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1.发明申请公开(公告)号：US20170274346A1
公开(公告)日：2017-09-28
申请号：US15503855
申请日：2015-08-17
Applicant: BAYER AKTIENGESELLSCHAFT
Inventor： LESLAW MLECZKO , AUREL WOLF , RALF SCHELLEN , KONSTANTINOS METAXAS , JENS STEFAN ROGGAN
CPC classification number: B01J19/1893 , B01J19/0013 , B01J19/2475 , B01J31/0231 , B01J2219/00085 , B01J2523/31 , C01B7/01 , C01B31/28 , C01B32/80 , C01F7/02 , C07C68/02 , C07C263/10 , C07C69/96
Abstract: The invention relates to a method particularly for reacting phosgene with compounds that contain hydroxyl, thiol, amino and/or formamide groups, comprising the steps of: (I) providing a reactor which has a first reaction chamber (300, 310, 320, 330, 340, 350) and a second reaction chamber (200, 210, 220, 230, 240, 250, 260), the first and the second reaction chambers being separated from one another by means of a porous carbon membrane (100, 110, 120, 130, 140, 150); (II) providing carbon monoxide and chlorine in the first reaction chamber; and simultaneously (III) providing a compound containing hydroxyl, thiol, amino and/or formamide groups in the second reaction chamber. The porous carbon membrane is configured to catalyse the reaction of carbon monoxide and chlorine to obtain phosgene, and to allow this formed phosgene to pass into the second reaction chamber. The invention also relates to a reactor that is suitable for carrying out the claimed method.
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公开(公告)号：US09586927B2
公开(公告)日：2017-03-07
申请号：US14903225
申请日：2014-07-18
Applicant: MARUZEN PETROCHEMICAL CO., LTD. , NATIONAL INSTITUTE OF ADVANCED INDUSTRIAL SCIENCE AND TECHNOLOGY
Inventor： Takashi Naniki , Yasunori Hayashi , Goro Sawada , Takuro Furukawa , Takeshi Haruna , Toshikazu Takahashi , Hiroyuki Yasuda , Shouji Yamamoto
IPC: C07D317/08 , C07D317/38 , B01J31/02
CPC classification number: C07D317/38 , B01J27/08 , B01J31/0231 , B01J31/0239 , B01J31/0254 , B01J31/0268 , B01J31/0269 , B01J31/0271 , B01J2231/341 , B01J2531/90
Abstract: Provided is a method for continuously producing a cyclic carbonate, by which generation of a glycol in a reaction for synthesizing a cyclic carbonate is suppressed, and a cyclic carbonate having a high purity can be efficiently obtained even by simple purification.A method for continuously producing a cyclic carbonate, including filling a catalyst in a fixed-bed tube reactor, and continuously feeding carbon dioxide and an epoxide to the fixed-bed tube reactor to thereby bringing the carbon dioxide and the epoxide into contact with the catalyst, while continuously withdrawing the reaction liquid in the fixed-bed tube reactor, wherein the method includes a pre-treatment step in which a pre-treatment liquid containing a cyclic carbonate is brought into contact with the catalyst before feeding the carbon dioxide and the epoxide to the fixed-bed tube reactor, and the generated glycol is removed out of the system.
Abstract translation: 一种连续生产环状碳酸酯的方法，包括在固定床管式反应器中填充催化剂，并将二氧化碳和环氧化物连续供给到固定床管式反应器中，从而使二氧化碳和环氧化物与催化剂接触 同时连续抽出固定床管式反应器中的反应液，其中该方法包括一预处理步骤，其中将含有环状碳酸酯的预处理液体与进料二氧化碳和环氧化物 到固定床管式反应器中，并将生成的二醇从系统中除去。
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公开(公告)号：US20160310936A1
公开(公告)日：2016-10-27
申请号：US15102428
申请日：2014-12-12
Applicant: SAUDI BASIC INDUSTRIES CORPORATION
Inventor： Roland Schmidt , Mohammed H. Al-Hazmi , Mohammed F. Al-Anazi , Pradhan DevRanjan
CPC classification number: B01J31/0212 , B01J31/02 , B01J31/0204 , B01J31/0231 , B01J31/0237 , B01J31/0274 , B01J31/0275 , B01J31/143 , B01J2231/12 , B01J2231/122 , B01J2231/20 , B01J2523/47 , B01J2531/004 , B01J2531/007 , C07C2/10 , C07C2/30 , C07C2531/02 , C07C2531/12 , C07C2531/14 , C08F2/04 , C08F10/00 , C08F10/02 , C08F10/08 , C08F110/02 , C08F2410/01 , C08F210/16 , C08F4/651 , C07C11/08
Abstract: A catalyst composition, including a titanate of the formula Ti(OR)4 wherein each R is the same or different, and is a hydrocarbon residue; a catalyst additive, wherein the catalyst additive is a dibutyl ether a silicate, a silazane, an aromatic ether, a fluorocarbon, or a combination comprising at least one of the foregoing; and an organic aluminium compound.
Abstract translation: 一种催化剂组合物，包括式Ti（OR）4的钛酸酯，其中每个R相同或不同，并且是烃残基; 催化剂添加剂，其中所述催化剂添加剂是二丁基醚硅酸盐，硅氮烷，芳族醚，碳氟化合物或包含至少一种前述物质的组合; 和有机铝化合物。
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公开(公告)号：US20160185691A1
公开(公告)日：2016-06-30
申请号：US14919557
申请日：2015-10-21
Inventor： John F. Hartwig , Hiroyuki Morimoto , Patrick Fier
IPC: C07C17/32 , C07C209/68 , C07C29/32 , C07B39/00 , C07D213/26 , C07D215/12 , C07D209/08 , C07C41/30 , C07C253/30
CPC classification number: C07C17/32 , B01J31/0231 , B01J31/0235 , B01J31/0244 , C07B39/00 , C07C17/263 , C07C22/08 , C07C29/32 , C07C37/11 , C07C41/30 , C07C41/48 , C07C45/63 , C07C45/68 , C07C67/293 , C07C67/343 , C07C201/12 , C07C209/68 , C07C231/12 , C07C253/30 , C07D209/08 , C07D209/10 , C07D213/26 , C07D213/61 , C07D215/12 , C07D215/18 , C07D239/22 , C07D239/54 , C07F1/08 , C07C43/225 , C07C33/46 , C07C47/55 , C07C49/80 , C07C69/63 , C07C43/1742 , C07C69/76 , C07C43/313 , C07C255/50 , C07C25/13 , C07C205/11 , C07C211/52 , C07C233/15
Abstract: A composition, consisting essentially of copper, a fluoroalkyl group, and a ligand comprising at least one group-V donor. The molar ratio of copper to the fluoroalkyl group is approximately 1.
Abstract translation: 一种组合物，其基本上由铜，氟代烷基和包含至少一个V族供体的配体组成。 铜与氟烷基的摩尔比约为1。
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公开(公告)号：US09193648B2
公开(公告)日：2015-11-24
申请号：US13770430
申请日：2013-02-19
Applicant: John F. Hartwig , Hiroyuki Morimoto , Patrick Fier
Inventor： John F. Hartwig , Hiroyuki Morimoto , Patrick Fier
IPC: C07C17/32 , C07C22/08 , C07B39/00 , C07C17/263 , C07C29/32 , C07C41/30 , C07C41/48 , C07C45/68 , C07C67/293 , C07C67/343 , C07C201/12 , C07C209/68 , C07C231/12 , C07C253/30 , C07D209/10 , C07D213/26 , C07D215/18 , C07D239/54 , C07F1/08 , C07C37/11 , C07C45/63 , C07D209/08 , C07D213/61 , C07D239/22
CPC classification number: C07C17/32 , B01J31/0231 , B01J31/0235 , B01J31/0244 , C07B39/00 , C07C17/263 , C07C22/08 , C07C29/32 , C07C37/11 , C07C41/30 , C07C41/48 , C07C45/63 , C07C45/68 , C07C67/293 , C07C67/343 , C07C201/12 , C07C209/68 , C07C231/12 , C07C253/30 , C07D209/08 , C07D209/10 , C07D213/26 , C07D213/61 , C07D215/12 , C07D215/18 , C07D239/22 , C07D239/54 , C07F1/08 , C07C43/225 , C07C33/46 , C07C47/55 , C07C49/80 , C07C69/63 , C07C43/1742 , C07C69/76 , C07C43/313 , C07C255/50 , C07C25/13 , C07C205/11 , C07C211/52 , C07C233/15
Abstract: A method of forming a fluorinated molecular entity includes reacting in a reaction mixture an aromatic halide, copper, a fluoroalkyl group, and a ligand. The aromatic halide includes an aromatic group and a halogen substituent bonded to the aromatic group. The ligand includes at least one group-V donor selected from phosphorus and an amine. The overall molar ratio of copper to aromatic halide in the reaction mixture is from 0.2 to 3. The method further includes forming a fluoroalkylarene including the aromatic group and the fluoroalkyl group bonded to the aromatic group. A composition, which may be used in the method, consists essentially of copper, the fluoroalkyl group, and the ligand, where the molar ratio of copper to the fluoroalkyl group is approximately 1.
Abstract translation: 形成氟化分子实体的方法包括在反应混合物中使芳族卤化物，铜，氟烷基和配体反应。 芳族卤化物包括芳族基团和与该芳族基团键合的卤素取代基。 配体包括至少一种选自磷和胺的V族供体。 反应混合物中铜与芳族卤化物的总摩尔比为0.2-3。该方法还包括形成包括芳族基团和与芳基键合的氟代烷基的氟烷基芳烃。 可用于该方法的组合物基本上由铜，氟代烷基和配体组成，其中铜与氟烷基的摩尔比约为1。
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Patent Agency Ranking
6.发明授权Compositions containing fluorine substituted olefins and methods and systems using same 有权含氟取代烯烃的组合物及其使用方法和系统公开(公告)号：US09157017B2
公开(公告)日：2015-10-13
申请号：US14225588
申请日：2014-03-26
Applicant: Honeywell International Inc.
Inventor： Rajiv R. Singh , Hang T. Pham , Ian Shankland
CPC classification number: C09K5/045 , A01N29/00 , A23L27/202 , A23V2002/00 , A61K9/008 , A61K47/06 , A61L2/18 , A62D1/00 , A62D1/0028 , A62D1/0057 , B01J31/0231 , B01J37/03 , B01J37/035 , C07C21/18 , C08J9/146 , C08J2203/164 , C08J2207/04 , C08J2325/06 , C09D7/20 , C09K3/00 , C09K3/30 , C09K21/08 , C09K2205/12 , C09K2205/126 , C09K2205/22 , C09K2205/24 , C11B9/0007 , C11D3/245 , C11D11/0047 , C11D17/0043 , Y02A40/965
Abstract: Disclosed are the use of fluorine substituted olefins, including tetra- and penta-fluoropropenes, in a variety of applications, including in methods of depositing catalyst on a solid support, methods of sterilizing articles, cleaning methods and compositions, methods of applying medicaments, fire extinguishing/suppression compositions and methods, flavor formulations, fragrance formulations and inflating agents.
Abstract translation: 公开了在各种应用中使用氟取代的烯烃，包括四氟和五氟丙烯，包括在固体载体上沉积催化剂的方法，消毒制品的方法，清洁方法和组合物，施用药物的方法，火 灭火/抑制组合物和方法，风味剂，香料配方和充气剂。
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公开(公告)号：US09102606B2
公开(公告)日：2015-08-11
申请号：US14398806
申请日：2013-05-08
Applicant: MITSUBISHI GAS CHEMICAL COMPANY, INC.
Inventor： Masaki Sugita
IPC: C07C45/50
CPC classification number: C07C45/505 , B01J31/0231 , B01J2231/321 , C07C45/50 , C07C47/02
Abstract: A method for producing a branched chain aldehyde, comprising: reacting an aliphatic olefin having a double bond at an end with carbon monoxide and hydrogen using an iodide of a Group 9 metal as a catalyst and at least one or more selected from the group consisting of hydrogen iodide and alkyl iodides as a promoter.
Abstract translation: 一种支链醛的制造方法，其特征在于，包括：使用第9族金属的碘化物作为催化剂使末端具有双键的脂肪族烯烃与一氧化碳和氢气反应，以及选自以下的至少一种或多种： 碘化氢和烷基碘化物作为助催化剂。
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公开(公告)号：US20130225815A1
公开(公告)日：2013-08-29
申请号：US13770430
申请日：2013-02-19
Applicant: John F. Hartwig , Hiroyuki Morimoto , Patrick Fier
Inventor： John F. Hartwig , Hiroyuki Morimoto , Patrick Fier
IPC: C07C17/32 , C07C209/68 , C07C37/11 , C07C45/63 , C07F1/08 , C07C201/12 , C07D213/61 , C07D239/22 , C07D215/18 , C07D209/08 , C07C41/30 , C07C253/30
CPC classification number: C07C17/32 , B01J31/0231 , B01J31/0235 , B01J31/0244 , C07B39/00 , C07C17/263 , C07C22/08 , C07C29/32 , C07C37/11 , C07C41/30 , C07C41/48 , C07C45/63 , C07C45/68 , C07C67/293 , C07C67/343 , C07C201/12 , C07C209/68 , C07C231/12 , C07C253/30 , C07D209/08 , C07D209/10 , C07D213/26 , C07D213/61 , C07D215/12 , C07D215/18 , C07D239/22 , C07D239/54 , C07F1/08 , C07C43/225 , C07C33/46 , C07C47/55 , C07C49/80 , C07C69/63 , C07C43/1742 , C07C69/76 , C07C43/313 , C07C255/50 , C07C25/13 , C07C205/11 , C07C211/52 , C07C233/15
Abstract: A method of forming a fluorinated molecular entity includes reacting in a reaction mixture an aromatic halide, copper, a fluoroalkyl group, and a ligand. The aromatic halide includes an aromatic group and a halogen substituent bonded to the aromatic group. The ligand includes at least one group-V donor selected from phosphorus and an amine. The overall molar ratio of copper to aromatic halide in the reaction mixture is from 0.2 to 3. The method further includes forming a fluoroalkylarene including the aromatic group and the fluoroalkyl group bonded to the aromatic group. A composition, which may be used in the method, consists essentially of copper, the fluoroalkyl group, and the ligand, where the molar ratio of copper to the fluoroalkyl group is approximately 1.
Abstract translation: 形成氟化分子实体的方法包括在反应混合物中使芳族卤化物，铜，氟烷基和配体反应。 芳族卤化物包括芳族基团和与该芳族基团键合的卤素取代基。 配体包括至少一个选自磷和胺的V族供体。 反应混合物中铜与芳族卤化物的总摩尔比为0.2-3。该方法还包括形成包括芳族基团和与芳基键合的氟代烷基的氟烷基芳烃。 可用于该方法的组合物基本上由铜，氟代烷基和配体组成，其中铜与氟烷基的摩尔比约为1。
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公开(公告)号：US20130172601A1
公开(公告)日：2013-07-04
申请号：US13716336
申请日：2012-12-17
Applicant: Eastman Chemical Company
Inventor： Zhidong George Zhu , Gerald Charles Tustin , Joseph Robert Zoeller , Mary Kathleen Moore , David Alan Jenkins
CPC classification number: B01J23/62 , B01J21/18 , B01J23/60 , B01J23/624 , B01J31/0231 , B01J37/0201 , B01J37/0215 , B01J37/0236 , B01J37/08 , C07C51/12 , C07C67/36 , C07C69/14 , C07C53/08
Abstract: A solid catalyst comprising an effective amount of iridium and at least one second metal selected from gallium, zinc, indium and germanium associated with a solid support material is useful for vapor phase carbonylation to produce carboxylic acids and esters from alkyl alcohols, esters, ethers or ester-alcohol mixtures. The iridium and at least one second metal are deposited on a support material. In some embodiments of the invention, the catalyst is useful for vapor phase carbonylation.
Abstract translation: 包含有效量的铱和选自与固体支持材料相关的镓，锌，铟和锗的至少一种第二金属的固体催化剂可用于汽相羰基化从烷基醇，酯，醚或其它物质制备羧酸和酯 酯 - 醇混合物。 铱和至少一个第二金属沉积在支撑材料上。 在本发明的一些实施方案中，催化剂可用于汽相羰基化。
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公开(公告)号：US20130090508A1
公开(公告)日：2013-04-11
申请号：US13704961
申请日：2011-06-03
Applicant: Gang Wang , Baojun Zhang , Jianzhong Li , Sihan Wang , Jiabo Qu , Defu He , Guizhi Wang , Qian Chen , Buwei Yu , Deshun Zhang , Libo Wang , Yali Wang , Liwei Liang , Yuxin Gao , Jie Li , Wenchao Zhang , Hua Li , Xiaoyu Gao , Shouhui Zha , Fuling Huang , Jing Wei , Xiuhui Wang , Xiangmin Yu , Jingying Zhao , Xuemei Han , Chunfeng Song , Junfeng Wei , Rui Meng
Inventor： Gang Wang , Baojun Zhang , Jianzhong Li , Sihan Wang , Jiabo Qu , Defu He , Guizhi Wang , Qian Chen , Buwei Yu , Deshun Zhang , Libo Wang , Yali Wang , Liwei Liang , Yuxin Gao , Jie Li , Wenchao Zhang , Hua Li , Xiaoyu Gao , Shouhui Zha , Fuling Huang , Jing Wei , Xiuhui Wang , Xiangmin Yu , Jingying Zhao , Xuemei Han , Chunfeng Song , Junfeng Wei , Rui Meng
IPC: C07C2/30
CPC classification number: C07C2/30 , B01J31/0231 , B01J31/143 , B01J31/2409 , B01J2231/20 , B01J2531/62 , C07C2/32 , C07C2531/02 , C07C2531/14 , C07C2531/22 , C07C11/02
Abstract: Disclosed is a method for preparing 1-octene in the presence of a catalyst system for ethylene oligomerization, which includes: premixing a part of ethylene gas as raw material with a solvent, mixing with the components a+b, c and d of the catalyst system, and then sending in a reactor; directly sending the rest of ethylene gas in the reactor; discharging the resultant liquid from the upper part of the reactor into an overflow channel; adding a catalysis stopping agent to the overflow channel; and then separating the resultant liquid. The advantages of the method are high selectivity of 1-octene and high catalytic activity.
Abstract translation: 公开了一种在乙烯低聚催化剂体系存在下制备1-辛烯的方法，其包括：将一部分乙烯气作为原料预先混合溶剂，与催化剂的组分a + b，c和d混合 系统，然后在反应堆中发送; 直接将其余的乙烯气体送回反应堆; 将得到的液体从反应器的上部排出到溢流通道中; 向溢流通道加入催化剂; 然后分离所得液体。 该方法的优点是1-辛烯的高选择性和高催化活性。
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