公开(公告)号：US20170312728A1

公开(公告)日：2017-11-02

申请号：US15447250

申请日：2017-03-02

Applicant: CEM Corporation

Inventor： IAN GOLDSTEIN ,  WYATT P. HARGETT, III

IPC: B01J19/02 ,  B01J19/12 ,  B01J19/24

CPC classification number: B01J19/02 ,  B01J3/03 ,  B01J3/042 ,  B01J19/126 ,  B01J19/24 ,  B01J2219/00141 ,  B01J2219/00162 ,  B01J2219/0295 ,  B01J2219/1218 ,  B01J2219/1224 ,  B01J2219/1227 ,  B01J2219/1233 ,  B01J2219/1236 ,  B01J2219/1943 ,  B01J2219/24

Abstract: A vessel system for high-pressure reactions is disclosed. The system includes a plugged polymer cylinder reaction vessel with a pressure vent opening extending radially through the wall of the reaction vessel and a supporting frame into which the vessel is received. Complementing keying structure elements on the vessel and on the frame limit the orientation of the reaction vessel in the supporting frame and the radially extending vent opening to a defined single position.

公开(公告)号：US20170081779A1

公开(公告)日：2017-03-23

申请号：US15269538

申请日：2016-09-19

Applicant: SORAA, INC.

Inventor： MARK PHILIP D'EVELYN ,  RAJEEV TIRUMALA PAKALAPATI

IPC: C30B7/10 ,  C30B29/40

CPC classification number: B01J3/008 ,  B01J3/042 ,  B08B7/0021 ,  C30B7/10 ,  C30B35/002 ,  Y02P20/544

Abstract: A pressure release mechanism for use with a capsule for processing materials or growing crystals in supercritical fluids is disclosed. The capsule with the pressure release mechanism is scalable up to very large volumes and is cost effective according to a preferred embodiment. In conjunction with suitable high pressure apparatus, the capsule with pressure release mechanism is capable of processing materials at pressures and temperatures of 20-2000 MPa and 25-1500° C., respectively. Of course, there can be other variations, modifications, and alternatives.

公开(公告)号：US20170015636A1

公开(公告)日：2017-01-19

申请号：US15123924

申请日：2015-03-09

Applicant: Casale SA

Inventor： Enrico Rizzi

IPC: C07D251/60 ,  B01J3/02 ,  B01J3/04

CPC classification number: C07D251/60 ,  B01J3/02 ,  B01J3/04 ,  B01J3/042 ,  B01J4/002 ,  B01J10/005 ,  B01J19/246 ,  B01J2219/00078 ,  B01J2219/00081 ,  C07D251/62

Abstract: Reactor for the synthesis of melamine from urea, in accordance with the high-pressure non-catalytic process, comprising: a vertical reactor body (1), at least one inlet (2) for the urea melt, a set of heating elements (3), and a central duct (7), said set of heating elements (3) being arranged inside said central duct.

Abstract translation: 用于从尿素合成三聚氰胺的反应器，根据高压非催化方法，包括：垂直反应器主体（1），用于尿素熔体的至少一个入口（2），一组加热元件（3 ）和中央导管（7），所述一组加热元件（3）布置在所述中心导管的内部。

公开(公告)号：US20160168470A1

公开(公告)日：2016-06-16

申请号：US14569018

申请日：2014-12-12

Applicant: Sustainable Waste Power Systems, Inc.

Inventor： Michael Joseph Gillespie, III ,  Christopher Paul Gillespie

IPC: C10B5/10 ,  C10B41/00 ,  C10B47/18 ,  C10B45/00

CPC classification number: C10L9/086 ,  B01J3/042 ,  B01J19/2425 ,  B01J2219/0006 ,  B01J2219/00063 ,  B01J2219/00065 ,  B01J2219/00085 ,  B01J2219/00162 ,  B01J2219/0027 ,  C10J2300/0906 ,  C10J2300/0916 ,  C10J2300/1246 ,  C10J2300/1662 ,  C10L3/08 ,  C10L9/08 ,  C10L2290/04 ,  C10L2290/06 ,  C10L2290/28 ,  C10L2290/58 ,  C10L2290/60

Abstract: This disclosure relates to a system and method for devolatilizing a carbonaceous feedstock. The system includes a devolatilization reactor having a unit shell, at least one tube bundle, a pump, and a control valve. The unit shell is configured to allow a heating fluid to flow within. The at least one tube bundle is configured to allow the feedstock to flow within the tube bundle and further configured to be positioned at least partially within the unit shell. The tube bundle comprises at least one tube and at least one tube bend. The at least one tube bend is disposed external to the unit shell. The pump is configured to pump the feedstock into the at least one tube bundle. The control valve is configured to control the flow rate of feedstock into the at least one tube bundle.

Abstract translation: 本公开涉及用于使含碳原料脱挥发分的系统和方法。 该系统包括具有单位壳体，至少一个管束，泵和控制阀的脱挥发反应器。 单元壳体被配置成允许加热流体流入。 至少一个管束被配置成允许原料在管束内流动并进一步构造成至少部分地位于单元壳体内。 管束包括至少一个管和至少一个管弯曲部。 至少一个管弯头设置在单元外壳的外部。 泵配置成将原料泵入至少一个管束。 控制阀被配置为控制进入至少一个管束的进料的流量。

公开(公告)号：US09157167B1

公开(公告)日：2015-10-13

申请号：US13556105

申请日：2012-07-23

Applicant: Rajeev T. Pakalapati ,  Mark P. D'Evelyn

Inventor： Rajeev T. Pakalapati ,  Mark P. D'Evelyn

IPC: C30B7/10

CPC classification number: C30B7/10 ,  B01J3/008 ,  B01J3/042 ,  B01J3/065 ,  B01J2203/0665 ,  B01J2203/067 ,  B01J2203/068 ,  B30B11/002 ,  B30B11/005 ,  C30B29/403 ,  C30B29/406 ,  Y02P20/544 ,  Y10T117/10 ,  Y10T117/1024 ,  Y10T117/1096

Abstract: A high pressure apparatus and related methods for processing supercritical fluids are disclosed. In certain embodiments, the present apparatus includes a capsule, a heater, at least one ceramic ring or multiple rings, optionally, with one or more scribe marks and/or cracks present. In certain embodiments, the apparatus has a metal sleeve containing each ceramic ring. The apparatus also has a high strength enclosure, end flanges with associated insulation, and a power control system. In certain embodiments, a high pressure apparatus is constructed such that the diametric annular gap between the outer diameter of the heater and the ceramic ring is selected to provide radial load-bearing contact above a particular temperature and pressure. In certain embodiments, the apparatus is capable of accessing pressures of 0.2 GPa to 2 GPa and temperatures of 400° C. to 1200° C.

Abstract translation: 公开了一种用于加工超临界流体的高压装置和相关方法。 在某些实施方案中，本装置包括胶囊，加热器，至少一个陶瓷环或多个环，任选地，存在一个或多个划痕和/或裂纹。 在某些实施例中，该装置具有包含每个陶瓷环的金属套筒。 该设备还具有高强度外壳，具有相关绝缘的端部法兰和功率控制系统。 在某些实施例中，高压设备被构造成使得加热器外径与陶瓷环之间的直径环形间隙被选择成在特定温度和压力之上提供径向承载接触。 在某些实施方案中，该装置能够获得0.2GPa至2GPa的压力和400℃至1200℃的温度。

公开(公告)号：US08038958B2

公开(公告)日：2011-10-18

申请号：US11995397

申请日：2006-07-12

Applicant: Fumihiko Kasuya ,  Masahiro Yamagata ,  Shigetoshi Suzuki ,  Tadashi Yoshida

Inventor： Fumihiko Kasuya ,  Masahiro Yamagata ,  Shigetoshi Suzuki ,  Tadashi Yoshida

IPC: B01J3/00 ,  B01J19/00

CPC classification number: B01J19/20 ,  B01J3/02 ,  B01J3/042 ,  B01J19/006 ,  B01J2219/00772 ,  B01J2219/185 ,  B01J2219/1943 ,  C07C209/62 ,  C07C2601/14 ,  C07C211/12 ,  C07C211/18 ,  C07C211/27 ,  C07C211/36 ,  C07C211/46 ,  C07C211/50 ,  C07C211/51 ,  C07C211/58

Abstract: The present invention relates to a method for decomposing and recovering an isocyanate compound, which comprises: continuously mixing and dispersing into water at high pressure and high temperature an isocyanate compound having at least one isocyanate group or group derived from an isocyanate group in a molten state or solution state, supplying a liquid mixture containing the isocyanate compound and the water at high pressure and high temperature continuously to a reactor, followed by subjecting the isocyanate compound to a decomposition reaction in the reactor, and recovering a raw material for the isocyanate compound or a derivative thereof; and an apparatus for decomposing and recovering an isocyanate compound, which comprises: a reactor which brings water at high pressure and high temperature into contact with an isocyanate compound having at least one isocyanate group or group derived from an isocyanate group to cause a decomposition reaction, a water supply line which continuously supplies the water at high pressure and high temperature to a reactor, a compound supply line which continuously supplies the isocyanate compound in a molten state or solution state to the water supply line, an on-off valve which communicates the compound supply line with a vicinity of a communication portion of the water supply line to the reactor, a dehydrating device which conducts a dehydration of a decomposition reaction product discharged from the reactor, and a purification device which purifies the decomposition reaction product after the dehydration.

Abstract translation: 本发明涉及一种分解和回收异氰酸酯化合物的方法，包括：在高压和高温下连续混合和分散在具有至少一种异氰酸酯基团或衍生自异氰酸酯基团的基团的异氰酸酯化合物处于熔融状态 或溶液状态，将含有异氰酸酯化合物和水的液体混合物在高压高温下连续供给反应器，然后使异氰酸酯化合物在反应器中进行分解反应，并回收异氰酸酯化合物的原料或 其衍生物; 以及用于分解和回收异氰酸酯化合物的装置，其包括：使高压高温水与具有至少一个异氰酸酯基的异氰酸酯化合物或衍生自异氰酸酯基团的异氰酸酯化合物接触引起分解反应的反应器， 向反应器连续供给高压高温的水的供水管线，向熔融状态或溶液状态连续供给异氰酸酯化合物的供给管线，供给管路，其将 化合物供给管线，与供水管路的连通部分邻近反应器，将从反应器排出的分解反应产物脱水的脱水装置，以及在脱水后净化分解反应产物的净化装置。

公开(公告)号：US20100031875A1

公开(公告)日：2010-02-11

申请号：US12534844

申请日：2009-08-03

Applicant: MARK P. D'EVELYN

Inventor： MARK P. D'EVELYN

IPC: C30B7/10

CPC classification number: C30B29/406 ,  B01J3/008 ,  B01J3/042 ,  B01J3/065 ,  B01J2203/0665 ,  B01J2203/068 ,  B30B11/002 ,  C30B7/10

Abstract: A method for large-scale manufacturing of gallium nitride boules. Large-area single crystal seed plates are suspended in a rack, placed in a large diameter autoclave or internally-heated high pressure apparatus along with ammonia and a mineralizer, and grown ammonothermally. The seed orientation and mounting geometry are chosen to provide efficient utilization of the seed plates and of the volume inside the autoclave or high pressure apparatus. The method is scalable up to very large volumes and is cost effective.

Abstract translation: 一种大规模生产氮化镓颗粒的方法。 将大面积单晶种子板悬挂在机架中，与氨和矿化剂一起放置在大直径的高压釜或内部加热的高压装置中，并进行氨热生长。 选择种子取向和安装几何形状以提供有效利用种子板和高压釜或高压装置内的体积。 该方法可扩展到非常大的卷，并且具有成本效益。

公开(公告)号：US20090301387A1

公开(公告)日：2009-12-10

申请号：US12133364

申请日：2008-06-05

Applicant: MARK P. D'EVELYN

Inventor： MARK P. D'EVELYN

IPC: C30B19/08

CPC classification number: C30B29/406 ,  B01J3/008 ,  B01J3/042 ,  B01J3/065 ,  B01J2203/0665 ,  B01J2203/067 ,  B01J2203/068 ,  B30B11/005 ,  C30B7/10 ,  C30B29/403 ,  Y02P20/544 ,  Y10T117/10 ,  Y10T117/1024 ,  Y10T117/1096

Abstract: A high pressure apparatus and related methods for processing supercritical fluids. In a specific embodiment, the present apparatus includes a capsule, a heater, at least one ceramic ring but can be multiple rings, optionally, with one or more scribe marks and/or cracks present. In a specific embodiment, the apparatus optionally has a metal sleeve containing each ceramic ring. The apparatus also has a high-strength enclosure, end flanges with associated insulation, and a power control system. IN a specific embodiment, the apparatus is capable of accessing pressures and temperatures of 0.2-2 GPa and 400-1200° C., respectively.

Abstract translation: 一种用于加工超临界流体的高压装置及相关方法。 在具体实施例中，本装置包括胶囊，加热器，至少一个陶瓷环，但可以是多个环，任选地，存在一个或多个划痕和/或裂纹。 在具体实施例中，该装置可选地具有包含每个陶瓷环的金属套筒。 该设备还具有高强度外壳，具有相关绝缘的端部法兰和电源控制系统。 在具体实施例中，该装置能够分别访问0.2-2GPa和400-1200℃的压力和温度。

公开(公告)号：US07521029B2

公开(公告)日：2009-04-21

申请号：US10541698

申请日：2003-01-31

Applicant: Friedrich Guetlhuber ,  Manfred Lehr

Inventor： Friedrich Guetlhuber ,  Manfred Lehr

IPC: F28D7/00 ,  B01J19/00 ,  B01J10/00 ,  B01J8/04 ,  G05D16/00

CPC classification number: B01J8/008 ,  B01J3/02 ,  B01J3/03 ,  B01J3/042 ,  B01J4/002 ,  B01J8/0085 ,  B01J8/065 ,  B01J8/067 ,  B01J19/002 ,  B01J19/0053 ,  B01J19/26 ,  B01J2208/00203 ,  B01J2208/00212 ,  B01J2208/00495 ,  B01J2208/0053 ,  B01J2208/00548 ,  B01J2208/00716 ,  B01J2208/00849 ,  B01J2219/00263 ,  B01J2219/00265 ,  C07C51/21 ,  F28D7/16 ,  F28F9/0229 ,  F28F9/0265 ,  F28F2225/08 ,  Y10T137/043 ,  Y10T137/1654

Abstract: The invention relates to a tubular reactor for carrying out catalytic gas-phase reactions, containing a catalyst tube bundle (8) that is traversed by the relevant reaction gas mixture, is filled with a catalyst, extends between two tube sheets (4, 148) and around which flows a heat transfer medium contained within a surrounding reactor jacket (6). The reactor also comprises gas entry and discharge hoods (2; 60) that cover the two tube sheets for supplying the relevant process gas to the catalyst tubes and for discharging the reacted process gas from the catalyst tubes. Together with all the parts that come into contact with the process gas mixture, the reactor is designed to have an appropriate strength for withstanding the deflagration and explosive pressures that are to be taken into account during its operation. The volume available to the process gas mixture prior to its entry into the catalyst tubes is restricted as much as possible in construction and flow engineering terms.

Abstract translation: 本发明涉及一种用于进行催化气相反应的管式反应器，其中包含由相关反应气体混合物穿过的催化剂管束（8），填充有催化剂，在两个管板（4,148）之间延伸， 并且在其周围流过包含在周围的反应器夹套（6）内的传热介质。 反应器还包括气体进入和排出罩（2; 60），其覆盖两个管板，用于将相关工艺气体供应到催化剂管并从催化剂管排出反应的工艺气体。 连同与工艺气体混合物接触的所有部件，反应器被设计为具有适当的强度，以承受在其操作期间要考虑的爆燃和爆炸压力。 过程气体混合物在其进入催化剂管之前可用的体积在结构和流程工程方面尽可能地受到限制。

公开(公告)号：US07473285B2

公开(公告)日：2009-01-06

申请号：US10239256

申请日：2001-03-23

Applicant: Richard W. Russell ,  Alfred H. Stiller

Inventor： Richard W. Russell ,  Alfred H. Stiller

IPC: C10L5/00

CPC classification number: B01J3/008 ,  B01J3/042 ,  B01J2219/00074 ,  B01J2219/00135 ,  C10G1/02 ,  C10G1/047 ,  C10G1/06 ,  C10G1/08 ,  Y02W30/43

Abstract: A method of making a liquid fuel from agricultural waste which may be animal manure, includes admixing agricultural waste with at least one material selected from the group consisting of hydrogen gas and water, at elevated pressure heating a mixture to about 300° C. to 400° C. for a predetermined time, subsequently cooling the mixture, and subsequently separating gas from liquid. The process produces a liquid fuel having a high heating BTU value per pound of fuel. The water preferably functions as both a solvent and the hydrogen donor for said agricultural waste. Corresponding apparatus is provided.

Abstract translation: 从农业废弃物制造液体燃料的方法可以是动物肥料，包括在升高的压力下将农业废物与选自氢气和水的至少一种材料混合加热至约300℃至400℃ ℃预定的时间，随后冷却混合物，随后将气体与液体分离。 该方法产生具有每磅燃料高的加热BTU值的液体燃料。 水优选用作所述农业废物的溶剂和氢供体。 提供相应的设备。