公告)号：US06797735B2

    公开(公告)日：2004-09-28

    申请号：US10332219

    申请日：2003-01-03

    Applicant: Kinya Nagasuna ,  Kenji Kadonaga ,  Hirotama Fujimaru ,  Kozo Nogi ,  Kenji Minami

    Inventor： Kinya Nagasuna ,  Kenji Kadonaga ,  Hirotama Fujimaru ,  Kozo Nogi ,  Kenji Minami

    IPC: C08J928

    CPC classification number: C08J9/28 ,  C08F2/32 ,  C08J2201/028 ,  C08J2201/0504 ,  C08J2333/06

    Abstract: A method of production is provided which is capable of efficiently producing in a very short period of time a porous polymer possessing a uniform foam structure and truly excelling in absorption properties and physical properties. It is a method for the production of a porous polymer, characterized by comprising (a) an emulsifying step for forming a water-in-oil type high internal phase emulsion (HIPE) by mixing and stirring an oil phase containing a polymerizing monomer component and a surfactant as essential components, (b) a shaping step for shaping the HIPE in a specific form, and (c) a polymerizing step for polymerizing the shaped HIPE and controlling the temperatures of the emulsion at the component steps (a)-(c) so that they may not produce a change exceeding 10° C. or controlling all the component steps so that they may proceed at temperatures of not lower than 80° C.

    Process for producing porous polymer
    8.
    发明申请
    Process for producing porous polymer 有权
    生产多孔聚合物的方法

    公开(公告)号：US20040002555A1

    公开(公告)日：2004-01-01

    申请号：US10332219

    申请日：2003-01-03

    Inventor： Kinya Nagasuna ,  Kenji Kadonaga ,  Hirotama Fujimaru ,  Kozo Nogi ,  Kenji Minami

    IPC: C08J009/00

    CPC classification number: C08J9/28 ,  C08F2/32 ,  C08J2201/028 ,  C08J2201/0504 ,  C08J2333/06

    Abstract: A method of production is provided which is capable of efficiently producing in a very short period of time a porous polymer possessing a uniform foam structure and truly excelling in absorption properties and physical properties. It is a method for the production of a porous polymer, characterized by comprising (a) an emulsifying step for forming a water-in-oil type high internal phase emulsion (HIPE) by mixing and stirring an oil phase containing a polymerizing monomer component and a surfactant as essential components, (b) a shaping step for shaping the HIPE in a specific form, and (c) a polymerizing step for polymerizing the shaped HIPE and controlling the temperatures of the emulsion at the component steps (a)-(c) so that they may not produce a change exceeding 10null C. or controlling all the component steps so that they may proceed at temperatures of not lower than 80null C.

    Abstract translation: 提供了一种生产方法，其能够在非常短的时间内有效地生产具有均匀泡沫结构并且真正优异的吸收性能和物理性能的多孔聚合物。 本发明是一种生产多孔聚合物的方法，其特征在于包括：（a）通过混合并搅拌含有聚合单体成分的油相和（b）形成油包水型高内相乳液（HIPE）的乳化步骤， 作为必要成分的表面活性剂，（b）用于使特定形式的HIPE成形的成型步骤，和（c）聚合步骤（a） - （c）的聚合步骤，用于使成形HIPE聚合并控制乳液的温度 ），使得它们不会产生超过10℃的变化，或控制所有组分步骤，使其可以在不低于80℃的温度下进行。

    Process for producing porous polymer
    10.
    发明申请
    Process for producing porous polymer 有权
    生产多孔聚合物的方法

    公开(公告)号：US20020193510A1

    公开(公告)日：2002-12-19

    申请号：US10149776

    申请日：2002-06-13

    Inventor： Kenji Kadonaga ,  Kenji Minami

    IPC: C08K003/00

    CPC classification number: C08J9/36 ,  C08F2/32 ,  C08J2201/028

    Abstract: This invention, with the object of producing a porous polymer from a water-in-oil type high internal phase emulsion, provides a method for the production of a porous polymer comprising a step of applying a physical treatment such as shaving to the surface of a porous polymer obtained by polymerizing the emulsion. By the physical treatment, it is made possible to diminish the difference in texture between the surface part and the inner part of the porous polymer and improve efficiently the absorption property of the porous polymer.

    Abstract translation: 本发明的目的是从油包水型高内相乳液制备多孔聚合物，提供了一种生产多孔聚合物的方法，包括如下步骤：将物理处理如剃须物质 通过聚合乳液获得的多孔聚合物。 通过物理处理，有可能减少多孔聚合物的表面部分和内部之间的质地差异，并且有效地提高多孔聚合物的吸收性能。

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